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1. 发明授权

US08840856B2 Method for producing imidic acid salt 有权
标题翻译：生产酰亚胺酸盐的方法
公开(公告)号：US08840856B2
公开(公告)日：2014-09-23
申请号：US13322782
申请日：2010-06-01
申请人： Takayoshi Morinaka , Tsutomu Nanmyo
发明人： Takayoshi Morinaka , Tsutomu Nanmyo
IPC分类号： C01B25/10 , C01B21/097 , C01B21/093 , C01B21/086 , B01J31/02
CPC分类号： C01B21/086 , B01J31/0245 , B01J31/0252 , C01B21/093 , C01B21/0975
摘要： To provide an imide salt represented by the formula wherein, R represents a halosulfonyl group (—SO2X1 where X1 is a halogen such as fluorine, chlorine, bromine and iodine) or dihalophosphoryl group (—POX2X3 where X2 and X3 are the same or different halogens such as fluorine, chlorine, bromine and iodine), and M represents an alkali metal; with high selectivity and high efficiency by using a low-cost starting material. In the production of an imide salt, an alkali metal fluoride, a sulfuryl halide or phosphoryl halide, and ammonia or an ammonium salt are reacted. According to this method, a desired imide salt can be produced with high yield, while greatly suppressing the production of a by-product.
摘要翻译：提供由下式表示的酰亚胺盐：其中，R表示卤代磺酰基（-SO2X1，其中X1是氟，氯，溴和碘等卤素）或二卤代磷酰基（-POX2X3，其中X2和X3是相同或不同的卤素例如氟，氯，溴和碘），M表示碱金属; 通过使用低成本起始材料，具有高选择性和高效率。在制备酰亚胺盐时，使碱金属氟化物，硫酰卤或磷酰卤，以及氨或铵盐反应。根据该方法，可以高产率地制造所需的酰亚胺盐，同时大大抑制副产物的生成。

2. 发明授权

US08815199B2 Method for producing imide compound 有权
标题翻译：生产酰亚胺化合物的方法
公开(公告)号：US08815199B2
公开(公告)日：2014-08-26
申请号：US13258988
申请日：2010-03-29
申请人： Takayoshi Morinaka , Tsutomu Nanmyo
发明人： Takayoshi Morinaka , Tsutomu Nanmyo
IPC分类号： C07C209/68 , C01B21/086 , C01B21/097
CPC分类号： C07F9/26 , B01J31/0252 , C01B21/086 , C01B21/093 , C01B21/0975
摘要： Disclosed is a method for producing “a salt or a complex comprising imide and an organic base”, characterized by reacting halogenated sulfuryl or halogenated phosphoryl with ammonia in the presence of an organic base. According to this method, a target imide compound can be produced in a high yield while significantly suppressing the production of by-products. Further, by reacting the obtained imide compound with an alkali metal hydroxide or an alkaline earth metal hydroxide, an imide metal salt can be easily derived.
摘要翻译：公开了一种生产“含有酰亚胺和有机碱的盐或络合物”的方法，其特征在于在有机碱的存在下使卤代磺酰基或卤代磷酰基与氨反应。根据该方法，可以高产率地制造目标酰亚胺化合物，同时显着抑制副产物的生成。此外，通过使所得酰亚胺化合物与碱金属氢氧化物或碱土金属氢氧化物反应，可以容易地得到酰亚胺金属盐。

3. 发明申请

US20120070358A1 Method for Producing Imidic Acid Salt 有权
标题翻译：产生酸性酸盐的方法
公开(公告)号：US20120070358A1
公开(公告)日：2012-03-22
申请号：US13322782
申请日：2010-06-01
申请人： Takayoshi Morinaka , Tsutomu Nanmyo
发明人： Takayoshi Morinaka , Tsutomu Nanmyo
IPC分类号： C01B21/097 , C01B21/086
CPC分类号： C01B21/086 , B01J31/0245 , B01J31/0252 , C01B21/093 , C01B21/0975
摘要： To provide an imide salt represented by the formula wherein, R represents a halosulfonyl group (—SO2X1 where X1 is a halogen such as fluorine, chlorine, bromine and iodine) or dihalophosphoryl group (—POX2X3 where X2 and X3 are the same or different halogens such as fluorine, chlorine, bromine and iodine), and M represents an alkali metal; with high selectivity and high efficiency by using a low-cost starting material. In the production of an imide salt, an alkali metal fluoride, a sulfuryl halide or phosphoryl halide, and ammonia or an ammonium salt are reacted. According to this method, a desired imide salt can be produced with high yield, while greatly suppressing the production of a by-product.
摘要翻译：提供由下式表示的酰亚胺盐：其中，R表示卤代磺酰基（-SO2X1，其中X1是氟，氯，溴和碘等卤素）或二卤代磷酰基（-POX2X3，其中X2和X3是相同或不同的卤素例如氟，氯，溴和碘），M表示碱金属; 通过使用低成本起始材料，具有高选择性和高效率。在制备酰亚胺盐时，使碱金属氟化物，硫酰卤或磷酰卤，以及氨或铵盐反应。根据该方法，可以高产率地制造所需的酰亚胺盐，同时大大抑制副产物的生成。

