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1. 发明申请

WO1997033193A3 CROSS-LINKABLE OR CHAIN EXTENDABLE POLYARYLPOLYAMINES AND FILMS THEREOF 审中-公开
公开(公告)号：WO1997033193A3
公开(公告)日：1997-09-12
申请号：PCT/US1997/002643
申请日：1997-02-20
申请人： THE DOW CHEMICAL COMPANY
发明人： WOO, Edmund, P. , INBASEKARAN, Michael , SHIANG, William, R. , ROOF, Gordon, R. , WU, Weishi
IPC分类号： H05B33/14
摘要： A compound of formula (XVI), wherein R 1 is independently in each occurrence hydrogen or formula (i); Ar 1 independently in each occurrence is a C 6-20 aromatic group or C 3-20 heterocyclic group, optionally substituted with up to 5 C 1-10 alkyl, alkoxy, thioalkoxy, aryloxy, or tertiary amine groups; Ar 2 is independently in each occurrence a C 6-20 aromatic group, optionally substituted with up to 4 C 1-10 alkyl, alkoxy, or thioalkoxy groups; E 1 is independently in each occurrence a C 1-20 hydrocarbyl radical, or a group capable of chemically reacting in a chain-reaction or step-reaction polymerization process at a temperature of less than 300 °C at 1 atmosphere, with the identical group or other reactive groups attached to a separate monomer or polymer species, forming a covalent bond therebetween; and wherein the nitrogen atoms attached to the Ar 2 groups are located in positions which permit them to be in conjugation with any other nitrogen atom attached to the same Ar 2 group; q is an integer of from 1 to 4; and s is an integer from 1 to 4. Films of the compounds of the invention, as well as films of polymers of cross-linkable species of such compounds, are efficient in the transport of positive charges when exposed to relatively low voltage levels.

2. 发明申请

WO2003007395A1 ELECTROACTIVE POLYMERS AND DEVICES MADE THEREFROM 审中-公开
标题翻译：电动聚合物及其制造方法
公开(公告)号：WO2003007395A1
公开(公告)日：2003-01-23
申请号：PCT/US2002/022308
申请日：2002-07-10
申请人： THE DOW CHEMICAL COMPANY
发明人： WU, Weishi , INBASEKARAN, Michael , BERNIUS, Mark, T. , O'BRIEN, James, J.
IPC分类号： H01L51/20
CPC分类号： H01B1/124 , C09K11/06 , C09K2211/1416 , C09K2211/1425 , C09K2211/1433 , C09K2211/1458 , C09K2211/1483 , H01L51/0036 , H01L51/0038 , H01L51/0039 , H01L51/0043 , H01L51/0059 , H01L51/5012
摘要： An organic block polymer useful in an electroluminescent polymer device (or in a polymer field effect transistor) that includes an emissive polymer block that is consistently conjugated along the backbone of the emissive polymer block (e.g., a copolymer of 2,7-linked 9,9 dioctyl fluorene and 4,7-linked 2,1,3 benxothiadiazole); and a positive charge carrier polymer block that is consistently conjugated along the backbone of the positive charge carrier polymer block (e.g., a copolymer of 2,7-linked 9,9 dioctyl fluorene and 4N, 4N'-linked N,N'-di(3-carboxomethoxyphenyl)benzidine) for transporting positive charge carriers to the emissive polymer block so that the positive charge carriers can combine with negative charge carriers to generate light.
摘要翻译：可用于电致发光聚合物装置（或聚合物场效应晶体管）中的有机嵌段聚合物，其包括沿发射聚合物嵌段的主链一致地共轭的发射聚合物嵌段（例如，2,7-连接的9， 9个二辛基芴和4,7-连接的2,1,3苯噻二唑）; 和正电荷载体聚合物嵌段，其沿着正电荷载体聚合物嵌段的主链一致地共轭（例如，2,7-连接的9,9二辛基芴和4N，4N'连接的N，N'-二（3-甲基甲氧基苯基）联苯胺），用于将正电荷载体输送到发射聚合物嵌段，使得正电荷载体可以与负电荷载体组合以产生光。

