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1. 发明授权

US07081202B2 Composite semipermeable membrane, production method thereof, and water treatment method using the same 失效
标题翻译：复合半透膜及其制造方法及使用其的水处理方法
公开(公告)号：US07081202B2
公开(公告)日：2006-07-25
申请号：US10296836
申请日：2002-03-08
申请人： Tomomi Ohara , Masahiko Hirose , Naoki Kurata
发明人： Tomomi Ohara , Masahiko Hirose , Naoki Kurata
IPC分类号： B01D63/00 , B01D71/56 , B01D61/00
CPC分类号： B01D67/0093 , B01D65/022 , B01D69/125 , B01D71/56 , B01D2321/168 , C02F1/441
摘要： A composite semipermeable membrance of the present invention comprises a thin film and a porous support membrane supporting the thin film, wherein the thin film includes polyamide based resin having a constituent unit with amide bond between diamine residue and di or tri carboxylic acid residue, in which nitrogen atom of the amide bond has a substituent of aromatic ring. A production method of this invention includes a contacting step of contacting the above composite semipermeable membrane with solution including an oxidizer. In addition, a water treatment method of this invention comprises a step of separating a raw water by a composite semipermeable membrane to obtain permeation water in which salt and/or organic substance is removed sufficiently in practical use, characterized in that the composite semipermeable membrane of this invention is used and a fungicide is added into the raw water.This invention provides a composite semipermeable membrane having practically permeability, and excellent desalting faculty and oxidizer resistance, a production method thereof, and water treatment method using the same.
摘要翻译：本发明的复合半透膜包括薄膜和支撑薄膜的多孔支撑膜，其中薄膜包括具有二胺残基和二或三羧酸残基之间具有酰胺键的构成单元的聚酰胺基树脂，其中酰胺键的氮原子具有芳环的取代基。本发明的制备方法包括使上述复合半透膜与包含氧化剂的溶液接触的接触步骤。此外，本发明的水处理方法包括通过复合半透膜分离原水以获得其中盐和/或有机物质在实际应用中被充分除去的渗透水的步骤，其特征在于，所述复合半透膜使用本发明，并将杀真菌剂加入原水中。本发明提供一种具有实用渗透性，优异的脱盐剂和耐氧化剂性的复合半透膜及其制造方法以及使用其的水处理方法。

2. 发明授权

US5733602A Method for producing highly permeable composite reverse osmosis membrane 失效
标题翻译：生产高渗透复合反渗透膜的方法
公开(公告)号：US5733602A
公开(公告)日：1998-03-31
申请号：US577158
申请日：1995-12-22
申请人： Masahiko Hirose , Hiroki Ito , Tomomi Ohara
发明人： Masahiko Hirose , Hiroki Ito , Tomomi Ohara
IPC分类号： B01D71/56 , B01D69/12 , B01D71/82 , B05D3/10 , B05D5/00 , C23C16/00
CPC分类号： B01D69/125
摘要： Disclosed is a method for producing a composite reverse osmosis membrane comprising the steps of coating a porous support with (A) a solution containing a compound having at least two reactive amino groups per molecule and bringing (B) a solution containing a polyfunctional acid halide into contact with the solution (A) to induce crosslinking to form a crosslinked polyamide skin layer, in which the crosslinking is carried out in the presence of a substance having a solubility parameter of 8 to 14 (cal/cm.sup.3).sup.1/2. The resulting composite reverse osmosis membrane exhibits high salt rejection and high water permeability.
摘要翻译：公开了一种复合反渗透膜的制造方法，其特征在于，包括以下步骤：（A）含有每分子具有至少2个反应性氨基的化合物的溶液，使（B）含有多官能酰卤的溶液与溶液（A）接触以诱导交联以形成交联的聚酰胺表层，其中交联在溶解度参数为8-14（cal / cm 3）+ E的物质的存在下进行， 2 + EE。所得到的复合反渗透膜具有高的耐盐析和高透水性。

