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1. 发明申请

US20080058476A1 TAILORABLE POLYIMIDE PREPOLYMER BLENDS, CROSSLINKED, POLYIMIDES, AND ARTICLES FORMED THEREFROM 审中-公开
标题翻译：可修饰的聚酰亚胺预聚物共混物，交联的聚酰亚胺和其形成的物品
公开(公告)号：US20080058476A1
公开(公告)日：2008-03-06
申请号：US11928210
申请日：2007-10-30
申请人： Stephen Whiteker , Warren Ronk , Lisa Shafer
发明人： Stephen Whiteker , Warren Ronk , Lisa Shafer
IPC分类号： C08J3/24
CPC分类号： C08G73/10 , C08G73/101 , C08G73/1014 , C08L79/08 , C08L2205/02 , C08L2666/20
摘要： A tailorable polyimide prepolymer blend including a diamine component including 1,3-phenylenediamine (mPDA), Bisaniline M, and 1,4-phenylenediamine (pPDA), a dianhydride component including 3,4,3′,4′-benzophenonetetracarboxylic dianhydride (BTDA) and 3,4,3′,4′-biphenyltetracarboxylic dianhydride (BPDA), and an end group component. The components may be provided as a monomeric mixture. The prepolymer blend, prior to cure, may provide at least one predetermined prepolymer blend property; and the cured prepolymer blend may provide a crosslinked polyimide matrix having at least one predetermined crosslinked matrix property. Articles formed from the tailorable polyimide prepolymer blend may include powders, neat resins, coating materials, films, adhesives, fibers, composites, laminates, prepregs and parts.
摘要翻译：包含二胺组分包括1,3-苯二胺（mPDA），双苯胺M和1,4-苯二胺（pPDA）的二聚体组分包括3,4,3'，4'-二苯甲酮四羧酸二酐（BTDA ）和3,4,3'，4'-联苯四羧酸二酐（BPDA）和端基组分。组分可以作为单体混合物提供。预聚物共混物在固化之前可以提供至少一种预定的预聚物共混物性质; 并且固化的预聚物共混物可以提供具有至少一种预定的交联基质特性的交联的聚酰亚胺基体。由可调节的聚酰亚胺预聚物共混物形成的制品可以包括粉末，纯树脂，涂料，膜，粘合剂，纤维，复合材料，层压材料，预浸料和部件。

2. 发明申请

US20070265417A1 CROSSLINKED POLYIMIDE COPOLYMER MATERIAL 审中-公开
标题翻译：交联聚酰亚胺共聚物
公开(公告)号：US20070265417A1
公开(公告)日：2007-11-15
申请号：US11383086
申请日：2006-05-12
申请人： Warren Ronk , Stephen Whiteker
发明人： Warren Ronk , Stephen Whiteker
IPC分类号： C08G73/00
CPC分类号： C08G73/101 , C08G73/1007 , C08G73/1014 , C08G73/1042
摘要： A crosslinked polyimide copolymer having a crosslinked matrix including an R1 group and a an R2 group, and/or an M group. The R1 group and R2 group independently comprise the formula: wherein V is a tetravalent substituted or unsubstited aromatic monocyclie or polycyclic linking structure; and R is a substituted or unsubstituted divalent organic radical. R2 structure is different than the structure for R1. The M group, when present, is selected from the group consisting of a diamine structure, a dianhydride structure and an end group structure, with the M group being in the reacted or unreacted form.
摘要翻译：具有交联基体的交联聚酰亚胺共聚物，其包含R 1和R 2基团和/或M基团。 R 1基团和R 2基团独立地包含下式：其中V是四价取代或未取代的芳族单环或多环连接结构; 并且R是取代或未取代的二价有机基团。 R 2结构不同于R 1'的结构。当M基团存在时，选自二胺结构，二酐结构和端基结构，M基团处于反应或未反应形式。

