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1. 发明申请

US20110294941A1 VINYL CHLORIDE-BASED RESIN COMPOSITION, METHOD OF PRODUCING VINYL CHLORIDE-BASED POLYMER COMPOSITION, AND VINYL CHLORIDE-BASED POLYMER COMPOSITION OBTAINED THEREBY 审中-公开
标题翻译：基于氯乙烯的树脂组合物，基于氯乙烯的聚合物组合物的制备方法和基于氯乙烯的聚合物组合物
公开(公告)号：US20110294941A1
公开(公告)日：2011-12-01
申请号：US13115369
申请日：2011-05-25
申请人： Tatsuya FUJIMOTO , Tadashi Amano , Manabu Furudate , Tomohiro Inoue , Shinji Fujimoto , Ken Yahata
发明人： Tatsuya FUJIMOTO , Tadashi Amano , Manabu Furudate , Tomohiro Inoue , Shinji Fujimoto , Ken Yahata
IPC分类号： C08K3/22 , B82Y30/00
CPC分类号： B82Y30/00
摘要： Provided is a vinyl chloride-based resin composition including a vinyl chloride-based resin and a titanium dioxide having an average particle diameter of 5 to 50 nm, in an amount of 1,000 ppm to 10,000 ppm, by mass, relative to the mass of the vinyl chloride-based resin. By adding a titanium dioxide having an average particle diameter of 5 to 50 nm to a vinyl chloride-based resin in an amount described above, a vinyl chloride-based resin composition of excellent thermal stability can be obtained. In the vinyl chloride-based resin composition, the crystalline form of the titanium dioxide is preferably anatase, rutile, or a combination thereof. Also provided is a method of producing a vinyl chloride-based polymer composition that includes subjecting a vinyl chloride monomer, or a mixture of a vinyl chloride monomer and a monomer that is copolymerizable therewith, to suspension polymerization within an aqueous medium, and also includes adding a titanium dioxide having an average particle diameter of 5 to 50 nm to the raw material prior to commencement of the polymerization, to the reaction mixture during the polymerization, to the reaction product following completion of the polymerization, or to a combination of two or more of the raw material, the reaction mixture and the reaction product. The vinyl chloride-based polymer composition obtained using this method exhibits excellent thermal stability.
摘要翻译：本发明提供一种氯乙烯类树脂组合物，其含有平均粒径为5〜50nm的氯乙烯类树脂和二氧化钛，相对于质量为1000〜10000ppm 氯乙烯类树脂。通过向上述量的氯乙烯类树脂中添加平均粒径为5〜50nm的二氧化钛，可以得到热稳定性优异的氯乙烯系树脂组合物。在氯乙烯系树脂组合物中，二氧化钛的结晶形态优选为锐钛矿型，金红石型，或其组合。还提供了一种生产氯乙烯基聚合物组合物的方法，该组合物包括使氯乙烯单体或氯乙烯单体与其可共聚的单体的混合物在水性介质中进行悬浮聚合，并且还包括加入在聚合开始前与原料平均粒径为5〜50nm的二氧化钛，聚合期间的反应混合物，聚合完成后的反应产物，或两种以上的组合的原料，反应混合物和反应产物。使用该方法获得的基于氯乙烯的聚合物组合物显示出优异的热稳定性。

2. 发明申请

US20060257660A1 Antistatic agent for vinyl chloride-based resins, vinyl chloride-based resin composition containing the same, and method for manufacturing this composition 失效
标题翻译：氯乙烯系树脂的防静电剂，含有它们的氯乙烯系树脂组合物及其制造方法
公开(公告)号：US20060257660A1
公开(公告)日：2006-11-16
申请号：US11430622
申请日：2006-05-09
申请人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
发明人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
IPC分类号： B32B5/16
CPC分类号： C08F6/008 , C08K3/36 , Y10T428/2982 , C08L27/06
摘要： The present invention provides an antistatic agent for vinyl chloride-based resins which can impart superior antistatic properties to the vinyl chloride-based resin, and which can thereby solve various problems arising from charging of the vinyl chloride-based resin with static electricity, a vinyl chloride-based resin composition containing this antistatic agent, and a method for manufacturing this composition. The present invention provides an antistatic agent for vinyl chloride-based resins which consists of silica particles containing at least 99.0% by mass of SiO2 and 0.00005% 80.5 ppm by mass or less of sodium, and which has such a particle size distribution that at least 98% by mass of the silica particles is occupied by the particles having a particle diameter in the range from 30 to 1,000 nm.
摘要翻译：本发明提供了一种氯乙烯类树脂的抗静电剂，其可以赋予氯乙烯类树脂优异的抗静电性能，从而可以解决由静电装入氯乙烯类树脂引起的各种问题，乙烯基含有该抗静电剂的氯化物系树脂组合物及其制造方法。本发明提供了一种氯乙烯类树脂的抗静电剂，其由含有至少99.0质量％SiO 2和0.00005％80.5质量ppm以下的二氧化硅粒子构成，其具有这样的粒度分布，使得至少98质量％的二氧化硅粒子被粒径在30〜1000nm的粒子占据。

