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1. 发明专利

JP2011143408A Catalyst and process for hydrocracking hydrocarbon-containing feedstocks 有权
标题翻译：含烃装置的催化剂和工艺
公开(公告)号：JP2011143408A
公开(公告)日：2011-07-28
申请号：JP2011089847
申请日：2011-04-14
申请人： IFP Energies Nouvelles , イエフペエネルジヌヴェルIfp Energies Nouvelles
发明人： EUZEN PATRICK , BOBIN CAROLE , ROY AUBERGER MAGALIE , BENAZZI ERIC , BOURGES PATRICK , GUERET CHRISTOPHE
IPC分类号： B01J23/85 , B01J21/12 , B01J23/24 , B01J23/42 , B01J23/74 , B01J23/888 , B01J32/00 , B01J35/00 , B01J35/02 , B01J35/10 , B01J37/00 , C10G45/02 , C10G47/12 , C10G47/14 , C10G47/16 , C10G47/20 , C10G47/30 , C10G65/12 , C10G65/14
CPC分类号： B01J35/10 , B01J21/12 , B01J23/24 , B01J23/42 , B01J23/74 , B01J23/85 , B01J23/888 , B01J35/002 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J35/108 , B01J37/0009 , C10G47/12 , C10G47/14 , C10G47/16 , C10G47/20 , C10G65/12 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/4018 , C10G2300/70
摘要： PROBLEM TO BE SOLVED: To provide a process to prepare a hydrocracking catalyst which is small in macropore amount and has an improved catalytic function in a hydrocracking process. SOLUTION: The catalyst comprises at least one dehydrogenating element selected from the group consisting of elements of group VIB and group VIII in the periodic table, a non-zeolitic silica-alumina-based substrate containing an amount of more than 10 wt.% and less than or equal to 80 wt.% of silica, and has the following characteristics: a mean pore diameter of 20 to 140 Å, measured by mercury porosimetry, a total pore volume of 0.1 to 0.6 ml/g, measured by mercury porosimetry, a total pore volume of 0.1 to 0.6 ml/g, measured by nitrogen porosimetry, a BET specific surface area in the range of 150 to 500 m 2 /g, a pore volume of less than 0.1 ml/g contained in the pores with diameters of larger than 140 Å, measured by mercury porosimetry, and a pore volume of less than 0.1 ml/g contained in the pores with diameters of larger than 160 Å, measured by mercury porosimetry. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种制备加氢裂化催化剂的方法，所述加氢裂化催化剂在大孔中的量很小，并且在加氢裂化方法中具有改进的催化功能。解决方案：催化剂包含至少一种选自元素周期表中VIB族和VIII族的元素的脱氢元素，非沸石二氧化硅 - 氧化铝基底，其含量大于10wt。％和小于或等于80重量％的二氧化硅，并且具有以下特征：通过水银孔率法测量的平均孔径为20至140，总孔体积为0.1至0.6ml / g，通过汞测量孔隙率法，通过氮气孔率法测量的总孔体积为0.1至0.6ml / g，BET比表面积在150至500m 2 / SP / g的范围内，孔体积小于0.1 通过水银孔率法测量直径大于140埃的孔中所含的ml / g，通过水银孔率法测量的直径大于160埃的孔中所含的孔体积小于0.1ml / g。版权所有（C）2011，JPO＆INPIT

