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1. 发明专利

CO7020925A2 Uso de un catalizador que comprende una zeolita modificada con fósforo en un procedimiento de deshidratación de un alcohol 未知
公开(公告)号：CO7020925A2
公开(公告)日：2014-08-11
申请号：CO14038375
申请日：2014-02-24
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOUVELLES
发明人： NESTERENKO NIKOLAI , MINOUX DELPHINE , ADAM CINDY , LOPEZ JOSEPH , EUZEN PATRICK
IPC分类号： B01J29/40

2. 发明专利

CA2842386A1 USE OF A CATALYST COMPRISING A PHOSPHORUS MODIFIED ZEOLITE IN AN ALCOHOL DEHYDRATION PROCESS 未知
公开(公告)号：CA2842386A1
公开(公告)日：2013-02-07
申请号：CA2842386
申请日：2012-07-25
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOUVELLES
发明人： NESTERENKO NIKOLAI , MINOUX DELPHINE , ADAM CINDY , DATH JEAN-PIERRE , LOPEZ JOSEPH , EUZEN PATRICK
IPC分类号： B01J29/40 , B01J29/85 , B01J37/10 , B01J37/28 , C07C1/20
摘要： The present invention relates, in a first embodiment, to the use of a catalyst to convert at least an alcohol into light olefins in a dehydration process to make an olefin having the same number of carbon atoms as the alcohol wherein said catalyst comprises a phosphorus modified zeolite and is made by a method comprising the following steps in this order, a) providing a zeolite comprising at least one ten members ring in the structure, optionally steaming said zeolite, b) mixing said zeolite of step a) with at least a component selected among one or more binders and shaping additives, then shaping said mixture, c) optionally making a ion-exchange, d) optionally steaming the shaped catalyst, optionally before step c), at least among said steaming of step d) and the steaming of step a) one is mandatory, e) introducing phosphorus on the catalyst to introduce at least 0.1 wt% of phosphorus, said introduction being made by dry impregnation or chemical vapor deposition, f) optionally introducing a metal, optionally simultaneously with step e), g) optionally washing the catalyst, h) optionally calcinating the catalyst, i) steaming the catalyst, also referred to as the equilibration step. In a second embodiment phosphorus can be introduced by any means and at step i) the steaming severity (X) is at least about 2. In said second embodiment the catalyst is advantageously steamed at a temperature above 625°C, preferably in the range 700 to 800°C. The metal of step f) is advantageously Calcium.

3. 发明专利

AR087461A1 USO DE UN CATALIZADOR QUE COMPRENDE UNA ZEOLITA MODIFICADA CON FOSFORO EN UN PROCESO DE DESHIDRATACION DE ALCOHOL 未知
公开(公告)号：AR087461A1
公开(公告)日：2014-03-26
申请号：ARP120102856
申请日：2012-08-03
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOUVELLES
发明人： NESTERENKO NIKOLAI , ADAM CINDY , EUZEN PATRICK , LOPEZ JOSEPH , MINOUX DELPHINE , DATH JEAN-PIERRE
IPC分类号： B01J29/40 , B01J29/85 , B01J37/10 , B01J37/28 , C07C1/20 , C07C1/24
摘要： La presente se refiere, en una primera realización, al uso de un catalizador para convertir al menos un alcohol en olefinas livianas en un proceso de deshidratación para producir una olefina que tiene el mismo número de átomos de carbono que el alcohol, en el que dicho catalizador comprende una zeolita modificada con fósforo y es realizada por medio de un procedimiento que comprende las siguientes etapas en este orden, a) proveer una zeolita que comprende al menos un anillo de diez miembros en la estructura, opcionalmente vaporizar dicha zeolita, b) mezclar dicha zeolita de la etapa a) con al menos un componente seleccionado entre uno o más ligantes y aditivos de conformación, después conformar dicha mezcla, c) opcionalmente realizar un intercambio iónico, d) opcionalmente vaporizar el catalizar conformado, de modo opcional antes de la etapa c), siendo al menos una entre dicha vaporización de la etapa d) y la vaporización de la etapa a) obligatoria, e) introducir fósforo en el catalizador para introducir al menos 0,1% en peso de fósforo, realizándose dicha introducción mediante impregnación seca o deposición química al vapor, f) opcionalmente introducir un metal, opcionalmente en forma simultánea con la etapa e), g) opcionalmente lavar el catalizador, h) opcionalmente calcinar el catalizador, i) vaporizar el catalizador, que también se denomina como etapa de equilibrado. En una segunda realización puede introducirse el fósforo por cualesquier medio y en la etapa i) la severidad de vaporización (X) es al menos aproximadamente 2. En dicha segunda realización, el catalizador ventajosamente es vaporizado a una temperatura superior a 625ºC, preferentemente en el intervalo 700 a 800ºC. El metal de la etapa f) es ventajosamente calcio.