4. 发明申请

US20120020867A1 Method for Producing Imide Compound 有权
标题翻译：生产酰亚胺化合物的方法
公开(公告)号：US20120020867A1
公开(公告)日：2012-01-26
申请号：US13258988
申请日：2010-03-29
申请人： Takayoshi Morinaka , Tsutomu Nanmyo
发明人： Takayoshi Morinaka , Tsutomu Nanmyo
IPC分类号： C01B21/086 , C07C209/68 , C07D213/18
CPC分类号： C07F9/26 , B01J31/0252 , C01B21/086 , C01B21/093 , C01B21/0975
摘要： Disclosed is a method for producing “a salt or a complex comprising imide and an organic base”, characterized by reacting halogenated sulfuryl or halogenated phosphoryl with ammonia in the presence of an organic base. According to this method, a target imide compound can be produced in a high yield while significantly suppressing the production of by-products. Further, by reacting the obtained imide compound with an alkali metal hydroxide or an alkaline earth metal hydroxide, an imide metal salt can be easily derived.
摘要翻译：公开了一种生产“含有酰亚胺和有机碱的盐或络合物”的方法，其特征在于在有机碱存在下使卤代磺酰基或卤代磷酰基与氨反应。根据该方法，可以高产率地制造目标酰亚胺化合物，同时显着抑制副产物的生成。此外，通过使所得酰亚胺化合物与碱金属氢氧化物或碱土金属氢氧化物反应，可以容易地得到酰亚胺金属盐。

5. 发明申请

US20130023695A1 Preparation Method for Perfluoroalkane Sulfinate 有权
标题翻译：全氟烷基亚磺酸盐的制备方法
公开(公告)号：US20130023695A1
公开(公告)日：2013-01-24
申请号：US13574138
申请日：2011-03-03
申请人： Takashi Kashiwaba , Tsutomu Nanmyo , Yoichi Takenaka
发明人： Takashi Kashiwaba , Tsutomu Nanmyo , Yoichi Takenaka
IPC分类号： C07C313/04
CPC分类号： C07C313/04
摘要： In a method for obtaining an alkali metal perfluoroalkanesulfinate by reacting a perfluoroalkanesulfonyl halide with a sulfur-containing reducing agent in the presence of water, a reaction liquid containing the alkali metal sulfinate obtained after the reaction is concentrated till a specific concentration, thereby inorganic salts, which are impurities in the solution, are precipitated and removed, and a filtrate after removing the inorganic salts is subjected to an operation such as concentration and drying, thereby obtaining the target alkali metal perfluorosulfinate with a high purity and a good operability. Furthermore, an organic solvent for extraction becomes unnecessary. Therefore, it is possible to greatly reduce wastes.
摘要翻译：在通过使全氟烷基磺酰卤与含硫还原剂在水的存在下反应来获得全氟烷基亚磺酸碱金属的方法中，将反应后得到的含有碱金属亚磺酸盐的反应液浓缩至特定浓度，将溶液中的杂质析出除去，除去无机盐后的滤液进行浓缩干燥等操作，得到纯度高，操作性好的目标碱金属全氟亚磺酸酯。此外，不需要用于萃取的有机溶剂。因此，可以大大减少废物。