3. 发明授权

US07847012B2 Vinyl chloride resin composition and molded article thereof 失效
标题翻译：氯乙烯树脂组合物及其模制品
公开(公告)号：US07847012B2
公开(公告)日：2010-12-07
申请号：US11758418
申请日：2007-06-05
申请人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
发明人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
IPC分类号： C08L27/06
CPC分类号： C08J9/0038 , C04B26/08 , C04B2111/00129 , C08J9/0066 , C08J2327/06 , C08K3/013 , C08K3/04 , C08K5/49 , C08L27/06 , C08L27/18 , C08L2205/02 , C04B14/024 , C04B14/042 , C04B14/06 , C04B14/10 , C04B14/28 , C04B14/303 , C04B14/304 , C04B14/305 , C04B24/003 , C04B24/2682 , C04B38/02 , C08L2666/04
摘要： A thermally expandable vinyl chloride resin composition is provided. It includes (A) 100 parts by mass of a vinyl chloride resin, (B) 5 to 200 parts by mass of an inorganic filler, (C) 10 to 300 parts by mass of a thermally expandable graphite, (D) 0.1 to 10 parts by mass of a fluororesin, and (E) 10 to 300 parts by mass of a phosphorus compound. The composition exhibits favorable thermal expansion properties and favorable shape retention following thermal expansion upon exposure to high temperatures.
摘要翻译：提供了一种热膨胀性氯乙烯树脂组合物。它包括（A）100质量份氯乙烯树脂，（B）5至200质量份无机填料，（C）10至300质量份可热膨胀石墨，（D）0.1至10 质量份的氟树脂，（E）10〜300质量份的磷化合物。该组合物在暴露于高温下时显示出良好的热膨胀性能和良好的热膨胀后的形状保持性。

4. 发明授权

US07514495B2 Antistatic agent for vinyl chloride-based resins, vinyl chloride-based resin composition containing the same, and method for manufacturing this composition 失效
标题翻译：氯乙烯系树脂的防静电剂，含有它们的氯乙烯系树脂组合物及其制造方法
公开(公告)号：US07514495B2
公开(公告)日：2009-04-07
申请号：US11430622
申请日：2006-05-09
申请人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
发明人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
IPC分类号： C08K3/36
CPC分类号： C08F6/008 , C08K3/36 , Y10T428/2982 , C08L27/06
摘要： The present invention provides an antistatic agent for vinyl chloride-based resins which can impart superior antistatic properties to the vinyl chloride-based resin, and which can thereby solve various problems arising from charging of the vinyl chloride-based resin with static electricity, a vinyl chloride-based resin composition containing this antistatic agent, and a method for manufacturing this composition. The present invention provides an antistatic agent for vinyl chloride-based resins which consists of silica particles containing at least 99.0% by mass of SiO2 and 0.00005% 80.5 ppm by mass or less of sodium, and which has such a particle size distribution that at least 98% by mass of the silica particles is occupied by the particles having a particle diameter in the range from 30 to 1,000 nm.
摘要翻译：本发明提供了一种氯乙烯类树脂的抗静电剂，其可以赋予氯乙烯类树脂优异的抗静电性能，从而可以解决由静电装入氯乙烯类树脂引起的各种问题，乙烯基含有该抗静电剂的氯化物系树脂组合物及其制造方法。本发明提供了一种氯乙烯类树脂的抗静电剂，其由含有至少99.0质量％的SiO 2和0.00005％的80.5质量ppm以下的二氧化硅粒子组成，并且其粒径分布至少为二氧化硅粒子的98质量％被粒径在30〜1000nm的粒子所占据。