3. 发明申请

US20060134396A1 Reinforced matrix composite containment duct 有权
标题翻译：钢筋基复合材料防渗管
公开(公告)号：US20060134396A1
公开(公告)日：2006-06-22
申请号：US11021805
申请日：2004-12-22
申请人： Lee Blanton , Gregory Meibers , Stephen Whiteker , Robert Fairbanks , Richard Price , Warren Ronk
发明人： Lee Blanton , Gregory Meibers , Stephen Whiteker , Robert Fairbanks , Richard Price , Warren Ronk
IPC分类号： D04H13/00 , D04H5/00
CPC分类号： F01D21/045 , B29C70/465 , B29L2031/7504 , F05D2300/614 , F05D2300/702 , Y02T50/672 , Y10T428/249924
摘要： A reinforced matrix composite containment duct for gas turbine engines comprising a reinforced matrix composite containment duct having high strength integral flanges and pre-stressed reinforcing fibers, the reinforced matrix composite having uniform distribution of matrix material; and the reinforced matrix composite having less than or equal to 2.5% void space.
摘要翻译：一种用于燃气涡轮发动机的增强基体复合容纳管，其包括具有高强度整体凸缘和预应力增强纤维的增强基体复合容纳管，所述增强基体复合材料具有均匀的基体材料分布; 和具有小于或等于2.5％空隙空间的增强基质复合材料。

4. 发明申请

US20070265420A1 FIBER REINFORCED GAS TURBINE ENGINE COMPONENT 审中-公开
标题翻译：纤维增强气体涡轮发动机部件
公开(公告)号：US20070265420A1
公开(公告)日：2007-11-15
申请号：US11383092
申请日：2006-05-12
申请人： Warren Ronk , Stephen Whiteker
发明人： Warren Ronk , Stephen Whiteker
IPC分类号： C08G69/26
CPC分类号： C08G73/101
摘要： A gas turbine engine component comprising a fiber reinforced matrix. The matrix includes a crosslinked matrix including an R1 group and a an R2 group, and/or an M group. The R1 group and R2 group independently comprise the formula: wherein V is a tetravalent substituted or unsubstituted aromatic monocyclie or polycyclic linking structure; and R is a substituted or unsubstituted divalent organic radical. R2 structure is different than the structure for R1. The M group, when present, is selected from the group consisting of a diamine structure, a dianhydride structure and an end group structure, with the M group being in the reacted or unreacted form. The crosslinked matrix has a glass transition temperature and a thermal oxidative stability sufficient to provide component stability for operational temperature up to about 550° F.
摘要翻译：一种燃气涡轮发动机部件，包括纤维增强基体。该基质包括含有R 1和R 2基团和/或M基团的交联基质。 R 1基团和R 2 H 2基团独立地包含下式：其中V是四价取代或未取代的芳族单环或多环连接结构; 并且R是取代或未取代的二价有机基团。 R 2结构不同于R 1'的结构。当M基团存在时，选自二胺结构，二酐结构和端基结构，M基团处于反应或未反应形式。交联基质具有足以提供高达约550°F的操作温度的组分稳定性的玻璃化转变温度和热氧化稳定性。

5. 发明申请

US20060130993A1 Method for fabricating reinforced composite materials 失效
标题翻译：制造增强复合材料的方法
公开(公告)号：US20060130993A1
公开(公告)日：2006-06-22
申请号：US11021804
申请日：2004-12-22
申请人： Lee Blanton , Gregory Meibers , Stephen Whiteker , Matthew Buczek , Robert Fairbanks , Richard Price , Warren Ronk
发明人： Lee Blanton , Gregory Meibers , Stephen Whiteker , Matthew Buczek , Robert Fairbanks , Richard Price , Warren Ronk
IPC分类号： B22D19/14
CPC分类号： B29C70/546 , B29C70/44 , B29C70/465 , B29L2031/7504 , F01D21/045 , F05D2300/614 , F05D2300/702 , Y02T50/672 , Y10T428/249928 , Y10T428/249933 , Y10T428/24994 , Y10T428/249944
摘要： A method for fabricating a reinforced matrix composite comprising the step of providing a composite preform having a fibrous structure and applying matrix material onto the preform in locations along the preform. A barrier material is applied to at least a portion of the coated preform to direct the flow of matrix material into the preform. The composite preform is heated to a temperature sufficient to render the matrix material viscous and insufficient to cure the matrix material. The pressure to the interior of the composite preform is reduced, while the pressure to the barrier material is increased. The temperature is maintained to flow the matrix material into the composite preform and to force gases from the fibrous structure. The composite preform is then cured and cooled to form a reinforced matrix composite having a low void content and a substantially uniform matrix distribution.
摘要翻译：一种用于制造增强基质复合材料的方法，包括提供具有纤维结构的复合预成型件并将基体材料施加到预型件上的预型件沿着预制件的位置的步骤。将阻挡材料施加到涂覆预型件的至少一部分以将基体材料流引导到预成型件中。将复合预制件加热到足以使基质材料粘稠并且不足以固化基质材料的温度。对复合预制件内部的压力降低，同时对阻挡材料的压力增加。保持温度以使基质材料流入复合预制件并迫使来自纤维结构的气体。然后将复合预成型件固化并冷却以形成具有低空隙含量和基本均匀的基体分布的增强基质复合材料。