6. 发明申请

US20140171678A1 Fluoroalkanesulfonic Acid Production Method 有权
标题翻译：氟烷基磺酸生产方法
公开(公告)号：US20140171678A1
公开(公告)日：2014-06-19
申请号：US14232450
申请日：2012-08-02
申请人： Tatsuya Irie , Kenji Isoyama , Tatsuo Miyazaki , Takashi Kashiwaba , Tsutomu Nanmyo
发明人： Tatsuya Irie , Kenji Isoyama , Tatsuo Miyazaki , Takashi Kashiwaba , Tsutomu Nanmyo
IPC分类号： C07C303/02
CPC分类号： C07C303/02 , C07C303/22 , C07C303/44 , C07C309/06
摘要： Disclosed is a method for producing a fluoroalkanesulfonic acid including (1) the step of reacting concentrated sulfuric acid and/or fuming sulfuric acid with a fluoroalkanesulfonate to cause an acid decomposition, thereby obtaining a reaction mixture containing the fluoroalkanesulfonic acid and a sulfur component; and (2) the step of adding an oxidizing agent to the reaction mixture obtained by the above step and then conducting a distillation, thereby obtaining the fluoroalkanesulfonic acid from the reaction mixture. It is possible by this method to efficiently reduce the sulfur component, thereby industrially advantageously obtaining fluoroalkanesulfonic acid of high purity.
摘要翻译：公开了一种氟烷烃磺酸的制造方法，其包括（1）使浓硫酸和/或发烟硫酸与氟烷基磺酸反应引起酸分解的步骤，从而得到含有氟代链烷磺酸和硫成分的反应混合物; 和（2）向通过上述步骤获得的反应混合物中加入氧化剂然后进行蒸馏的步骤，由反应混合物得到氟代烷基磺酸。通过该方法可以有效地降低硫成分，从而在工业上有利地获得高纯度的氟烷烃磺酸。

7. 发明申请

US20100022803A1 Method for Producing Tris(Perfluoroalkanesulfonyl)Methide Acid Salt 有权
标题翻译：生产三（全氟烷基磺酰基）甲酸盐的方法
公开(公告)号：US20100022803A1
公开(公告)日：2010-01-28
申请号：US12520178
申请日：2007-12-18
申请人： Tsutomu Nanmyo , Shintaro Sasaki , Takashi Kume
发明人： Tsutomu Nanmyo , Shintaro Sasaki , Takashi Kume
IPC分类号： C07C315/00
CPC分类号： C07C315/00 , C07C315/04 , C07F3/02 , C07C317/04
摘要： There is provided a method for producing a tris(perfluoroalkanesulfonyl)methide acid salt represented by formula [1], including the steps of (a) reacting a methylmagnesium halide represented by formula [2] with a perfluoroalkanesulfonyl fluoride represented by formula [3], thereby obtaining a reaction mixture; and (b) directly reacting the obtained reaction mixture with at least one selected from the group consisting of alkali metal halides, quaternary ammonium salts, and quaternary phosphonium salts. By this method, it is possible to easily produce the target methide acid salt with high yield.
摘要翻译：提供了一种由式[1]表示的三（全氟烷基磺酰基）甲基化物酸盐的制备方法，其包括以下步骤：（a）使式[2]表示的甲基卤化镁与式[3]表示的全氟烷基磺酰氟反应，从而得到反应混合物; 和（b）使所得反应混合物与选自碱金属卤化物，季铵盐和季鏻盐中的至少一种直接反应。通过该方法，可以容易地以高产率制备目标甲基化酸盐。

8. 发明授权

US09073828B2 Preparation method for perfluoroalkane sulfinate 有权
标题翻译：全氟烷基亚磺酸盐的制备方法
公开(公告)号：US09073828B2
公开(公告)日：2015-07-07
申请号：US13574138
申请日：2011-03-03
申请人： Takashi Kashiwaba , Tsutomu Nanmyo , Yoichi Takenaka
发明人： Takashi Kashiwaba , Tsutomu Nanmyo , Yoichi Takenaka
IPC分类号： C07C313/04
CPC分类号： C07C313/04
摘要： In a method for obtaining an alkali metal perfluoroalkanesulfinate by reacting a perfluoroalkanesulfonyl halide with a sulfur-containing reducing agent in the presence of water, a reaction liquid containing the alkali metal sulfinate obtained after the reaction is concentrated till a specific concentration, thereby inorganic salts, which are impurities in the solution, are precipitated and removed, and a filtrate after removing the inorganic salts is subjected to an operation such as concentration and drying, thereby obtaining the target alkali metal perfluorosulfinate with a high purity and a good operability. Furthermore, an organic solvent for extraction becomes unnecessary. Therefore, it is possible to greatly reduce wastes.
摘要翻译：在通过使全氟烷基磺酰卤与含硫还原剂在水的存在下反应来获得全氟烷基亚磺酸碱金属的方法中，将反应后得到的含有碱金属亚磺酸盐的反应液浓缩至特定浓度，将溶液中的杂质析出除去，除去无机盐后的滤液进行浓缩干燥等操作，得到纯度高，操作性好的目标碱金属全氟亚磺酸酯。此外，不需要用于萃取的有机溶剂。因此，可以大大减少废物。