5. 发明申请

US20070282027A1 VINYL CHLORIDE RESIN COMPOSITION AND MOLDED ARTICLE THEREOF 失效
标题翻译： VINYL氯化物树脂组合物及其成型品
公开(公告)号：US20070282027A1
公开(公告)日：2007-12-06
申请号：US11758418
申请日：2007-06-05
申请人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
发明人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
IPC分类号： C08L75/00
CPC分类号： C08J9/0038 , C04B26/08 , C04B2111/00129 , C08J9/0066 , C08J2327/06 , C08K3/013 , C08K3/04 , C08K5/49 , C08L27/06 , C08L27/18 , C08L2205/02 , C04B14/024 , C04B14/042 , C04B14/06 , C04B14/10 , C04B14/28 , C04B14/303 , C04B14/304 , C04B14/305 , C04B24/003 , C04B24/2682 , C04B38/02 , C08L2666/04
摘要： A thermally expandable vinyl chloride resin composition is provided. It includes (A) 100 parts by mass of a vinyl chloride resin, (B) 5 to 200 parts by mass of an inorganic filler, (C) 10 to 300 parts by mass of a thermally expandable graphite, (D) 0.1 to 10 parts by mass of a fluororesin, and (E) 10 to 300 parts by mass of a phosphorus compound. The composition exhibits favorable thermal expansion properties and favorable shape retention following thermal expansion upon exposure to high temperatures.
摘要翻译：提供了一种热膨胀性氯乙烯树脂组合物。它包括（A）100质量份氯乙烯树脂，（B）5至200质量份无机填料，（C）10至300质量份可热膨胀石墨，（D）0.1至10 质量份的氟树脂，（E）10〜300质量份的磷化合物。该组合物在暴露于高温下时显示出良好的热膨胀性能和良好的热膨胀后的形状保持性。

6. 发明授权

US5916675A Polycarbodiimide resin-containing adhesive and flexible printed circuit board 失效
标题翻译：含聚碳酰亚胺树脂的粘合剂和柔性印刷电路板
公开(公告)号：US5916675A
公开(公告)日：1999-06-29
申请号：US873947
申请日：1997-06-12
申请人： Yasuyoshi Komoto , Akira Hayashida , Michio Aizawa , Hitoshi Arai , Ken Yahata
发明人： Yasuyoshi Komoto , Akira Hayashida , Michio Aizawa , Hitoshi Arai , Ken Yahata
IPC分类号： B32B15/08 , C08G73/00 , C08G73/06 , H05K1/00 , H05K3/38 , B32B7/12
CPC分类号： H05K3/386 , B32B15/08 , C08G73/00 , C08G73/06 , H05K1/0393 , H05K2201/0154 , H05K2201/0355 , Y10T428/2852 , Y10T428/2861 , Y10T428/2896 , Y10T428/31551 , Y10T428/31605
摘要： Described is an adhesive containing a polycarbodiimide resin having repeating units represented by the following formula:.paren open-st.R--N.dbd.C.dbd.N.paren close-st..sub.nwherein R is a divalent hydrocarbon group and n is an integer of 5 to 250, and also described is a flexible printed circuit board and a coverlay film fabricated using the above-described polycarbodiimide resin-containing adhesive.
摘要翻译：描述了含有具有由下式表示的重复单元的聚碳化二亚胺树脂的粘合剂：+545RN = C = N + 546 n其中R是二价烃基，n是5至250的整数，并且还描述了柔性印刷电路板和使用上述含聚碳酰亚胺树脂的粘合剂制成的覆盖膜。

7. 发明授权

US5821325A Polycarbodiimide derivatives and method for preparing the same 失效
标题翻译：聚碳二亚胺衍生物及其制备方法
公开(公告)号：US5821325A
公开(公告)日：1998-10-13
申请号：US763982
申请日：1996-12-10
申请人： Ken Yahata , Yasuyuki Takiguchi , Hiroshi Miyoshi , Yasuyoshi Komoto , Akira Hayashida
发明人： Ken Yahata , Yasuyuki Takiguchi , Hiroshi Miyoshi , Yasuyoshi Komoto , Akira Hayashida
IPC分类号： C08G18/02 , C08G73/10 , C08G63/06 , C08G75/04
CPC分类号： C08G18/025
摘要： A hydroxy- or mercapto-bearing organic compound is caused to react with a polycarbodiimide compound in the presence of an alcoholate of an alkali metal or of an alkaline earth metal. The carbodiimide linkage in the polymer which results from the above-described reaction is crosslinked.
摘要翻译：使含羟基或巯基的有机化合物在碱金属或碱土金属的醇化物的存在下与聚碳化二亚胺化合物反应。由上述反应得到的聚合物中的碳二亚胺键被交联。