6. 发明授权

US07999060B2 Tailorable polyimide prepolymer blends, crosslinked polyimides, and articles formed therefrom 有权
标题翻译：可聚聚酰亚胺预聚物共混物，交联聚酰亚胺和由其形成的制品
公开(公告)号：US07999060B2
公开(公告)日：2011-08-16
申请号：US11928274
申请日：2007-10-30
申请人： Warren Ronk , Lisa Shafer
发明人： Warren Ronk , Lisa Shafer
IPC分类号： C08G73/00
CPC分类号： C08G73/10 , C08G73/101 , C08G73/1014 , C08G73/12 , C08L79/08 , C08L2205/02 , C08L2666/20
摘要： A tailorable polyimide prepolymer blend comprising an end group component, a dianhydride component, and a diamine component. The dianhydride component includes at least 3,4,3′,4′-benzophenonetetracarboxylic dianhydride (BTDA), derivatives thereof, or combinations thereof, and 3,4,3′,4′-biphenyltetracarboxylic dianhydride (BPDA), derivatives thereof, or combinations thereof. The diamine component includes at least 1,3-phenylenediamine (mPDA), derivatives thereof, or combinations thereof; 1,4-phenylenediamine (pPDA), derivatives thereof, or combinations thereof; bis amino phenoxy benzene (APB), derivatives thereof, and combinations thereof; and optionally, 4,4′-(1,3-phenylene-bis(1-methylethylidene)bisaniline (Bis-M), derivatives thereof, and combinations thereof. A cured polyimide matrix has a glass transition temperature of at least about 450° F. (232° C.). An article formed from the tailorable polyimide prepolymer blend may be a powder, a neat resin, a coating material, a film, an adhesive, a fiber, a composite, a laminate, a prepreg, a part, and combinations thereof.
摘要翻译：包含端基组分，二酐组分和二胺组分的可调节的聚酰亚胺预聚物共混物。二酐组分包括至少3,4,3'，4'-二苯甲酮四羧酸二酐（BTDA），其衍生物或其组合，和3,4,3'，4'-联苯四羧酸二酐（BPDA），其衍生物或其组合。二胺组分包括至少1,3-苯二胺（mPDA），其衍生物或其组合; 1,4-苯二胺（pPDA），其衍生物或其组合; 双氨基苯氧基苯（APB），其衍生物及其组合; 和任选的4,4' - （1,3-亚苯基 - 双（1-甲基亚乙基）双苯胺（Bis-M），其衍生物及其组合。固化的聚酰亚胺基质的玻璃化转变温度至少为约450° F.（232℃）由可调节聚酰亚胺预聚物共混物形成的制品可以是粉末，纯树脂，涂料，膜，粘合剂，纤维，复合材料，层压材料，预浸料，部分及其组合。

