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1. 发明专利

CA1247115A METHOD OF PRODUCING PHENOL-TYPE NATURAL ANTIOXIDATIVE MATERIALS 未知
公开(公告)号：CA1247115A
公开(公告)日：1988-12-20
申请号：CA504821
申请日：1986-03-24
申请人： TAKEMOTO OIL & FAT CO LTD
发明人： NAMIKI MITSUO , OSAWA TOSHIHIKO , FUKUDA YASUKO , OZAKI TATSUHIKO
IPC分类号： C07D493/04 , C09K15/08 , C09K15/34
摘要： Phenol-type natural antioxidative materials containing analogs of sesamin or sesamolin are manufactured by processing a processed sesame seed product with an acid catalyst and subsequently condensing and separating the desired materials by a physical means such as extraction, distillation and adsorption.

2. 发明专利

DE3664046D1 METHOD OF MANUFACTURING PHENOL-TYPE NATURAL ANTIOXIDANTS 未知
公开(公告)号：DE3664046D1
公开(公告)日：1989-07-27
申请号：DE3664046
申请日：1986-06-26
申请人： TAKEMOTO OIL & FAT CO LTD
发明人： NAMIKI MITSUO , OSAWA TOSHIHIKO , FUKUDA YASUKO , OZAKI TATSUHIKO
IPC分类号： C07D493/04 , C09K15/08 , C09K15/34 , C09K15/06

3. 发明专利

DE3764838D1 未知
公开(公告)号：DE3764838D1
公开(公告)日：1990-10-18
申请号：DE3764838
申请日：1987-02-18
申请人： TAKEMOTO OIL & FAT CO LTD
发明人： NAMIKI MITSUO , OSAWA TOSHIHIKO , ISOBE MINORU , FUKUDA YASUKO
IPC分类号： A23L3/3544 , C07D493/04 , C09K15/08 , C09K15/34 , C09K15/06
摘要： An active antioxidant containing a compound of structural formula is produced by applying an acid catalyst to sesamolin in the substantial absence of active hydrogen compounds.

4. 发明专利

CA1263962A METHOD OF PRODUCING ACTIVE ANTIOXYDANT 未知
公开(公告)号：CA1263962A
公开(公告)日：1989-12-19
申请号：CA533307
申请日：1987-03-30
申请人： TAKEMOTO OIL & FAT CO LTD
发明人： NAMIKI MITSUO , OSAWA TOSHIHIKO , ISOBE MINORU , FUKUDA YASUKO
IPC分类号： A23L3/3544 , C07D493/04 , C09K15/08 , C09K15/34
摘要： An active antioxydant containing a compound shown by structural formula is produced by applying an acid catalyst to sesamolin substantially in the absence of active hydrogen compounds.

5. 发明专利

JPS6244793B2 失效
公开(公告)号：JPS6244793B2
公开(公告)日：1987-09-22
申请号：JP3163283
申请日：1983-02-25
申请人： TAKEMOTO OIL & FAT CO LTD
发明人： NAMIKI MITSUO , OOSAWA TOSHIHIKO , FUKUDA YASUKO , OZAKI TATSUHIKO
IPC分类号： C09K15/34 , A23L3/34 , A23L3/3472 , C11B5/00

6. 发明专利

JPS62230786A PRODUCTION OF SUBSTANCE HAVING ANTIOXIDATION ACTIVITY 失效
公开(公告)号：JPS62230786A
公开(公告)日：1987-10-09
申请号：JP7536186
申请日：1986-03-31
申请人： TAKEMOTO OIL & FAT CO LTD
发明人： NAMIKI MITSUO , OSAWA TOSHIHIKO , ISOBE MINORU , FUKUDA YASUKO
IPC分类号： A23L3/3544 , C07D493/04 , C09K15/08 , C09K15/34
摘要： PURPOSE:To economically produce the titled compound on an industrial scale from sesamolin which hitherto has been discarded, by reacting sesamolin with an acid catalyst under a condition free from participation of active hydrogen compound. CONSTITUTION:The objective compound of formula can be produced by reacting sesamolin with an acid catalyst (preferably acid clay, active clay, zeolite, silica- titanium oxide, cation exchange resin or organic or inorganic Brphinstedt acid) under a condition essentially (e.g. water, alcohol, phenol, etc.). The reaction temperature of the catalyst is preferably 70-200 deg.C.