4. 发明专利

JP2011143408A Catalyst and process for hydrocracking hydrocarbon-containing feedstocks 有权
标题翻译：含烃装置的催化剂和工艺
公开(公告)号：JP2011143408A
公开(公告)日：2011-07-28
申请号：JP2011089847
申请日：2011-04-14
申请人： IFP Energies Nouvelles , イエフペエネルジヌヴェルIfp Energies Nouvelles
发明人： EUZEN PATRICK , BOBIN CAROLE , ROY AUBERGER MAGALIE , BENAZZI ERIC , BOURGES PATRICK , GUERET CHRISTOPHE
IPC分类号： B01J23/85 , B01J21/12 , B01J23/24 , B01J23/42 , B01J23/74 , B01J23/888 , B01J32/00 , B01J35/00 , B01J35/02 , B01J35/10 , B01J37/00 , C10G45/02 , C10G47/12 , C10G47/14 , C10G47/16 , C10G47/20 , C10G47/30 , C10G65/12 , C10G65/14
CPC分类号： B01J35/10 , B01J21/12 , B01J23/24 , B01J23/42 , B01J23/74 , B01J23/85 , B01J23/888 , B01J35/002 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J35/108 , B01J37/0009 , C10G47/12 , C10G47/14 , C10G47/16 , C10G47/20 , C10G65/12 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/4018 , C10G2300/70
摘要： PROBLEM TO BE SOLVED: To provide a process to prepare a hydrocracking catalyst which is small in macropore amount and has an improved catalytic function in a hydrocracking process. SOLUTION: The catalyst comprises at least one dehydrogenating element selected from the group consisting of elements of group VIB and group VIII in the periodic table, a non-zeolitic silica-alumina-based substrate containing an amount of more than 10 wt.% and less than or equal to 80 wt.% of silica, and has the following characteristics: a mean pore diameter of 20 to 140 Å, measured by mercury porosimetry, a total pore volume of 0.1 to 0.6 ml/g, measured by mercury porosimetry, a total pore volume of 0.1 to 0.6 ml/g, measured by nitrogen porosimetry, a BET specific surface area in the range of 150 to 500 m 2 /g, a pore volume of less than 0.1 ml/g contained in the pores with diameters of larger than 140 Å, measured by mercury porosimetry, and a pore volume of less than 0.1 ml/g contained in the pores with diameters of larger than 160 Å, measured by mercury porosimetry. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种制备加氢裂化催化剂的方法，所述加氢裂化催化剂在大孔中的量很小，并且在加氢裂化方法中具有改进的催化功能。解决方案：催化剂包含至少一种选自元素周期表中VIB族和VIII族的元素的脱氢元素，非沸石二氧化硅 - 氧化铝基底，其含量大于10wt。％和小于或等于80重量％的二氧化硅，并且具有以下特征：通过水银孔率法测量的平均孔径为20至140，总孔体积为0.1至0.6ml / g，通过汞测量孔隙率法，通过氮气孔率法测量的总孔体积为0.1至0.6ml / g，BET比表面积在150至500m 2 / SP / g的范围内，孔体积小于0.1 通过水银孔率法测量直径大于140埃的孔中所含的ml / g，通过水银孔率法测量的直径大于160埃的孔中所含的孔体积小于0.1ml / g。版权所有（C）2011，JPO＆INPIT