3. 发明申请

WO1998006773A1 POLY(ARYLAMINES) AND FILMS THEREOF 审中-公开
标题翻译： POLY（ARYLAMINES）及其薄膜
公开(公告)号：WO1998006773A1
公开(公告)日：1998-02-19
申请号：PCT/US1997012478
申请日：1997-07-14
申请人： THE DOW CHEMICAL COMPANY
发明人： THE DOW CHEMICAL COMPANY , WU, Weishi , SHIANG, William, R. , WOO, Edmund, P.
IPC分类号： C08G73/02
CPC分类号： C08G73/026 , Y10T428/31573 , Y10T428/3158 , Y10T428/31678
摘要： The invention relates to a poly(arylamine) composition of one or more compounds of from 5 to 1000 of monomer. The monomers useful in the preparation of poly(arylamines) comprise two amino moieties wherein each amino moiety is bound to three aryl moieties wherein two halo moieties are optionally bound to the monomer. The invention further relates to films prepared from such poly(arylamines), as well as electrophotographic devices and electroluminescent devices containing such films, such as polymeric light-emitting diodes. The invention also relates to processes for the preparation of poly(arylamines). The polymers of the invention form films which are relatively high molecular weight charge transport compounds which are capable of forming films. The films can be prepared using relatively small amounts of polymer while still maintaining the desirable properties of transporting positive charges. The processes disclosed herein provide efficient means of preparing the disclosed compounds.
摘要翻译：本发明涉及一种或多种5至1000种单体的化合物的聚（芳基胺）组合物。可用于制备聚（芳基胺）的单体包含两个氨基部分，其中每个氨基部分与三个芳基部分结合，其中两个卤素部分任选地与单体结合。本发明还涉及由这种聚（芳基胺）制备的膜，以及包含这种膜的电子照相装置和电致发光装置，例如聚合物发光二极管。本发明还涉及制备聚（芳基胺）的方法。本发明的聚合物形成了能够形成膜的相对高分子量电荷输送化合物的膜。可以使用相对少量的聚合物制备膜，同时仍然保持输送正电荷的期望性质。本文公开的方法提供了制备所公开的化合物的有效手段。

4. 发明公开

EP0988337A1 FLUORENE-CONTAINING POLYMERS AND ELECTROLUMINESCENT DEVICES THEREFROM 有权
标题翻译：含芴聚合物及其电LUMINESCENT安排
公开(公告)号：EP0988337A1
公开(公告)日：2000-03-29
申请号：EP99918475.7
申请日：1999-04-09
申请人： THE DOW CHEMICAL COMPANY
发明人： WOO, Edmund, P. , BERNIUS, Mark, T. , INBASEKARAN, Michael , WU, Weishi
IPC分类号： C08G73/02 , C08G61/00 , C09K11/06 , H05B33/14
CPC分类号： H05B33/14 , C07C25/22 , C08G61/00 , C08G61/02 , C08G61/12 , C08G73/02 , C08G73/026 , C09K11/06 , H01L51/0039 , H01L51/0043 , H01L51/0059 , H01L51/5012 , Y10S428/917 , Y10T428/31678
摘要： A copolymer comprising 10-90 % by weight of groups of Formula (I) and from 10-90 % by weight of groups selected from Formulas (II), (III), and (IV) and mixtures thereof; wherein R1 is independently in each occurrence H, C¿1?-C20 hydrocarbyl or C1-C20 hydrocarbyl containing one or more S, N, O, P or Si atoms, C4-C16 hydrocarbyl carbonyloxy, C4-C16 aryl(trialkylsiloxy) or both R?1¿ may form with the 9-carbon on the fluorene ring a C¿5?-C20 cycloaliphatic structure or a C4-C20 cycloaliphatic structure containing one or more heteroatoms of S, N, or O; R?2¿ is independently in each occurrence C¿1?-C20 hydrocarbyl, C1-C20 hydrocarbyloxy, C1-C20 thioether, C1-C20 hydrocarbylcarbonyloxy or cyano; R?3¿ is independently in each occurrence carboxyl, C¿1?-C20 alkyl, C1-C20 alkoxy or a group of the formula -CO2R?4¿ wherein R4 is a C¿1?-C20 alkyl; and a and b are independently in each occurrence an integer from 0 to 3.