9. 发明授权

US08987507B2 Fluoroalkanesulfonic acid production method 有权
标题翻译：氟烷基磺酸生产方法
公开(公告)号：US08987507B2
公开(公告)日：2015-03-24
申请号：US14232450
申请日：2012-08-02
申请人： Tatsuya Irie , Kenji Isoyama , Tatsuo Miyazaki , Takashi Kashiwaba , Tsutomu Nanmyo
发明人： Tatsuya Irie , Kenji Isoyama , Tatsuo Miyazaki , Takashi Kashiwaba , Tsutomu Nanmyo
IPC分类号： C07C309/00 , C07C303/02 , C07C303/22 , C07C303/44
CPC分类号： C07C303/02 , C07C303/22 , C07C303/44 , C07C309/06
摘要： Disclosed is a method for producing a fluoroalkanesulfonic acid including (1) the step of reacting concentrated sulfuric acid and/or fuming sulfuric acid with a fluoroalkanesulfonate to cause an acid decomposition, thereby obtaining a reaction mixture containing the fluoroalkanesulfonic acid and a sulfur component; and (2) the step of adding an oxidizing agent to the reaction mixture obtained by the above step and then conducting a distillation, thereby obtaining the fluoroalkanesulfonic acid from the reaction mixture. It is possible by this method to efficiently reduce the sulfur component, thereby industrially advantageously obtaining fluoroalkanesulfonic acid of high purity.
摘要翻译：公开了一种氟烷烃磺酸的制造方法，其包括（1）使浓硫酸和/或发烟硫酸与氟烷基磺酸反应引起酸分解的步骤，从而得到含有氟代烷烃磺酸和硫成分的反应混合物; 和（2）向通过上述步骤获得的反应混合物中加入氧化剂然后进行蒸馏的步骤，由反应混合物得到氟代烷基磺酸。通过该方法可以有效地降低硫成分，从而在工业上有利地获得高纯度的氟烷烃磺酸。

10. 发明授权

US08304580B2 Method for producing tris(perfluoroalkanesulfonyl)methide acid salt 有权
标题翻译：三（全氟烷基磺酰基）甲基化物酸盐的制备方法
公开(公告)号：US08304580B2
公开(公告)日：2012-11-06
申请号：US12520178
申请日：2007-12-18
申请人： Tsutomu Nanmyo , Shintaro Sasaki , Takashi Kume
发明人： Tsutomu Nanmyo , Shintaro Sasaki , Takashi Kume
IPC分类号： C07C315/00
CPC分类号： C07C315/00 , C07C315/04 , C07F3/02 , C07C317/04
摘要： There is provided a method for producing a tris(perfluoroalkanesulfonyl)methide acid salt represented by formula [1], including the steps of (a) reacting a methylmagnesium halide represented by formula [2] with a perfluoroalkanesulfonyl fluoride represented by formula [3], thereby obtaining a reaction mixture; and (b) directly reacting the obtained reaction mixture with at least one selected from the group consisting of alkali metal halides, quaternary ammonium salts, and quaternary phosphonium salts. By this method, it is possible to easily produce the target methide acid salt with high yield.
摘要翻译：提供了一种由式[1]表示的三（全氟烷基磺酰基）甲基化物酸盐的制备方法，其包括以下步骤：（a）使式[2]表示的甲基卤化镁与式[3]表示的全氟烷基磺酰氟反应，从而得到反应混合物; 和（b）使所得反应混合物与选自碱金属卤化物，季铵盐和季鏻盐中的至少一种直接反应。通过该方法，可以容易地以高产率制备目标甲基化酸盐。

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