5. 发明申请

WO2013093221A3 METHOD FOR MANUFACTURING SPHEROIDAL ALUMINA PARTICLES 审中-公开
标题翻译：制造氧化铝颗粒的方法
公开(公告)号：WO2013093221A3
公开(公告)日：2013-12-19
申请号：PCT/FR2012000466
申请日：2012-11-16
申请人： IFP ENERGIES NOUVELLES
发明人： LACOMBE SYLVIE , AVENIER PRISCILLA , BOUALLEG MALIKA , BAZER-BACHI DELPHINE , EUZEN PATRICK , LOPEZ JOSEPH
IPC分类号： C01F7/02 , B01J21/04 , B01J35/10 , B01J37/00 , C01F7/44 , C04B35/111 , C04B35/626
CPC分类号： B01J21/04 , B01J27/135 , B01J35/1019 , B01J35/1042 , B01J35/108 , B01J37/0072 , C01F7/02 , C01F7/447 , C01P2004/32 , C01P2006/11 , C01P2006/12 , C01P2006/14 , C01P2006/21 , C04B35/111 , C04B35/6263 , C04B2235/3218 , C04B2235/322 , C04B2235/5436 , C04B2235/94
摘要： The present invention relates to spheroidal alumina particles, to catalysts including such particles as a support, and to a method for manufacturing spheroidal alumina particles that includes the following steps: a) preparing a suspension including water, an acid, and at least one boehmite powder, the ratio of the crystallite sizes of which in directions [020] and [120], obtained by X-ray diffraction using the Scherrer equation, is between 0.7 and 1; b) adding a porogenic agent, a surfactant, and optionally water, or an emulsion including at least one porogenic agent, a surfactant, and water, to the suspension of step a); c) mixing the suspension obtained in step b); d) shaping the spheroidal particles from the suspension obtained in step c) by drop coagulation; e) drying the particles obtained in step d); and f) calcining the particles obtained in step e).
摘要翻译：本发明涉及球状氧化铝颗粒，包括作为载体的颗粒的催化剂，以及制造球状氧化铝颗粒的方法，包括以下步骤：a）制备包括水，酸和至少一种勃姆石粉末的悬浮液，使用Scherrer方程通过X射线衍射获得的方向[020]和[120]的微晶尺寸的比率在0.7和1之间; b）向步骤a）的悬浮液中加入致孔剂，表面活性剂和任选的水，或包含至少一种致孔剂，表面活性剂和水的乳液; c）将步骤b）中获得的悬浮液混合; d）通过液滴凝结从步骤c）中获得的悬浮液中形成球状颗粒; e）干燥步骤d）中获得的颗粒; 和f）煅烧步骤e）中获得的颗粒。

6. 发明专利

PL2739390T3 Sposób przekształcania co najmniej jednego alkoholu w olefiny lekkie 未知
公开(公告)号：PL2739390T3
公开(公告)日：2021-10-11
申请号：PL12738463
申请日：2012-07-25
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOW
发明人： NESTERENKO NIKOLAI , MINOUX DELPHINE , ADAM CINDY , DATH JEAN-PIERRE , LOPEZ JOSEPH , EUZEN PATRICK
IPC分类号： B01J29/40 , B01J29/85 , B01J37/10 , B01J37/28 , C07C1/20

7. 发明专利

DK2739390T3 FREMGANGSMÅDE TIL OMDANNELSE AF MINDST EN ALKOHOL TIL LETTE OLEFINER 未知
公开(公告)号：DK2739390T3
公开(公告)日：2021-03-29
申请号：DK12738463
申请日：2012-07-25
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOW
发明人： DATH JEAN-PIERRE , NESTERENKO NIKOLAI , MINOUX DELPHINE , ADAM CINDY , LOPEZ JOSEPH , EUZEN PATRICK
IPC分类号： B01J29/40 , B01J29/85 , B01J37/10 , B01J37/28 , C07C1/20

8. 发明专利

CA2842388C METHOD FOR MAKING A CATALYST COMPRISING A PHOSPHORUS MODIFIED ZEOLITE AND USE OF SAID ZEOLITE 未知
公开(公告)号：CA2842388C
公开(公告)日：2020-10-06
申请号：CA2842388
申请日：2012-07-25
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOW
发明人： NESTERENKO NIKOLAI , MINOUX DELPHINE , ADAM CINDY , DATH JEAN-PIERRE , LOPEZ JOSEPH , EUZEN PATRICK
IPC分类号： B01J29/40 , B01J29/85 , B01J37/10 , B01J37/28 , C07C1/20
摘要： The present invention relates, in a first embodiment, to a method to make a phosphorus modified zeolite comprising the following steps in this order, a) providing a zeolite comprising at least one ten members ring in the structure, optionally steaming said zeolite, b) mixing said zeolite of step a) with at least a component selected among one or more binders and shaping additives, then shaping said mixture, c) optionally making a ion-exchange, d) optionally steaming the shaped catalyst, optionally before step c), at least among said steaming of step d) and the steaming of step a) one is mandatory, e) introducing phosphorus on the catalyst to introduce at least 0.1 wt% of phosphorus, said introduction being made by dry impregnation or chemical vapor deposition, f) introducing a metal, optionally simultaneously with step e), g) optionally washing the catalyst, h) optionally calcinating the catalyst, i) steaming the catalyst, also referred to as the equilibration step. In a second embodiment phosphorus can be introduced by any means and at step i) the steaming severity (X) is at least about 2. In said second embodiment the catalyst is advantageously steamed at a temperature above 625°C, preferably in the range 700 to 800°C. The metal of step f) is advantageously Calcium. The present invention also relates to the use said catalyst in the alcohol dehydration, the olefin cracking to make lighter olefins, the MTO and the alkylation of aromatics by alcohols with olefins and/or alcohols.