2. 发明申请

WO2013093221A3 METHOD FOR MANUFACTURING SPHEROIDAL ALUMINA PARTICLES 审中-公开
标题翻译：制造氧化铝颗粒的方法
公开(公告)号：WO2013093221A3
公开(公告)日：2013-12-19
申请号：PCT/FR2012000466
申请日：2012-11-16
申请人： IFP ENERGIES NOUVELLES
发明人： LACOMBE SYLVIE , AVENIER PRISCILLA , BOUALLEG MALIKA , BAZER-BACHI DELPHINE , EUZEN PATRICK , LOPEZ JOSEPH
IPC分类号： C01F7/02 , B01J21/04 , B01J35/10 , B01J37/00 , C01F7/44 , C04B35/111 , C04B35/626
CPC分类号： B01J21/04 , B01J27/135 , B01J35/1019 , B01J35/1042 , B01J35/108 , B01J37/0072 , C01F7/02 , C01F7/447 , C01P2004/32 , C01P2006/11 , C01P2006/12 , C01P2006/14 , C01P2006/21 , C04B35/111 , C04B35/6263 , C04B2235/3218 , C04B2235/322 , C04B2235/5436 , C04B2235/94
摘要： The present invention relates to spheroidal alumina particles, to catalysts including such particles as a support, and to a method for manufacturing spheroidal alumina particles that includes the following steps: a) preparing a suspension including water, an acid, and at least one boehmite powder, the ratio of the crystallite sizes of which in directions [020] and [120], obtained by X-ray diffraction using the Scherrer equation, is between 0.7 and 1; b) adding a porogenic agent, a surfactant, and optionally water, or an emulsion including at least one porogenic agent, a surfactant, and water, to the suspension of step a); c) mixing the suspension obtained in step b); d) shaping the spheroidal particles from the suspension obtained in step c) by drop coagulation; e) drying the particles obtained in step d); and f) calcining the particles obtained in step e).
摘要翻译：本发明涉及球状氧化铝颗粒，包括作为载体的颗粒的催化剂，以及制造球状氧化铝颗粒的方法，包括以下步骤：a）制备包括水，酸和至少一种勃姆石粉末的悬浮液，使用Scherrer方程通过X射线衍射获得的方向[020]和[120]的微晶尺寸的比率在0.7和1之间; b）向步骤a）的悬浮液中加入致孔剂，表面活性剂和任选的水，或包含至少一种致孔剂，表面活性剂和水的乳液; c）将步骤b）中获得的悬浮液混合; d）通过液滴凝结从步骤c）中获得的悬浮液中形成球状颗粒; e）干燥步骤d）中获得的颗粒; 和f）煅烧步骤e）中获得的颗粒。

3. 发明专利

SG10201602108UA METHOD FOR MANUFACTURING SPHEROIDAL ALUMINA PARTICLES 未知
公开(公告)号：SG10201602108UA
公开(公告)日：2016-04-28
申请号：SG10201602108U
申请日：2012-11-16
申请人： IFP ENERGIES NOUVELLES
发明人： LACOMBE SYLVIE , AVENIER PRISCILLA , BOUALLEG MALIKA , BAZER-BACHI DELPHINE , EUZEN PATRICK , LOPEZ JOSEPH
摘要： The present invention concerns spheroidal alumina particles, catalysts comprising such particles as a support and a process for the production of spheroidal alumina particles, comprising the following steps: a) preparing a suspension comprising water, an acid and at least one boehmite powder for which the ratio of the crystallite dimensions in the [020] and [120] directions obtained using the Scherrer X-ray diffraction formula is in the range 0.7 to 1; b) adding a pore-forming agent, a surfactant and optionally water, or an emulsion comprising at least one pore-forming agent, a surfactant and water to the suspension of step a); c) mixing the suspension obtained in step b); d) shaping the spheroidal particles by the oil-drop method using the suspension obtained in step c); e) drying the particles obtained in step d); f) calcining the particles obtained in step e).

