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1. 发明申请

US20110031935A1 NEGATIVE ELECTRODE FOR LITHIUM-ION SECONDARY BATTERY AND MANUFACTURING PROCESS FOR THE SAME 审中-公开
标题翻译：用于锂离子二次电池的负极及其制造方法
公开(公告)号：US20110031935A1
公开(公告)日：2011-02-10
申请号：US12988491
申请日：2009-03-17
申请人： Manabu Miyoshi , Hitotoshi Murase , Akira Kojima , Junichi Niwa , Takayuki Hirose , Kazuhiro Izumoto , Hideki Goda
发明人： Manabu Miyoshi , Hitotoshi Murase , Akira Kojima , Junichi Niwa , Takayuki Hirose , Kazuhiro Izumoto , Hideki Goda
IPC分类号： H01M10/44 , H01M4/58 , H01M2/14 , H01M4/62
CPC分类号： H01M4/622 , H01M4/134 , H01M4/136 , H01M4/1395 , H01M4/38 , H01M4/386 , H01M4/387 , H01M4/5825 , H01M4/621 , H01M4/661 , H01M4/74 , H01M10/052 , H01M10/44
摘要： The present invention is characterized in that, in a negative electrode for lithium-ion secondary battery, the negative electrode being manufactured via an application step of applying a binder resin and an active material onto a surface of collector, the binder resin is an alkoxysilyl group-containing resin that has a structure being specified by formula (I); and the active material includes a lithium-inactive metal that does not form any intermetallic compounds with lithium, or a silicide of the lithium-inactive metal, and an elemental substance of Si. It is possible to upgrade cyclic characteristics by means of using the negative electrode for lithium-ion secondary battery according to the present invention. wherein “R1” is an alkyl group whose number of carbon atoms is from 1 to 8; “R2” is an alkyl group or alkoxyl group whose number of carbon atoms is from 1 to 8; and “q” is an integer of from 1 to 100.
摘要翻译：本发明的特征在于，在锂离子二次电池用负极中，通过将粘合剂树脂和活性物质涂布在集电体的表面上的施加步骤制造负极，粘合剂树脂为烷氧基甲硅烷基（I）所示结构的树脂; 并且活性材料包括不与锂形成任何金属间化合物的锂惰性金属，或锂惰性金属的硅化物和Si的元素物质。通过使用本发明的锂离子二次电池用负极，能够提高循环特性。其中“R1”是碳原子数为1〜8的烷基; “R2”是碳原子数为1〜8的烷基或烷氧基; “q”为1〜100的整数。

2. 发明申请

US20120202117A1 NEGATIVE ELECTRODE FOR NON-AQUEOUS-SYSTEM SECONDARY BATTERY AND MANUFACTURING PROCESS FOR THE SAME 审中-公开
标题翻译：用于非水系统二次电池的负极和其制造方法
公开(公告)号：US20120202117A1
公开(公告)日：2012-08-09
申请号：US13501977
申请日：2010-10-06
申请人： Takayuki Hirose , Manabu Miyoshi , Hitotoshi Murase , Hideki Goda , Kazuhiro Izumoto
发明人： Takayuki Hirose , Manabu Miyoshi , Hitotoshi Murase , Hideki Goda , Kazuhiro Izumoto
IPC分类号： H01M4/64 , B05D5/12
CPC分类号： H01M4/621 , H01M4/134 , H01M4/386 , H01M4/622
摘要： It is equipped with a negative-electrode current collector, and a negative-electrode mixture-material layer comprising a negative-electrode mixture material that includes a negative-electrode active material containing silicon (Si) and a binding agent at least, the negative-electrode mixture-material layer being formed on a surface of the negative-electrode current collector; and the binding agent includes a polyimide-silica hybrid resin being made by subjecting a silane-modified polyamic acid to sol-gel curing and dehydration ring-closing, the silane-modified polyamic acid being expressed by the following formula (wherein: “R1” specifies an aromatic tetracarboxylic dianhydride residue including 3,3′,4,4′-biphenyltetracarboxylic dianhydride residue in an amount of 90% by mole or more; “R2” specifies an aromatic diamine residue including a 4,4′-diaminodiphenyl ether residue in an amount of 90% by mole or more; “R3” specifies an alkyl group whose number of carbon atoms is from 1 to 8; “R4” specifies an alkyl group or an alkoxy group whose number of carbon atoms is from 1 to 8 independently of one another; “q” is from 1 to 5,000; “r” is from 1 to 1,000; and “m” is from 1 to 100).
摘要翻译：具备负极集电体和负极混合材料层，负极混合材料层至少含有含有硅（Si）和结合剂的负极活性物质的负极混合材料，电极复合材料层形成在负极集电体的表面上; 粘合剂包括通过使硅烷改性聚酰胺酸进行溶胶 - 凝胶固化和脱水闭环而制成的聚酰亚胺 - 二氧化硅杂化树脂，所述硅烷改性聚酰胺酸由下式表示（其中：“R1” 指定含有90摩尔％以上的3,3'，4,4'-联苯四羧酸二酐残基的芳香族四羧酸二酐残基;“R2”表示包含4,4'-二氨基二苯醚残基的芳香族二胺残基 90摩尔％以上，“R3”表示碳原子数1〜8的烷基，“R4”表示碳原子数为1〜8的烷基或烷氧基， “q”为1〜5,000;“r”为1〜1000，“m”为1〜100）。