3. 发明授权

US06723422B1 Composite reverse osmosis membrane and process for preparing the same 失效
标题翻译：复合反渗透膜及其制备方法
公开(公告)号：US06723422B1
公开(公告)日：2004-04-20
申请号：US09462109
申请日：1999-12-30
申请人： Masahiko Hirose , Hiroki Ito , Tomomi Ohara
发明人： Masahiko Hirose , Hiroki Ito , Tomomi Ohara
IPC分类号： B32B2000
CPC分类号： B01D69/02 , B01D69/125 , B01D71/56 , B32B27/34 , Y10T428/249987 , Y10T428/249991 , Y10T428/249992
摘要： A composite reverse osmosis membrane is described, which includes a polyamide skin layer on a porous support, with a contact angle between the polyamide skin layer surface and water of 45° or less. The composite reverse osmosis membrane has a high salt rejection and also a high water permeability. This composite reverse osmosis membrane is produced by forming a polyamide skin layer on a porous support having the steps of: forming a layer on the porous support by coating a solution A including one or more compounds having at least two reactive amino groups; contacting the layer with a solution B comprising one or more polyfunctional acid halide compounds; and subsequently, contacting the layer with a solution C comprising the polyfunctional acid halide compound of a higher concentration than the solution C. The concentration of the polyfunctional acid halide compound in the solution C is preferably at least 1.2 times of the solution B.
摘要翻译：描述了一种复合反渗透膜，其包括多孔载体上的聚酰胺表层，聚酰胺表层与水之间的接触角为45°以下。复合反渗透膜具有高的耐盐性和高透水性。该复合反渗透膜是通过在多孔载体上形成聚酰胺表皮层而制成的，其具有以下步骤：通过涂覆包含一种或多种具有至少两个反应性氨基的化合物的溶液A在多孔载体上形成层; 使该层与包含一种或多种多官能酰卤化合物的溶液B接触; 并且随后使该层与包含比溶液C更高浓度的多官能酰卤化合物的溶液C接触。溶液C中多官能酰卤化合物的浓度优选为溶液B的至少1.2倍。

4. 发明授权

US06171497B2 Highly permeable composite reverse osmosis membrane 失效
标题翻译：高透性复合反渗透膜
公开(公告)号：US06171497B2
公开(公告)日：2001-01-09
申请号：US08786628
申请日：1997-01-21
申请人： Masahiko Hirose , Tomomi Ohara , Masaaki Ando
发明人： Masahiko Hirose , Tomomi Ohara , Masaaki Ando
IPC分类号： B01D7156
CPC分类号： B01D67/0093 , B01D69/125 , B01D2323/30
摘要： A module that can be practically used at a pressure of about 3 kgf/cm2 is obtained by treating a polyamide based reverse osmosis membrane with an oxidizing agent. A composite reverse osmosis membrane comprises a thin film which is a polyamide based skin layer obtained by polycondensation of a compound having two or more reactive amino groups and a polyfunctional acid halide compound having two or more reactive acid halide groups, and a microporous support for supporting the thin film. The polyamide based skin layer formed on the surface of the membrane has a mean roughness of 50 nm or more. The composite reverse osmosis membrane is treated with an oxidizing agent. A salt rejection of 99% or more and a flux of 1.5 m3/m2·day or more are obtained when evaluated by using a solution having pH 6.5 containing 500 ppm of sodium chloride at an operating pressure of 7.5 kgf/cm2 and a temperature of 25° C.
摘要翻译：通过用氧化剂处理聚酰胺类反渗透膜，可以在约3kgf / cm 2的压力下实际使用的模块。复合反渗透膜包括通过具有两个或更多个反应性氨基的化合物和具有两个或更多个反应性酰卤基团的多官能酰卤化合物缩聚获得的聚酰胺基皮层的薄膜和用于支撑的多孔载体薄膜。形成在膜表面的聚酰胺类皮肤层的平均粗糙度为50nm以上。复合反渗透膜用氧化剂处理。当在7.5kgf / cm 2的操作压力下使用含有500ppm氯化钠的pH6.5的溶液进行评价时，可以获得99％以上的脱盐率和1.5m 3 / m 2·天以上的通量， 25°C