4. 发明专利

AR087461A1 USO DE UN CATALIZADOR QUE COMPRENDE UNA ZEOLITA MODIFICADA CON FOSFORO EN UN PROCESO DE DESHIDRATACION DE ALCOHOL 未知
公开(公告)号：AR087461A1
公开(公告)日：2014-03-26
申请号：ARP120102856
申请日：2012-08-03
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOUVELLES
发明人： NESTERENKO NIKOLAI , ADAM CINDY , EUZEN PATRICK , LOPEZ JOSEPH , MINOUX DELPHINE , DATH JEAN-PIERRE
IPC分类号： B01J29/40 , B01J29/85 , B01J37/10 , B01J37/28 , C07C1/20 , C07C1/24
摘要： La presente se refiere, en una primera realización, al uso de un catalizador para convertir al menos un alcohol en olefinas livianas en un proceso de deshidratación para producir una olefina que tiene el mismo número de átomos de carbono que el alcohol, en el que dicho catalizador comprende una zeolita modificada con fósforo y es realizada por medio de un procedimiento que comprende las siguientes etapas en este orden, a) proveer una zeolita que comprende al menos un anillo de diez miembros en la estructura, opcionalmente vaporizar dicha zeolita, b) mezclar dicha zeolita de la etapa a) con al menos un componente seleccionado entre uno o más ligantes y aditivos de conformación, después conformar dicha mezcla, c) opcionalmente realizar un intercambio iónico, d) opcionalmente vaporizar el catalizar conformado, de modo opcional antes de la etapa c), siendo al menos una entre dicha vaporización de la etapa d) y la vaporización de la etapa a) obligatoria, e) introducir fósforo en el catalizador para introducir al menos 0,1% en peso de fósforo, realizándose dicha introducción mediante impregnación seca o deposición química al vapor, f) opcionalmente introducir un metal, opcionalmente en forma simultánea con la etapa e), g) opcionalmente lavar el catalizador, h) opcionalmente calcinar el catalizador, i) vaporizar el catalizador, que también se denomina como etapa de equilibrado. En una segunda realización puede introducirse el fósforo por cualesquier medio y en la etapa i) la severidad de vaporización (X) es al menos aproximadamente 2. En dicha segunda realización, el catalizador ventajosamente es vaporizado a una temperatura superior a 625ºC, preferentemente en el intervalo 700 a 800ºC. El metal de la etapa f) es ventajosamente calcio.

5. 发明专利

FR3022235A1 GEL HAUTE DISPERSIBILITE ET SON PROCEDE DE PREPARATION 未知
公开(公告)号：FR3022235A1
公开(公告)日：2015-12-18
申请号：FR1455421
申请日：2014-06-13
申请人： IFP ENERGIES NOUVELLES
发明人： BOUALLEG MALIKA , BOUVRY CELINE , EUZEN PATRICK
IPC分类号： C01F7/02 , C01F7/14
摘要： On décrit un nouveau gel d'alumine présentant un indice de dispersibilité élevé, et en particulier un indice de dispersibilité supérieur à 70%, une taille de cristallite comprise entre 1 à 35 nm, ainsi qu'une teneur en soufre comprise entre 0,001% et 2% poids et une teneur en sodium comprise entre 0,001% et 2 % poids, les pourcentages poids étant exprimés par rapport à la masse totale de gel d'alumine. La présente invention concerne également le procédé de préparation dudit gel comprenant au moins une étape de précipitation d'au moins un sel d'aluminium, au moins une étape de chauffage de la suspension obtenue et une étape finale de traitement thermique pour former le gel d'alumine.

6. 发明专利

CO7020925A2 Uso de un catalizador que comprende una zeolita modificada con fósforo en un procedimiento de deshidratación de un alcohol 未知
公开(公告)号：CO7020925A2
公开(公告)日：2014-08-11
申请号：CO14038375
申请日：2014-02-24
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOUVELLES
发明人： NESTERENKO NIKOLAI , MINOUX DELPHINE , ADAM CINDY , LOPEZ JOSEPH , EUZEN PATRICK
IPC分类号： B01J29/40

7. 发明专利

FR2984180A1 PROCEDE DE FABRICATION DE PARTICULES SPHEROIDALES D'ALUMINE 未知
公开(公告)号：FR2984180A1
公开(公告)日：2013-06-21
申请号：FR1103998
申请日：2011-12-20
申请人： IFP ENERGIES NOUVELLES
发明人： LACOMBE SYLVIE , AVENIER PRISCILLA , BOUALLEG MALIKA , BAZER BACHI DELPHINE , EUZEN PATRICK , LOPEZ JOSEPH
IPC分类号： B01J2/08 , B01J32/00 , C10G11/02 , C10G35/06 , C10G45/04 , C10G47/12
摘要： La présente invention concerne un procédé de fabrication de particules sphéroïdales d'alumine comprenant les étapes suivantes: a) préparation d'une suspension comprenant de l'eau, un acide et au moins une poudre de boehmite présentant des raies de diffraction X [020] et [120] dont le rapport des intensités de raie [020]/[120] est compris entre 0,7 et 1 ; b) préparation d'une émulsion comprenant un agent porogène, un tensioactif et de l'eau; c) mélange de la suspension de l'étape a) et l'émulsion de l'étape b); d) mise en forme des particules sphéroïdales par coagulation en goutte à partir du mélange de l'étape c); e) séchage des particules obtenues à l'étape d); f) calcination des particules obtenues à l'étape e).