3. 发明申请

US20140106226A1 LITHIUM ION SECONDARY CELL 有权
标题翻译：锂离子二次电池
公开(公告)号：US20140106226A1
公开(公告)日：2014-04-17
申请号：US14122973
申请日：2012-05-10
申请人： Keiichi Hayashi , Manabu Miyoshi , Takayuki Hirose , Hitotoshi Murase , Hideyuki Morimoto , Shin-ichi Tobishima
发明人： Keiichi Hayashi , Manabu Miyoshi , Takayuki Hirose , Hitotoshi Murase , Hideyuki Morimoto , Shin-ichi Tobishima
IPC分类号： H01M4/36
CPC分类号： H01M4/364 , B82Y30/00 , C01G49/06 , C01P2002/50 , C01P2002/72 , C01P2004/03 , C01P2004/16 , C01P2004/54 , C01P2004/62 , C01P2006/12 , C01P2006/14 , H01M4/485 , H01M4/525 , H01M10/0525 , H01M2004/021
摘要： Provided is a negative-electrode active material, which is capable of constituting a lithium ion secondary cell exhibiting excellent cell characteristics.The negative-electrode active material for a lithium ion secondary cell of the invention includes a mixed material of silicon oxide particles composed of silicon oxide and rod-shaped iron oxide particles composed of iron oxide. It is preferable to use iron oxide particles having a plurality of pores in a surface, and an electrode reaction is effectively carried out.
摘要翻译：提供一种负极活性物质，其能够构成表现出优异的电池特性的锂离子二次电池。本发明的锂离子二次电池用负极活性物质包括由氧化硅构成的氧化硅粒子和由氧化铁构成的棒状氧化铁粒子的混合物。优选在表面使用具有多个孔的氧化铁颗粒，并且有效地进行电极反应。

4. 发明授权

US09735422B2 Lithium ion secondary cell 有权
公开(公告)号：US09735422B2
公开(公告)日：2017-08-15
申请号：US14122973
申请日：2012-05-10
申请人： Keiichi Hayashi , Manabu Miyoshi , Takayuki Hirose , Hitotoshi Murase , Hideyuki Morimoto , Shin-ichi Tobishima
发明人： Keiichi Hayashi , Manabu Miyoshi , Takayuki Hirose , Hitotoshi Murase , Hideyuki Morimoto , Shin-ichi Tobishima
IPC分类号： H01M4/36 , C01G49/06 , H01M4/485 , H01M4/525 , B82Y30/00 , H01M10/0525 , H01M4/02
CPC分类号： H01M4/364 , B82Y30/00 , C01G49/06 , C01P2002/50 , C01P2002/72 , C01P2004/03 , C01P2004/16 , C01P2004/54 , C01P2004/62 , C01P2006/12 , C01P2006/14 , H01M4/485 , H01M4/525 , H01M10/0525 , H01M2004/021
摘要： Provided is a negative-electrode active material, which is capable of constituting a lithium ion secondary cell exhibiting excellent cell characteristics.The negative-electrode active material for a lithium ion secondary cell of the invention includes a mixed material of silicon oxide particles composed of silicon oxide and rod-shaped iron oxide particles composed of iron oxide. It is preferable to use iron oxide particles having a plurality of pores in a surface, and an electrode reaction is effectively carried out.