5. 发明授权

US6024873A Highly permeable composite reverse osmosis membrane and a reverse osmosis membrane module using the same 失效
标题翻译：高透性复合反渗透膜和使用其的反渗透膜组件
公开(公告)号：US6024873A
公开(公告)日：2000-02-15
申请号：US819326
申请日：1997-03-18
申请人： Masahiko Hirose , Hiroki Ito , Tomomi Ohara
发明人： Masahiko Hirose , Hiroki Ito , Tomomi Ohara
IPC分类号： B01D61/02 , B01D69/12 , B01D71/64 , B01D29/00
CPC分类号： B01D69/125
摘要： The present invention provides a composite reverse osmosis membrane and a reverse osmosis membrane module using the same, having a high salt rejection, high water permeability, and a high rejection of organic substances such as isopropyl alcohol, which can be used to remove organic substances as well as ionic substances with suitable efficiency and economy. The highly permeable composite reverse osmosis membrane of the invention can be produced by adding alcohols or ethers or the like having a solubility parameter of 8-14 (cal/cm.sup.3).sup.1/2 to the solution containing at least one compound selected from the group consisting of a compound having two or more reactive amino groups and a polyfunctional acid halide having two or more reactive acid halide groups which is used when conducting the polycondensation of a compound having two or more reactive amino groups and a polyfunctional acid halide having two or more reactive acid halide groups on a microporous support.
摘要翻译：本发明提供一种复合反渗透膜和使用该复合反渗透膜组件的反渗透膜组件，其具有高的耐盐析性，高透水性，以及异丙醇等有机物质的高排斥性，可用于除去有机物质作为以及具有合适效率和经济性的离子物质。本发明的高渗透性复合反渗透膜可以通过将溶解度参数为8-14（cal / cm 3）+ E，fra 1/2 + EE的醇或醚等加入到含有至少一种选自具有两个或更多个反应性氨基的化合物和具有两个或多个反应性酰卤基团的多官能酰卤的化合物，其在进行具有两个或多个反应性氨基的化合物的缩聚时使用的多官能酸在微孔载体上具有两个或多个反应性酰卤基团的卤化物。

6. 发明授权

US08348289B2 Rack-and-pinion mechanism and steering system 有权
标题翻译：齿条齿轮机构和转向系统
公开(公告)号：US08348289B2
公开(公告)日：2013-01-08
申请号：US13008451
申请日：2011-01-18
申请人： Takahiro Tanaka , Masahiko Hirose , Yoshiaki Izumi
发明人： Takahiro Tanaka , Masahiko Hirose , Yoshiaki Izumi
IPC分类号： B62D3/12
CPC分类号： B62D3/123 , F16H55/283 , Y10T74/18088
摘要： With a rack-and-pinion mechanism, an impact force is absorbed and reduction in assembling performance is suppressed. An annular fitting groove (51) that extends in the circumferential direction of a rack guide (41) is formed in an outer peripheral face (41a) of the rack guide (41), and an O-ring (52) is fitted in the fitting groove (51) in a state in which the axial movement of the O-ring (52) is restricted. A communication groove (61) that provides communication between an internal space (55), defined by the fitting groove (51) and the O-ring (52), and the outside of the rack guide (41) is formed in the rack guide (41).
摘要翻译：利用齿条齿轮机构，吸收冲击力并抑制组装性能的降低。在齿条引导件（41）的外周面（41a）上形成有在齿条引导件（41）的圆周方向上延伸的环形嵌合槽（51），并且O形环在所述O形环（52）的轴向移动受到限制的状态下的嵌合槽（51）。在所述齿条引导件中形成有在由所述嵌合槽（51）和所述O形环（52）限定的内部空间（55）与所述齿条引导件（41）的外部之间提供连通的连通槽（61）（41）。

7. 发明授权

US07739793B2 Method of manufacturing rack guide base body in rack-and-pinion type steering apparatus and rack guide 有权
标题翻译：齿条 - 小齿轮转向装置和齿条引导件中的齿条引导件基体的制造方法
公开(公告)号：US07739793B2
公开(公告)日：2010-06-22
申请号：US11587954
申请日：2005-04-26
申请人： Kazuhiro Yamamoto , Masao Shimura , Yoshiro Kuzumi , Masahiko Hirose , Masaaki Hashimoto , Takahiro Tanaka , Katsutoshi Nishimura
发明人： Kazuhiro Yamamoto , Masao Shimura , Yoshiro Kuzumi , Masahiko Hirose , Masaaki Hashimoto , Takahiro Tanaka , Katsutoshi Nishimura
IPC分类号： B21D53/28 , F16H1/04
CPC分类号： B22D17/22 , B62D3/123 , F16H55/283 , Y10T29/49474 , Y10T29/49988 , Y10T29/49989 , Y10T74/1967
摘要： A method of manufacturing a rack guide base body wherein a cavity (40) is formed which has a pair of semicylindrical convex surfaces (44a and 44b) and a pair of flat surfaces (45) each located between the semicylindrical convex surfaces (44a and 44b), and has a recessed surface (41) located on one axial end portion side inwardly of the semicylindrical convex surfaces (44a and 44b) and the flat surfaces (45) and a cylindrical surface (42) located on the other axial end portion side inwardly of the semicylindrical convex surfaces (44a and 44b) and the flat surfaces (45); a hollow portion (9c) is formed for allowing the cavity (40) to communicate with a hollow portion (10c) at one flat surface (45) and with a hollow portion (8c) at the other flat surface (45); a rack guide base body (50) is die cast by forcing molten metal of aluminum from the hollow portion (10c) into the cavity (40); and runners (56) integrally joined to flat surfaces (55) of the rack guide base body (50) formed by the respective flat surfaces (45) are cut off.
摘要翻译：一种制造齿条导向器基体的方法，其中形成有一对半圆柱形凸表面（44a和44b）和一对平面（45）的空腔（40），所述一对平面位于所述半圆柱形凸表面（44a和44b）之间），并且具有位于半圆柱形凸表面（44a和44b）的内侧的一个轴向端部侧上的凹面（41）和位于另一轴向端部侧的平面（45）和圆柱面（42）在半圆柱形凸表面（44a和44b）和平坦表面（45）的内部; 形成中空部分（9c），用于允许空腔（40）在一个平坦表面（45）处与中空部分（10c）连通，并且在另一个平坦表面（45）处与中空部分（8c）连通; 通过将铝的熔融金属从中空部分（10c）推入空腔（40）而将铸造导体基体（50）压铸成型; 并且与由各个平面（45）形成的齿条导向器基体（50）的平坦表面（55）整体接合的流道（56）被切断。