5. 发明公开

EP1155096A1 FLUORENE COPOLYMERS AND DEVICES MADE THEREFROM 有权
标题翻译：芴共聚物和器件由其制
公开(公告)号：EP1155096A1
公开(公告)日：2001-11-21
申请号：EP99916596.2
申请日：1999-04-09
申请人： THE DOW CHEMICAL COMPANY
发明人： INBASEKARAN, Michael , WOO, Edmund, P. , WU, Weishi , BERNIUS, Mark, T.
IPC分类号： C09K11/06 , C08G61/10 , H01L51/20
CPC分类号： H01L51/5012 , C08G61/02 , C08G61/10 , C09K11/06 , H01L51/0036 , H01L51/0038 , H01L51/0039 , H01L51/0043 , H01L51/0059 , Y02E10/549
摘要： This invention relates to: (a) fluorene copolymers comprising at least 10% (by residual monomeric units) of 9-substituted and/or 9,9-disubstituted fluorene moieties and at least two other monomeric units containing delocalized p-electrons, (b) polymer blends comprising at least 10 weight % of a copolymer specified in (a), and (c) electronic devices (such as polymer light emitting diodes) containing one or more films derived from these copolymers.

6. 发明公开

EP1025142A1 PROCESS FOR PREPARING CONJUGATED POLYMERS 失效
标题翻译：用于生产共轭聚合物
公开(公告)号：EP1025142A1
公开(公告)日：2000-08-09
申请号：EP98923397.8
申请日：1998-05-13
申请人： THE DOW CHEMICAL COMPANY
发明人： INBASEKARAN, Michael , WOO, Edmund, P. , WU, Weishi
IPC分类号： C08G61/00
CPC分类号： H01L51/0039 , C08G61/02 , H01L51/0035 , H01L51/0036 , H01L51/0043 , H01L51/0059 , H01L51/5012
摘要： A process for preparing conjugated polymers which comprises contacting (i) monomers having two reactive groups selected from boronic acid C1-C6 boronic acid ester, C1-C6 borane, and combinations thereof, with aromatic dihalide-functional monomers or (ii) monomers having one reactive boronic acid, boronic acid ester, or borane group and one reactive halide-functional group, with each other; (wherein the monomers are selected so that the polymerization reaction product of such has conjugated unsaturated internal groups) in a reaction mixture which contains: (a) an organic solvent in which the polymer forms at least a 1 percent solution; (b) an aqueous solution of an inorganic base having a pKa in the range of from 9 to 13, said solution having a concentration of at least 0.1 N; (c) a catalytic amount of a palladium complex; and (d) at least 0.01 mole percent of a phase transfer catalyst, based on the number of moles of boronic acid, boric acid ester, and borane groups in the reaction mixture; under reaction conditions sufficient to form the corresponding conjugated polymer.

7. 发明授权

EP0918811B1 POLY(ARYLAMINES) AND FILMS THEREOF 失效
标题翻译：聚（芳香胺）及其薄膜
公开(公告)号：EP0918811B1
公开(公告)日：2000-12-27
申请号：EP97939338.6
申请日：1997-07-14
申请人： THE DOW CHEMICAL COMPANY
发明人： WU, Weishi , SHIANG, William, R. , WOO, Edmund, P.
IPC分类号： C08G73/02
CPC分类号： C08G73/026 , Y10T428/31573 , Y10T428/3158 , Y10T428/31678

8. 发明公开

EP0918811A1 POLY(ARYLAMINES) AND FILMS THEREOF 失效
标题翻译：聚（芳香胺）及其薄膜
公开(公告)号：EP0918811A1
公开(公告)日：1999-06-02
申请号：EP97939338.0
申请日：1997-07-14
申请人： THE DOW CHEMICAL COMPANY
发明人： WU, Weishi , SHIANG, William, R. , WOO, Edmund, P.
IPC分类号： C08G73
CPC分类号： C08G73/026 , Y10T428/31573 , Y10T428/3158 , Y10T428/31678
摘要： The invention relates to a poly(arylamine) composition of one or more compounds of from 5 to 1000 of monomer. The monomers useful in the preparation of poly(arylamines) comprise two amino moieties wherein each amino moiety is bound to three aryl moieties wherein two halo moieties are optionally bound to the monomer. The invention further relates to films prepared from such poly(arylamines), as well as electrophotographic devices and electroluminescent devices containing such films, such as polymeric light-emitting diodes. The invention also relates to processes for the preparation of poly(arylamines). The polymers of the invention form films which are relatively high molecular weight charge transport compounds which are capable of forming films. The films can be prepared using relatively small amounts of polymer while still maintaining the desirable properties of transporting positive charges. The processes disclosed herein provide efficient means of preparing the disclosed compounds.

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