9. 发明专利

CA2844363C CATALYST COMPRISING A PHOSPHORUS MODIFIED ZEOLITE AND HAVING PARTLY AN ALPO STRUCTURE 未知
公开(公告)号：CA2844363C
公开(公告)日：2020-07-14
申请号：CA2844363
申请日：2012-07-25
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOW
发明人： NESTERENKO NIKOLAI , MINOUX DELPHINE , ADAM CINDY , DATH JEAN-PIERRE , LOPEZ JOSEPH , EUZEN PATRICK
IPC分类号： B01J29/40 , B01J29/85 , B01J37/10 , B01J37/28 , C07C1/20
摘要： The present invention relates to a catalyst comprising a phosphorus modified zeolite, said phosphorus modified zeolite having partly an ALPOstructure, wherein, the catalyst comprises a P-modified zeolite and a binder, the zeolite comprises at least one ten members ring in the structure, optionally the catalyst comprises one or more metal oxides, the ALPO structure is determined by a signal between 35-45 ppm in 27 Al MAS NMR spectrum. The present invention also relates to the use of the above catalyst wherein said catalyst is operated in presence of steam at high temperature. "high temperature" means above 300°C and up to 800°C. By way of example one can cite, the alcohol dehydration to convert at least an alcohol into the corresponding olefin, the olefin cracking to make lighter olefins, the MTO and the alkylation of aromatic compounds with olefins and/or alcohols to produce, by way of example, paraxylene, ethylbenzene, cumene etc.

10. 发明专利

EA028628B1 ПРИМЕНЕНИЕ КАТАЛИЗАТОРА НА ОСНОВЕ МОДИФИЦИРОВАННОГО ФОСФОРОМ ЦЕОЛИТА В ПРОЦЕССЕ ДЕГИДРАТАЦИИ СПИРТОВ 未知
公开(公告)号：EA028628B1
公开(公告)日：2017-12-29
申请号：EA201490359
申请日：2012-07-25
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOW
发明人： NESTERENKO NIKOLAI , MINOUX DELPHINE , ADAM CINDY , DATH JEAN-PIERRE , LOPEZ JOSEPH , EUZEN PATRICK
IPC分类号： B01J29/40 , B01J29/85 , B01J37/10 , B01J37/28 , C07C1/20
摘要： Впервомвариантереализациинастоящееизобретениеотноситсяк применениюкатализаторадляконвертациипоменьшеймереодногоспиртав лёгкиеолефиныв процесседегидратациис получениемолефина, имеющегоодинаковоесоспиртомчислоатомовуглерода, приэтомкатализаторприготовленнаосновемодифицированногофосфоромцеолитаспособом, включающимследующиешагив указаннойпоследовательности: a) взятьцеолит, вструктурукотороговходитхотябыоднодесятичленноекольцо, поусмотрениюобработатьцеолитпаром; b) смешатьцеолит, указанныйв шаге a), какминимумс однимизсвязующихкомпонентови структуронаправляющихагентов, послечегосформоватьсмесь; c) поусмотрениювыполнитьионообмен; d) поусмотрениюобработатьпаромсформованныйкатализатор, произвольно - передшагом c), приэтомпоменьшеймереоднаизуказанныхобработокпаромнашаге d) инашаге a) обязательна; e) ввестив катализаторпоменьшеймере 0,1 мас.% фосфора, применяясухуюимпрегнациюилипарофазноехимическоеосаждение; f) поусмотрениюввестиметалл, произвольно - одновременнос шагом e); g) поусмотрениюпромытькатализатор; h) поусмотрениюкальцинировать (прокалить) катализатор; i) обработатькатализаторпаром - шаг, называемыйтакжеприведениемв равновесноесостояние. Вовторомвариантереализациифосформожетбытьвведёнлюбымспособом, инашаге i) интенсивностьпарообработки (X) поменьшеймереоколо 2. Вовторомвариантереализациикатализаторпредпочтительноподвергаютобработкепаромпритемпературевыше 625°C, преимущественнов диапазонеот 700 до 800°C. Металлнашаге f) предпочтительнокальций.

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