8. 发明申请

US20090263206A1 Method and Structure for Preventing Screw From Loosening and Method of Manufacturing Male Screw 审中-公开
标题翻译：用于防止松动螺丝的方法和结构以及制造螺丝的方法
公开(公告)号：US20090263206A1
公开(公告)日：2009-10-22
申请号：US11989368
申请日：2005-07-29
申请人： Masahiko Hirose , Masaaki Hashimoto , Katsutoshi Nishimura , Katsuaki Mitsuda
发明人： Masahiko Hirose , Masaaki Hashimoto , Katsutoshi Nishimura , Katsuaki Mitsuda
IPC分类号： F16B39/00 , F16B39/30 , B21H3/02
CPC分类号： B62D3/123 , F16B39/284 , F16H55/283
摘要： Prior to engaging a male screw formed on the outer circumference of a second member with a female screw formed on the inner circumference of a hole in a first member, protruding parts which protrude outward in the radial direction and are positioned at one end side of the male screw in the axial direction are formed in a plurality of regions which are separated from each other in the circumferential direction on the outer circumference of the second member on which the male screw is formed. The male screw is then engaged with the female screw from the other end side of the male screw in the axial direction. The torque required to rotate the male screw engaged with the female screw in the loosening direction is set so as to be greater in a state where the protruding parts are interposed between the male screw and the female screw than in a state where the protruding parts are not so interposed.
摘要翻译：在形成在第二构件的外周上的外螺纹与形成在第一构件的孔的内周上的内螺纹接合之前，沿径向向外突出并位于第一构件的一端侧的突出部外螺纹沿轴向形成在多个区域中，该多个区域在形成有外螺纹的第二构件的外周上沿圆周方向彼此分离。然后将外螺纹从外螺纹的另一端侧沿轴向与内螺纹接合。在突出部分为凸状部分的状态下，突出部分插入在阳螺纹和阴螺纹之间的状态下，将与松动方向啮合的外螺纹旋转的扭矩设定得较大没有插入