7. 发明申请

US20080108781A1 TAILORABLE POLYIMIDE PREPOLYMER BLENDS, CROSSLINKED POLYIMIDES, AND ARTICLES FORMED THEREFROM 有权
标题翻译：可固化的聚酰亚胺预聚物共混物，交联的聚酰亚胺和其形成的制品
公开(公告)号：US20080108781A1
公开(公告)日：2008-05-08
申请号：US11928274
申请日：2007-10-30
申请人： Warren Ronk , Lisa Shafer
发明人： Warren Ronk , Lisa Shafer
IPC分类号： C08G73/12
CPC分类号： C08G73/10 , C08G73/101 , C08G73/1014 , C08G73/12 , C08L79/08 , C08L2205/02 , C08L2666/20
摘要： A tailorable polyimide prepolymer blend comprising an end group component, a dianhydride component, and a diamine component. The dianhydride component includes at least 3,4,3′,4′-benzophenonetetracarboxylic dianhydride (BTDA), derivatives thereof, or combinations thereof, and 3,4,3′,4′-biphenyltetracarboxylic dianhydride (BPDA), derivatives thereof, or combinations thereof. The diamine component includes at least 1,3-phenylenediamine (mPDA), derivatives thereof, or combinations thereof, 1,4-phenylenediamine (pPDA), derivatives thereof, or combinations thereof, bis amino phenoxy benzene (APB), derivatives thereof, and combinations thereof, and optionally, 4,4′-(1,3-phenylene-bis(1-methylethylidene) bisaniline (Bis-M), derivatives thereof, and combinations thereof. A cured polyimide matrix has a glass transition temperature of at least about 450° F. (232° C.). An article formed from the tailorable polyimide prepolymer blend may be a powder, a neat resin, a coating material, a film, an adhesive, a fiber, a composite, a laminate, a prepreg, a part, and combinations thereof.
摘要翻译：包含端基组分，二酐组分和二胺组分的可调节的聚酰亚胺预聚物共混物。二酐组分包括至少3,4,3'，4'-二苯甲酮四羧酸二酐（BTDA），其衍生物或其组合，和3,4,3'，4'-联苯四羧酸二酐（BPDA），其衍生物或其组合。二胺组分包括至少1,3-苯二胺（mPDA），其衍生物或其组合，1,4-苯二胺（pPDA），其衍生物或其组合，双氨基苯氧基苯（APB），其衍生物和其组合，和任选的4,4' - （1,3-亚苯基 - 双（1-甲基亚乙基）双苯胺（Bis-M），其衍生物及其组合。固化的聚酰亚胺基体的玻璃化转变温度至少为由可调节的聚酰亚胺预聚物共混物形成的制品可以是粉末，纯树脂，涂料，膜，粘合剂，纤维，复合材料，层压材料，预浸料，部件及其组合。

8. 发明申请

US20080152853A1 COMPOSITE CONTAINMENT CASINGS FOR TURBINE ENGINE AND METHODS FOR FABRICATING THE SAME 审中-公开
标题翻译：用于涡轮发动机的复合容纳箱及其制造方法
公开(公告)号：US20080152853A1
公开(公告)日：2008-06-26
申请号：US11614439
申请日：2006-12-21
申请人： Lee Alan Blanton , Stephen Mark Whiteker , Matthew Bernard Buczek , Warren Ronk , Curt Brian Curtis , David Scott Miller
发明人： Lee Alan Blanton , Stephen Mark Whiteker , Matthew Bernard Buczek , Warren Ronk , Curt Brian Curtis , David Scott Miller
IPC分类号： B05D3/12 , B28B23/02
CPC分类号： B29C70/44 , Y10T428/1372
摘要： A method for fabricating a turbine engine composite containment casing is provided. The method comprising impregnating a plurality of fiber-reinforced layers with a resin to form a preform, heating the preform to a first temperature, applying a vacuum to the preform, varying an amount of pressure applied to the preform when the temperature reaches the first temperature, heating the preform from the first temperature to a second temperature at a first temperature rate, and heating the preform from the second temperature to a third temperature at a second temperature rate to facilitate curing of the preform.
摘要翻译：提供一种制造涡轮发动机复合容纳壳体的方法。所述方法包括用树脂浸渍多个纤维增强层以形成预制件，将预成型件加热到第一温度，向预成型件施加真空，当温度达到第一温度时改变施加到预成型件的压力量，以第一温度将预成型件从第一温度加热到第二温度，并以第二温度将预成型件从第二温度加热到第三温度，以便于预成型件的固化。

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