8. 发明专利

CA2842386A1 USE OF A CATALYST COMPRISING A PHOSPHORUS MODIFIED ZEOLITE IN AN ALCOHOL DEHYDRATION PROCESS 未知
公开(公告)号：CA2842386A1
公开(公告)日：2013-02-07
申请号：CA2842386
申请日：2012-07-25
申请人： TOTAL RES & TECHNOLOGY FELUY , IFP ENERGIES NOUVELLES
发明人： NESTERENKO NIKOLAI , MINOUX DELPHINE , ADAM CINDY , DATH JEAN-PIERRE , LOPEZ JOSEPH , EUZEN PATRICK
IPC分类号： B01J29/40 , B01J29/85 , B01J37/10 , B01J37/28 , C07C1/20
摘要： The present invention relates, in a first embodiment, to the use of a catalyst to convert at least an alcohol into light olefins in a dehydration process to make an olefin having the same number of carbon atoms as the alcohol wherein said catalyst comprises a phosphorus modified zeolite and is made by a method comprising the following steps in this order, a) providing a zeolite comprising at least one ten members ring in the structure, optionally steaming said zeolite, b) mixing said zeolite of step a) with at least a component selected among one or more binders and shaping additives, then shaping said mixture, c) optionally making a ion-exchange, d) optionally steaming the shaped catalyst, optionally before step c), at least among said steaming of step d) and the steaming of step a) one is mandatory, e) introducing phosphorus on the catalyst to introduce at least 0.1 wt% of phosphorus, said introduction being made by dry impregnation or chemical vapor deposition, f) optionally introducing a metal, optionally simultaneously with step e), g) optionally washing the catalyst, h) optionally calcinating the catalyst, i) steaming the catalyst, also referred to as the equilibration step. In a second embodiment phosphorus can be introduced by any means and at step i) the steaming severity (X) is at least about 2. In said second embodiment the catalyst is advantageously steamed at a temperature above 625°C, preferably in the range 700 to 800°C. The metal of step f) is advantageously Calcium.

9. 发明专利

SG11201403195UA METHOD FOR MANUFACTURING SPHEROIDAL ALUMINA PARTICLES 未知
公开(公告)号：SG11201403195UA
公开(公告)日：2014-09-26
申请号：SG11201403195U
申请日：2012-11-16
申请人： IFP ENERGIES NOUVELLES
发明人： LACOMBE SYLVIE , AVENIER PRISCILLA , BOUALLEG MALIKA , BAZER-BACHI DELPHINE , EUZEN PATRICK , LOPEZ JOSEPH
IPC分类号： C01F7/02 , B01J21/04 , B01J35/10 , B01J37/00 , C01F7/44 , C04B35/111 , C04B35/626
摘要： The present invention concerns spheroidal alumina particles, catalysts comprising such particles as a support and a process for the production of spheroidal alumina particles, comprising the following steps: a) preparing a suspension comprising water, an acid and at least one boehmite powder for which the ratio of the crystallite dimensions in the [020] and [120] directions obtained using the Scherrer X-ray diffraction formula is in the range 0.7 to 1; b) adding a pore-forming agent, a surfactant and optionally water, or an emulsion comprising at least one pore-forming agent, a surfactant and water to the suspension of step a); c) mixing the suspension obtained in step b); d) shaping the spheroidal particles by the oil-drop method using the suspension obtained in step c); e) drying the particles obtained in step d); f) calcining the particles obtained in step e).

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