7. 发明专利

JPS63436B2 失效
公开(公告)号：JPS63436B2
公开(公告)日：1988-01-07
申请号：JP3163383
申请日：1983-02-25
申请人： TAKEMOTO OIL & FAT CO LTD
发明人： NAMIKI MITSUO , OOSAWA TOSHIHIKO , FUKUDA YASUKO , OZAKI TATSUHIKO
IPC分类号： C09K15/08 , C07D493/04 , C12P17/18 , C12R1/07

8. 发明专利

JPS59157173A Antioxidant 失效
标题翻译：抗氧化
公开(公告)号：JPS59157173A
公开(公告)日：1984-09-06
申请号：JP3163283
申请日：1983-02-25
申请人： Takemoto Oil & Fat Co Ltd
发明人： NAMIKI MITSUO , OOSAWA TOSHIHIKO , FUKUDA YASUKO , OZAKI TATSUHIKO
IPC分类号： C09K15/34 , A23L3/34 , A23L3/3472 , C11B5/00
摘要： PURPOSE: To provide an antioxidant capable of effectively suppressing the degradation of a food by oxidation, by treating crushed sesame seeds with β- glucosidase, and using the product as an active component of the antioxidant.
CONSTITUTION: Crushed sesame seeds (e.g. defatted sesame seeds after oil expression) or extract of sesame seeds with a solvent (preferably extracted with a hydrated alcohol composed of a mixture of a 1W4C alcohol and water at a weight ratio of 10:90W90:10) are treated with β-glucosidase preferably at 30W 60°C and 3W7pH. The reaction product is extracted with a hardly water-soluble solvent such as ethyl acetate to obtain the objective antioxidant.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：提供能够通过氧化来有效抑制食物降解的抗氧化剂，通过用β-葡糖苷酶处理破碎的芝麻籽，并使用该产物作为抗氧化剂的活性成分。构成：粉碎的芝麻（例如油表达后的脱脂芝麻）或芝麻籽用溶剂提取物（优选用由1-4C醇和水的混合物组成的水合醇以10：90〜 90:10）用β-葡萄糖苷酶优选在30-60℃和3-7pH处理。反应产物用难溶于水的溶剂如乙酸乙酯萃取，得到客观的抗氧化剂。

9. 发明专利

JPS59157086A Tetrahydro-1-(3-methoxy-4-hydroxyphenoxy)-4-(3,4- (methylenedioxy)phenyl)-1h,3h-furo(3,4-c)furan and antioxidant containing the same 失效
标题翻译：四氢-1-（3-甲氧基-4-羟基苯氧基）-4-（3,4-（甲基二氧基）苯基）-1H，3H-呋喃（3,4-C）FURAN和含有它的抗氧化剂
公开(公告)号：JPS59157086A
公开(公告)日：1984-09-06
申请号：JP3163383
申请日：1983-02-25
申请人： Takemoto Oil & Fat Co Ltd
发明人： NAMIKI MITSUO , OOSAWA TOSHIHIKO , FUKUDA YASUKO , OZAKI TATSUHIKO
IPC分类号： C09K15/08 , C07D493/04 , C12P17/18 , C12R1/07
摘要： NEW MATERIAL:Tetrahydro-1-[ 3-methoxy-4-hydroxyphenoxy ] -4- [ 3,4-(methylenedioxy)phenyl]-1H,3H-furo[3,4-c]furane.
USE: Antioxidant: it has high safety.
PREPARATION: β-Glucosidase or a microorganism such as Bacillus Natto or Rhizopus oligosporus is made to act on sesami seeds, defatted sesami seeds or their extract to give the compound of formula I . When the substrate is treated with the enzyme, the extract is dissolved or suspended in water, sterilized by cell filtration or with humid heat and kept at such a temperature and a pH as β-glucosidase can easily develop its action (usually pH 3W7 and 30W65°C). On treatment with the microorganism, the extract is combined with water, sterilized, when necessary, adjusted in pH to 4W7, then the microorganism is inoculated and cultured.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：四氢-1- [3-甲氧基-4-羟基苯氧基] -4- [3,4-（亚甲二氧基）苯基] -1H-，3H-呋喃并[3,4-c]呋喃。用途：抗氧化：安全性高。制备：制备β-葡萄糖苷酶或微生物如纳豆或芽孢杆菌以作用于芝麻种子，脱脂芝麻种子或其提取物，得到式I化合物。当用酶处理底物时，将提取物溶解或悬浮在水中，通过细胞过滤或潮湿加热灭菌，并保持在这样的温度，并且如β-葡糖苷酶的pH可以容易地发挥其作用（通常为pH 3-7 和30-65℃）。在用微生物处理时，将提取物与水合并，灭菌，必要时将pH调节至4-7，然后将微生物接种培养。

10. 发明专利

JPH0546351B2 失效
公开(公告)号：JPH0546351B2
公开(公告)日：1993-07-13
申请号：JP7536186
申请日：1986-03-31
申请人： TAKEMOTO OIL & FAT CO LTD
发明人： NAMIKI MITSUO , OOSAWA TOSHIHIKO , ISOBE MINORU , FUKUDA YASUKO
IPC分类号： A23L3/3544 , C07D493/04 , C09K15/08 , C09K15/34

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