5. 发明申请

US20120244435A1 NEGATIVE ELECTRODE FOR LITHIUM-ION SECONDARY BATTERY 审中-公开
标题翻译：用于锂离子二次电池的负极
公开(公告)号：US20120244435A1
公开(公告)日：2012-09-27
申请号：US13514856
申请日：2010-12-09
申请人： Takayuki Hirose , Manabu Miyoshi , Hitotoshi Murase
发明人： Takayuki Hirose , Manabu Miyoshi , Hitotoshi Murase
IPC分类号： H01M4/62 , H01M4/64 , H01M4/38 , H01M4/13
CPC分类号： H01M4/134 , H01M4/1395 , H01M4/366 , H01M4/62 , H01M4/622 , H01M10/0525
摘要： To provide a negative electrode for lithium-ion secondary battery, negative electrode which has good cyclability by suppressing the active material from coming off or falling down from the current collector.It has a current collector 1; and an active-material layer 6 in which a conductive additive 3; and an active material 2 being surface-treated with use of a surface treatment agent that is specified by a general formula: X—Si(CH3)n—(OR)3-n wherein: “n” is 0, 1 or 2; “OR” is a methoxy group, or an ethoxy group; and “X” is a methoxy group, an ethoxy group, or a vinyl group; are bound onto a surface of the current collector 1 via a binder 4 comprising a resin that has an alkoxy group-containing silane-modified part.
摘要翻译：为了提供一种锂离子二次电池用负极，通过抑制活性物质从集电体脱落或落下而具有良好的循环性的负极。它有一个集电器1; 和其中导电添加剂3的活性材料层6; 和使用由通式X-Si（CH3）n-（OR）3-n表示的表面处理剂进行表面处理的活性物质2，其中：“n”为0,1或2; “OR”是甲氧基或乙氧基; “X”为甲氧基，乙氧基或乙烯基; 经由包含含有含烷氧基的硅烷改性部分的树脂的粘合剂4结合到集电体1的表面上。

6. 发明授权

US09184439B2 Negative-electrode active material for non-aqueous-system secondary battery and production process for the same 有权
标题翻译：用于非水系二次电池的负电极活性材料及其制备方法
公开(公告)号：US09184439B2
公开(公告)日：2015-11-10
申请号：US13516974
申请日：2010-12-08
申请人： Manabu Miyoshi , Hideaki Ishikawa , Hitotoshi Murase
发明人： Manabu Miyoshi , Hideaki Ishikawa , Hitotoshi Murase
IPC分类号： H01M4/58 , H01M4/36 , C01B33/24 , H01M4/38 , H01M4/485 , H01M4/62 , H01M10/052
CPC分类号： H01M4/364 , C01B33/24 , H01M4/386 , H01M4/485 , H01M4/62 , H01M10/052
摘要： Providing a noble negative-electrode active material including silicon, and a production process for the same.A negative-electrode active material for non-aqueous-system secondary battery including a silicon phase and a composite oxide phase (a CaSiO3 phase, for instance) is obtained by mixing a silicon oxide (SiO, for instance) with a silicon compound (CaSi2, for instance), which includes silicon and at least one member of elements being selected from the group consisting of Group 2 (or Group 2A) elements in the Periodic Table, to prepare a mixed raw material, and then reacting the mixed raw material. The composite oxide phase demonstrates the advantage of inhibiting electrolytic solutions from decomposing in a smaller amount than does the conventional SiO2 phase.
摘要翻译：提供含有硅的贵负极活性物质及其制造方法。通过将氧化硅（例如SiO）与硅化合物（CaSi 2）相混合，得到含有硅相和复合氧化物相（例如CaSiO 3相）的非水系二次电池用负极活性物质例如），其包括硅和选自元素周期表中的组2（或组2A）元素的元素中的至少一个元素，以制备混合原料，然后使混合原料反应。复合氧化物相显示了抑制电解液比常规SiO 2相分解更少的优点。