8. 发明授权

US5750637A Process for the preparation of a polycarbodiimide solution 失效
标题翻译：制备聚碳二亚胺溶液的方法
公开(公告)号：US5750637A
公开(公告)日：1998-05-12
申请号：US658166
申请日：1996-06-04
申请人： Yasuyuki Takiguchi , Ken Yahata , Yasuyoshi Komoto , Akira Hayashida , Minoru Takamizawa
发明人： Yasuyuki Takiguchi , Ken Yahata , Yasuyoshi Komoto , Akira Hayashida , Minoru Takamizawa
IPC分类号： C08G18/00 , C08G18/02 , C08G73/00 , C08G73/10
CPC分类号： C08G73/00 , C08G18/025
摘要： This invention provides a process for the preparation of a polycarbodiimide solution wherein the polycarbodiimide is synthesized by heating an organic diisocyanate (e.g., 2,4-tolylene diisocyanate or 2,6-tolylene diisocyanate) in the presence of a carbodiimidation catlayst characterized in that a non-chlorinated aromatic hydrocarbon is used as the solvent and the resulting polycarbodiimide has a number average molecular weight from about 3,000 to about 10,000; wherein the synthesis is performed in the temperature range of from about 100.degree. to about 120.degree. C.
摘要翻译：本发明提供一种制备聚碳二亚胺溶液的方法，其中聚碳二亚胺通过在碳二亚胺二酰亚胺存在下加热有机二异氰酸酯（例如，2,4-甲苯二异氰酸酯或2,6-甲苯二异氰酸酯）来合成，其特征在于，使用非氯化芳烃作为溶剂，所得聚碳二亚胺的数均分子量为约3,000至约10,000; 其中合成在约100℃至约120℃的温度范围内进行。

9. 发明授权

US5837801A Method for preparing crosslinked polycarbodiimides 失效
标题翻译：交联聚碳化二亚胺的制备方法
公开(公告)号：US5837801A
公开(公告)日：1998-11-17
申请号：US759381
申请日：1996-12-04
申请人： Ken Yahata , Hiroshi Miyoshi , Yasuyuki Takiguchi , Yasuyoshi Komoto , Akira Hayashida
发明人： Ken Yahata , Hiroshi Miyoshi , Yasuyuki Takiguchi , Yasuyoshi Komoto , Akira Hayashida
IPC分类号： C04B35/524 , C08G18/02 , C08G73/10 , C08G95/04
CPC分类号： C08G18/025 , C04B35/524
摘要： The method for preparing a crosslinked polycarbodiimide according to the present invention comprises reacting a polydicarbodiimide compound with a compound, which has in a molecule thereof two or more hydroxy or mercapto groups, in the presence of an alcoholate of an alkali metal or of an alkaline earth metal. The crosslinked polycarbodiimide obtained according to the method is excellent in heat resistance and mechanical properties.
摘要翻译：根据本发明的制备交联聚碳化二亚胺的方法包括在碱金属或碱土金属的醇盐存在下使聚二碳酰亚胺化合物与分子中具有两个或多个羟基或巯基的化合物金属。根据该方法得到的交联聚碳化二亚胺具有优异的耐热性和机械性能。

10. 发明授权

US5750636A Process for the preparation of a high-molecular-weight polycarbodiimide solution 失效
标题翻译：制备高分子量聚碳二亚胺溶液的方法
公开(公告)号：US5750636A
公开(公告)日：1998-05-12
申请号：US658165
申请日：1996-06-04
申请人： Yasuyoshi Komoto , Yasuyuki Takiguchi , Ken Yahata , Akira Hayashida , Minoru Takamizawa
发明人： Yasuyoshi Komoto , Yasuyuki Takiguchi , Ken Yahata , Akira Hayashida , Minoru Takamizawa
IPC分类号： C08G18/00 , C08G18/02 , C08G73/00 , C08G73/10
CPC分类号： C08G73/00 , C08G18/025
摘要： This invention provides a process wherein a stable solution of polycarbodiimide with a number-average molecular-weight of 5,000 to 60,000 can be very easily prepared by using an organic diisocyanate (e.g., 2,4-tolylene diisocyanate or 2,6-tolylene diisocyanate) as starting material, a cyclic phosphine oxide as catalyst and a chlorinated aromatic compound as solvent and by controlling certain reaction conditions within the reaction temperature range of 110.degree. to 150.degree. C.
摘要翻译：本发明提供一种方法，其中通过使用有机二异氰酸酯（例如，2,4-甲苯二异氰酸酯或2,6-甲苯二异氰酸酯）可以非常容易地制备数均分子量为5,000至60,000的聚碳化二亚胺的稳定溶液，作为起始原料，作为催化剂的环状氧化膦和氯化芳族化合物作为溶剂，并通过在110℃至150℃的反应温度范围内控制某些反应条件。

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