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    • 2. 发明授权
    • High-quality SGOI by annealing near the alloy melting point
    • 高品质SGOI通过在合金熔点附近退火
    • US07679141B2
    • 2010-03-16
    • US12027561
    • 2008-02-07
    • Stephen W. BedellHuajie ChenAnthony G. DomenicucciKeith E. FogelRichard J. MurphyDevendra K. Sadana
    • Stephen W. BedellHuajie ChenAnthony G. DomenicucciKeith E. FogelRichard J. MurphyDevendra K. Sadana
    • H01L31/392
    • H01L21/26506H01L21/324H01L21/7624H01L21/76254H01L29/1054
    • A method of forming a low-defect, substantially relaxed SiGe-on-insulator substrate material is provided. The method includes first forming a Ge-containing layer on a surface of a first single crystal Si layer which is present atop a barrier layer that is resistant to Ge diffusion. A heating step is then performed at a temperature that approaches the melting point of the final SiGe alloy and retards the formation of stacking fault defects while retaining Ge. The heating step permits interdiffusion of Ge throughout the first single crystal Si layer and the Ge-containing layer thereby forming a substantially relaxed, single crystal SiGe layer atop the barrier layer. Moreover, because the heating step is carried out at a temperature that approaches the melting point of the final SiGe alloy, defects that persist in the single crystal SiGe layer as a result of relaxation are efficiently annihilated therefrom. In one embodiment, the heating step includes an oxidation process that is performed at a temperature from about 1230° to about 1320° C. for a time period of less than about 2 hours. This embodiment provides SGOI substrate that have minimal surface pitting and reduced crosshatching.
    • 提供一种形成低缺陷,基本上松弛的绝缘体上硅衬底材料的方法。 该方法包括首先在耐Ge扩散的阻挡层上存在的第一单晶Si层的表面上形成含Ge层。 然后在接近最终SiGe合金的熔点的温度下进行加热步骤,并且在保留Ge的同时延缓层叠缺陷缺陷的形成。 加热步骤允许Ge遍及第一单晶Si层和含Ge层的相互扩散,从而在阻挡层顶部形成基本松弛的单晶SiGe层。 此外,由于加热步骤在接近最终SiGe合金的熔点的温度下进行,所以由于弛豫而在单晶SiGe层中持续存在的缺陷被有效地湮灭。 在一个实施方案中,加热步骤包括氧化过程,其在约1230℃至约1320℃的温度下进行约少于约2小时的时间。 该实施例提供具有最小表面点蚀和减少的交叉阴影的SGOI衬底。
    • 5. 发明授权
    • High-quality SGOI by annealing near the alloy melting point
    • 高品质SGOI通过在合金熔点附近退火
    • US07348253B2
    • 2008-03-25
    • US10855915
    • 2004-05-27
    • Stephen W. BedellHuajie ChenAnthony G. DomenicucciKeith E. FogelRichard J. MurphyDevendra K. Sadana
    • Stephen W. BedellHuajie ChenAnthony G. DomenicucciKeith E. FogelRichard J. MurphyDevendra K. Sadana
    • H01L21/84
    • H01L21/26506H01L21/324H01L21/7624H01L21/76254H01L29/1054
    • A method of forming a low-defect, substantially relaxed SiGe-on-insulator substrate material is provided. The method includes first forming a Ge-containing layer on a surface of a first single crystal Si layer which is present atop a barrier layer that is resistant to Ge diffusion. A heating step is then performed at a temperature that approaches the melting point of the final SiGe alloy and retards the formation of stacking fault defects while retaining Ge. The heating step permits interdiffusion of Ge throughout the first single crystal Si layer and the Ge-containing layer thereby forming a substantially relaxed, single crystal SiGe layer atop the barrier layer. Moreover, because the heating step is carried out at a temperature that approaches the melting point of the final SiGe alloy, defects that persist in the single crystal SiGe layer as a result of relaxation are efficiently annihilated therefrom. In one embodiment, the heating step includes an oxidation process that is performed at a temperature from about 1230° to about 1320° C. for a time period of less than about 2 hours. This embodiment provides SGOI substrate that have minimal surface pitting and reduced crosshatching.
    • 提供一种形成低缺陷,基本上松弛的绝缘体上硅衬底材料的方法。 该方法包括首先在耐Ge扩散的阻挡层上存在的第一单晶Si层的表面上形成含Ge层。 然后在接近最终SiGe合金的熔点的温度下进行加热步骤,并且在保留Ge的同时延缓层叠缺陷缺陷的形成。 加热步骤允许Ge遍及第一单晶Si层和含Ge层的相互扩散,从而在阻挡层顶部形成基本松弛的单晶SiGe层。 此外,由于加热步骤在接近最终SiGe合金的熔点的温度下进行,所以由于弛豫而在单晶SiGe层中持续存在的缺陷被有效地湮灭。 在一个实施方案中,加热步骤包括氧化过程,其在约1230℃至约1320℃的温度下进行约少于约2小时的时间。 该实施例提供具有最小表面点蚀和减少的交叉阴影的SGOI衬底。
    • 9. 发明授权
    • Electron microscope magnification standard providing precise calibration in the magnification range 5000X-2000,000X
    • 电子显微镜放大标准提供5000X-2000,000X倍率范围内的精确校准
    • US06875982B2
    • 2005-04-05
    • US10604989
    • 2003-08-29
    • Stephen W. BedellJohn BruleyAnthony G. DomenicucciDevendra K. Sadana
    • Stephen W. BedellJohn BruleyAnthony G. DomenicucciDevendra K. Sadana
    • G01N1/28G01N23/04H01J37/26
    • G01N23/04G01N2001/2893H01J37/261H01J2237/2826
    • A method and calibration standard for fabricating on a single substrate a series of crystalline pairs such that the d-spacing difference between the pairs will generate Moire fringes of the correct spacings to optimally calibrate the magnification settings of an electron microscope over a variety of magnification settings in the range of 5000× to 200,000×. The invention enables the tailoring of Moire fringe spacings to a desired magnification setting for calibration purposes by fabricating a series of patterns on a single substrate whereby each magnification setting is easily calibrated using a specific SGOI structure that is selected by a simple x-y translation across the top plan surface of the SGOI structure, therein eliminating the need for removing calibration samples in and out of the electron microscope. The method and calibration standard may be used for calibrating electron microscopes, such as, scanning transmission electron microscopes and transmission electron microscopes.
    • 一种用于在单个基板上制造一系列晶体对的方法和校准标准,使得对之间的d间距差会产生正确间隔的莫尔条纹,以便通过各种放大设置最佳地校准电子显微镜的放大倍率设置 在5000x到200,000x的范围内。 通过在单个基板上制造一系列图案,本发明可以通过在单个基板上制造一系列图案来将莫尔条纹间距定制到所需的放大倍率设置,从而可以使用特定的SGOI结构轻松校准每个放大倍数设置,该SGOI结构通过顶部的简单xy平移 SGOI结构的平面表面,其中不需要将校准样品移入和移出电子显微镜。 该方法和校准标准可用于校准电子显微镜,例如扫描透射电子显微镜和透射电子显微镜。