7. 发明申请

US20140186704A1 LITHIUM ION SECONDARY BATTERY ELECTRODE, MANUFACTURING PROCESS FOR THE SAME, AND LITHIUM ION SECONDARY BATTERY USING THE ELECTRODE 有权
标题翻译：锂离子二次电池电极，其制造方法和使用电极的锂离子二次电池
公开(公告)号：US20140186704A1
公开(公告)日：2014-07-03
申请号：US14119239
申请日：2012-05-02
申请人： Junichi Niwa , Yuichi Hirakawa , Manabu Miyoshi , Keiichi Hayashi , Hitotoshi Murase
发明人： Junichi Niwa , Yuichi Hirakawa , Manabu Miyoshi , Keiichi Hayashi , Hitotoshi Murase
IPC分类号： H01M4/62 , H01M4/04 , H01M4/139
CPC分类号： H01M4/139 , H01M4/0404 , H01M4/0471 , H01M4/13 , H01M4/131 , H01M4/136 , H01M4/1391 , H01M4/1397 , H01M4/366 , H01M4/38 , H01M4/485 , H01M4/505 , H01M4/62 , H01M4/622 , H01M10/0525 , Y02E60/122 , Y02P70/54
摘要： To provide a lithium ion secondary battery electrode in which a coated layer is held on a surface of an active material layer over a long period of time to suppress decomposition of the electrolysis solution and to enhance the cyclability, a manufacturing process for the same, and a lithium ion secondary battery using the electrode.A lithium ion secondary battery electrode includes a current collector, an active material layer containing a binder formed on a surface of the current collector, and a coated layer formed on the surface of at least a part of the active material layer, wherein the coated layer consists of an acrylic type copolymer cured substance comprising an acrylic type main chain and a side chain having polyester or polyether graft-polymerized to said acrylic type main chain and the coated layer is chemically bonded with the binder.
摘要翻译：为了提供一种锂离子二次电池电极，其中将涂层长时间地保持在活性物质层的表面上，以抑制电解液的分解并提高其循环性，其制造方法和使用该电极的锂离子二次电池。锂离子二次电池电极包括集电体，含有形成在集电体的表面上的粘合剂的活性物质层和形成在活性物质层的至少一部分的表面上的被覆层，其中，涂布层由丙烯酸型主链和丙烯酸类主链接枝聚合的聚酯或聚醚的侧链构成的丙烯酸类共聚物固化物，涂层与粘合剂化学键合。

8. 发明授权

US08822083B2 Negative electrode for lithium-ion secondary battery and manufacturing process for the same 有权
标题翻译：锂离子二次电池用负极及其制造工艺
公开(公告)号：US08822083B2
公开(公告)日：2014-09-02
申请号：US13497717
申请日：2010-09-01
申请人： Manabu Miyoshi , Hitotoshi Murase , Keiichi Hayashi , Shinji Suzuki
发明人： Manabu Miyoshi , Hitotoshi Murase , Keiichi Hayashi , Shinji Suzuki
IPC分类号： H01M2/16 , H01M4/02 , B05D5/12 , H01M4/88
CPC分类号： H01M4/1395 , H01G11/28 , H01M4/134 , H01M4/62 , H01M4/621 , H01M10/052 , H01M10/4235
摘要： A negative electrode for a lithium-ion secondary battery, has a current collector and an active-material layer bound on a surface of the current collector. The active-material layer includes active materials, binders, conductive additives, and buffer materials. The active materials include Si and/or Sn, and the buffer materials comprise a silicone composite powder in which a spherical silicone-rubber powder is covered with a silicone resin.
摘要翻译：锂离子二次电池用负极具有在集电体的表面上结合的集电体和活性物质层。活性材料层包括活性材料，粘合剂，导电添加剂和缓冲材料。活性材料包括Si和/或Sn，缓冲材料包括硅氧烷复合粉末，其中球形硅橡胶粉末被硅树脂覆盖。