9. 发明授权

US5843351A Highly permeable composite reverse osmosis membrane, method of producing the same 失效
标题翻译：高透性复合反渗透膜，其生产方法
公开(公告)号：US5843351A
公开(公告)日：1998-12-01
申请号：US702383
申请日：1996-08-14
申请人： Masahiko Hirose , Hiroki Ito , Masatoshi Maeda , Kazuo Tanaka
发明人： Masahiko Hirose , Hiroki Ito , Masatoshi Maeda , Kazuo Tanaka
IPC分类号： B01D61/02 , B01D67/00 , B01D69/00 , B01D69/12 , B29D33/48
CPC分类号： B01D67/0088 , B01D61/022 , B01D69/00 , B01D69/12 , B01D69/125
摘要： This invention provides a composite reverse osmosis membrane having a polyamide type skin layer whose average surface roughness is at least 55 nm, and the polyamide type skin layer comprises the reaction product of a compound having amino groups and polyfunctional acid halide compound having acid halide groups. The composite reverse osmosis membrane of this invention is superior in salt rejection and water permeability. A polymer film is formed on a supporting film by contacting a solution containing e.g., m-phenylenediamine with a porous polysulfone supporting film so as to form a layer of the solution on the supporting film, then contacting the film with a solution of trimesic acid chloride and holding the film in a hot air dryer so that a polymer film is formed on the supporting film. The surface of the polyamide type skin layer can also be treated with quaternary ammonium salt and coated with a crosslinked layer of an organic polymer having positively-charged groups. Raw liquid is transmitted from a raw liquid tank to a membrane module for the first stage through a first transmission pump, and the first stage of reverse osmosis treatment is carried out. The composite reverse osmosis membrane coated with the crosslinked layer is used when another reverse osmosis treatment is carried out by using another membrane module for the second stage.
摘要翻译：本发明提供一种具有平均表面粗糙度为55nm以上的聚酰胺型表层的复合反渗透膜，聚酰胺型表皮层包含具有氨基的化合物与具有酰卤基的多官能酰卤化合物的反应产物。本发明的复合反渗透膜的耐盐析性和透水性优异。通过使含有例如间苯二胺的溶液与多孔聚砜负载膜接触，在支持膜上形成聚合物膜，以在支撑膜上形成溶液层，然后将该膜与均苯三甲酸并将膜保持在热空气干燥器中，使得在支撑膜上形成聚合物膜。聚酰胺型表皮层的表面也可以用季铵盐处理，并涂布有具有带正电荷基团的有机聚合物的交联层。原料液体通过第一传动泵从原液槽传送到第一级的膜组件，并进行第一阶段的反渗透处理。当通过使用用于第二阶段的另一个膜组件进行另一个反渗透处理时，使用涂覆有交联层的复合反渗透膜。

10. 发明授权

US5614099A Highly permeable composite reverse osmosis membrane, method of producing the same, and method of using the same 失效
标题翻译：高透性复合反渗透膜及其制造方法及其使用方法
公开(公告)号：US5614099A
公开(公告)日：1997-03-25
申请号：US572900
申请日：1995-12-18
申请人： Masahiko Hirose , Hiroki Ito , Masatoshi Maeda , Kazuo Tanaka
发明人： Masahiko Hirose , Hiroki Ito , Masatoshi Maeda , Kazuo Tanaka
IPC分类号： B01D61/02 , B01D67/00 , B01D69/00 , B01D69/12 , B01D61/00
CPC分类号： B01D67/0088 , B01D61/022 , B01D69/00 , B01D69/12 , B01D69/125
摘要： This invention provides a composite reverse osmosis membrane having a polyamide type skin layer whose average surface roughness is at least 55 nm, and the polyamide type skin layer comprises the reaction product of a compound having amino groups and polyfunctional acid halide compound having acid halide groups. The composite reverse osmosis membrane of this invention is superior in salt rejection and water permeability. A polymer film is formed on a supporting film by contacting a solution containing e.g., m-phenylenediamine with a porous polysulfone supporting film so as to form a layer of the solution on the supporting film, then contacting the film with a solution of trimesic acid chloride and holding the film in a hot air dryer so that a polymer film is formed on the supporting film. The surface of the polyamide type skin layer can also be treated with quaternary ammonium salt and coated with a crosslinked layer of an organic polymer having positively-charged groups. Raw liquid is transmitted from a raw liquid tank to a membrane module for the first stage through a first transmission pump, and the first stage of reverse osmosis treatment is carried out. The composite reverse osmosis membrane coated with the crosslinked layer is used when another reverse osmosis treatment is carried out by using another membrane module for the second stage.
摘要翻译：本发明提供一种具有平均表面粗糙度为55nm以上的聚酰胺型表层的复合反渗透膜，聚酰胺型表皮层包含具有氨基的化合物与具有酰卤基的多官能酰卤化合物的反应产物。本发明的复合反渗透膜的耐盐析性和透水性优异。通过使含有例如间苯二胺的溶液与多孔聚砜负载膜接触，在支撑膜上形成聚合物膜，以在支撑膜上形成溶液层，然后将该膜与均苯三甲酸并将膜保持在热空气干燥器中，使得在支撑膜上形成聚合物膜。聚酰胺型表皮层的表面也可以用季铵盐处理，并涂布有具有带正电荷基团的有机聚合物的交联层。原料液体通过第一传动泵从原液槽传送到第一级的膜组件，并进行第一阶段的反渗透处理。当通过使用用于第二阶段的另一个膜组件进行另一个反渗透处理时，使用涂覆有交联层的复合反渗透膜。

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