9. 发明申请

US20140099542A1 LITHIUM ION SECONDARY BATTERY ELECTRODE, MANUFACTURING PROCESS FOR THE SAME, AND LITHIUM ION SECONDARY BATTERY USING THE ELECTRODE 有权
标题翻译：锂离子二次电池电极，其制造方法和使用电极的锂离子二次电池
公开(公告)号：US20140099542A1
公开(公告)日：2014-04-10
申请号：US14119235
申请日：2012-05-02
申请人： Junichi Niwa , Yuichi Hirakawa , Manabu Miyoshi , Keiichi Hayashi , Hitotoshi Murase
发明人： Junichi Niwa , Yuichi Hirakawa , Manabu Miyoshi , Keiichi Hayashi , Hitotoshi Murase
IPC分类号： H01M4/62 , H01M4/04
CPC分类号： H01M4/628 , H01M4/0404 , H01M4/13 , H01M4/139 , H01M4/622 , H01M10/4235 , Y02E60/122 , Y02P70/54
摘要： To provide a lithium ion secondary battery electrode in which a coated layer is held on a surface of an active material layer over a long period of time to suppress decomposition of the electrolysis solution and to enhance the cyclability, a manufacturing process for the same, and a lithium ion secondary battery using the electrode.A lithium ion secondary battery electrode includes a current collector, an active material layer containing a binder formed on a surface of the current collector, and a coated layer formed on the surface of at least a part of the active material layer, wherein the coated layer contains a silicone-acrylic graft copolymer cured substance including an acrylic type main chain having a functional group and a side chain having a silicone graft-polymerized to the acrylic type main chain, and the coated layer is chemically bonded with the binder.
摘要翻译：为了提供一种锂离子二次电池电极，其中将涂层长时间地保持在活性物质层的表面上，以抑制电解液的分解并提高其循环性，其制造方法和使用该电极的锂离子二次电池。锂离子二次电池电极包括集电体，含有形成在集电体的表面上的粘合剂的活性物质层和形成在活性物质层的至少一部分的表面上的涂层，其中，涂布层含有具有官能团的丙烯酸类主链和具有与丙烯酸类主链接枝聚合的硅氧烷的侧链的有机硅 - 丙烯酸接枝共聚物固化物，并且涂层与粘合剂化学键合。

10. 发明申请

US20120177992A1 NEGATIVE ELECTRODE FOR LITHIUM-ION SECONDARY BATTERY AND MANUFACTURING PROCESS FOR THE SAME 有权
标题翻译：用于锂离子二次电池的负极及其制造方法
公开(公告)号：US20120177992A1
公开(公告)日：2012-07-12
申请号：US13497717
申请日：2010-09-01
申请人： Manabu Miyoshi , Hitotoshi Murase , Keiichi Hayashi , Shinji Suzuki
发明人： Manabu Miyoshi , Hitotoshi Murase , Keiichi Hayashi , Shinji Suzuki
IPC分类号： H01M4/38 , H01M4/64 , H01M4/62 , H01M4/04
CPC分类号： H01M4/1395 , H01G11/28 , H01M4/134 , H01M4/62 , H01M4/621 , H01M10/052 , H01M10/4235
摘要： To provide a negative electrode for lithium-ion secondary battery, negative electrode which has good cyclability by suppressing the active material from coming off or falling down from the current collector, and a manufacturing process for the same.It is characterized in that, in a negative electrode for lithium-ion secondary battery, the negative electrode having a current collector 1 and an active-material layer 6 being bound on a surface of the current collector 1, the active-material layer 6 includes active materials 2, binders 5, conductive additives 4, and buffer materials 3, the active materials 2 include Si and/or Sn, and the buffer materials 3 comprise a silicone composite powder in which a spherical silicone-rubber powder is covered with a silicone resin.
摘要翻译：为了提供锂离子二次电池用负极，通过抑制活性物质从集电体脱落或脱落而具有良好的循环性的负极及其制造方法。其特征在于，在锂离子二次电池用负极中，具有集电体1和活性物质层6的负极结合在集电体1的表面上，活性物质层6包括活性材料2，粘合剂5，导电添加剂4和缓冲材料3，活性材料2包括Si和/或Sn，缓冲材料3包括硅氧烷复合粉末，其中球形硅橡胶粉末被硅氧烷覆盖树脂。

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