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1. 发明授权

US06509103B1 Method for coating reactors for high pressure polymerization of 1-olefins 失效
标题翻译：用于1-烯烃高压聚合反应器的涂布方法
公开(公告)号：US06509103B1
公开(公告)日：2003-01-21
申请号：US09869147
申请日：2001-06-26
申请人： Stephan Hüffer , Andreas Deckers , Wilhelm Weber , Roger Klimesch , Dieter Littmann , Jürgen Sturm , Götz Lerch
发明人： Stephan Hüffer , Andreas Deckers , Wilhelm Weber , Roger Klimesch , Dieter Littmann , Jürgen Sturm , Götz Lerch
IPC分类号： B05D722
CPC分类号： F28F19/02 , C23C18/1616 , C23C18/1662 , C23C18/36 , Y10T428/12556 , Y10T428/12944 , Y10T428/31678
摘要： A process for coating a reactor, which comprises depositing a metal layer or a metal/polymer dispersion layer on the internal surface of the reactor in an electroless manner by bringing the surfaces into contact with a metal electrolyte solution which, besides the metal electrolyte, comprises a reducing agent and optionally a halogenated polymer to be deposited in dispersed form.
摘要翻译：一种用于涂覆反应器的方法，其包括通过使金属电解质溶液与金属电解质溶液接触而以化学方式沉积在反应器内表面上的金属层或金属/聚合物分散层还原剂和任选的以分散形式沉积的卤化聚合物。

2. 发明授权

US5739242A Preparation of copolymers of ethylene with alkenecarboxylic acids 失效
标题翻译：乙烯与烯烃羧酸的共聚物的制备
公开(公告)号：US5739242A
公开(公告)日：1998-04-14
申请号：US544442
申请日：1995-11-17
申请人： Andreas Deckers , Dieter Littmann , Roger Klimesch
发明人： Andreas Deckers , Dieter Littmann , Roger Klimesch
IPC分类号： C08F210/02 , C08F220/04
CPC分类号： C08F210/02
摘要： A process for the preparation of copolymers of ethylene and dicarboxylic acid in the presence of a free-radical inhibitor. The process comprises of warming a mixture of ethylene and C.sub.3 -C.sub.6 -alkenecarboxylic acid to a temperature of from 60.degree. to 100.degree. C. before addition of the free-radical inhibitor. The maximum polymerization temperature to recover said copolymers of ethylene is in the range of from 100.degree. to 260.degree. C.; and wherein said copolymer comprises from 94 to 99.5 mol % of ethylene and from 0.5 to 6.0 mol % of C.sub.3 -C.sub.6 -alkenecarboxylic acid.
摘要翻译：一种在自由基抑制剂存在下制备乙烯和二羧酸的共聚物的方法。该方法包括在加入自由基抑制剂之前将乙烯和C 3 -C 6 - 链烯羧酸的混合物加热到60℃至100℃的温度。回收所述乙烯共聚物的最大聚合温度在100至260℃的范围内。并且其中所述共聚物包含94-99.5mol％的乙烯和0.5-6.0mol％的C 3 -C 6 - 烯烃羧酸。

3. 发明授权

US06844408B2 Preparation of polyethylene 有权
标题翻译：聚乙烯的制备
公开(公告)号：US06844408B2
公开(公告)日：2005-01-18
申请号：US10221202
申请日：2001-03-13
申请人： Andrei Gonioukh , Lars Wittkowski , Thomas Dröge , Ernst Fischer , Roger Klimesch , Philipp Rosendorfer , Gernot Köhler , Dieter Littmann
发明人： Andrei Gonioukh , Lars Wittkowski , Thomas Dröge , Ernst Fischer , Roger Klimesch , Philipp Rosendorfer , Gernot Köhler , Dieter Littmann
IPC分类号： C08F4/38 , C08F10/00 , C08F10/02 , C08F110/02
CPC分类号： C08F10/02 , C08F110/02 , C08F4/38 , C08F4/36 , C08F2/00 , C08F2500/12 , C08F2500/26
摘要： Ethylene homopolymers and copolymers are prepared in a tube reactor at from 160° C. to 350° C. and pressures in the range from 500 to 5000 bar, with or without use of molar mass regulators, using a peroxide mixture comprising from 1 to 95 mol %, based on the total amount of the peroxide mixture, of at least one cyclic peroxide of the formula I, where the radicals R are identical or different and are selected from among alkyl groups and aryl groups, as polymerization initiator.
摘要翻译：乙烯均聚物和共聚物在管式反应器中在160℃至350℃下制备，压力范围为500至5000巴，使用或不使用摩尔质量调节剂，使用包含1至95的过氧化物混合物摩尔％，基于过氧化物混合物的总量，至少一种式I的环状过氧化物，其中基团R相同或不同，并且选自烷基和芳基，作为聚合引发剂。

4. 发明授权

US5684108A Ethylene-based copolymers and their use as flow improvers in mineral oil middle distillates 失效
标题翻译：乙烯基共聚物及其在矿物油中间馏分中作为流动改进剂的用途
公开(公告)号：US5684108A
公开(公告)日：1997-11-04
申请号：US615175
申请日：1996-04-02
申请人： Hans-Joachim Muller , Bernd Wenderoth , Albin Berger , Dieter Littmann , Roger Klimesch , Knut Oppenlander , Bernd Lothar Marczinke , Thomas Ruhl , Marc Heider
发明人： Hans-Joachim Muller , Bernd Wenderoth , Albin Berger , Dieter Littmann , Roger Klimesch , Knut Oppenlander , Bernd Lothar Marczinke , Thomas Ruhl , Marc Heider
IPC分类号： C08F10/00 , C08F210/02 , C10L1/22 , C10L1/236 , C10L10/14 , C08F226/02 , C08F218/04 , C10L1/18
CPC分类号： C10L1/2366 , C08F210/02 , C10L1/2368
摘要： An ethylene-based copolymer which is suitable as a flow improver for mineral oil middle distillates and is composed of a) from 50 to 94% by weight of ethylene; b) from 3 to 30% by weight of one or more vinyl esters of C.sub.2 -C.sub.6 -monocarboxylic acids; c) from 3 to 20% by weight of one or more aminoalkyl acrylates of the formula I ##STR1## which R.sup.1 is hydrogen or methyl, R.sup.2 and R.sup.3 are identical or different and are each hydrogen or C.sub.1 -C.sub.6 -alkyl and A.sup.1 is straight-chain or branched C.sub.2 -C.sub.10 -alkylene; and d) from 0 to 10% by weight of one or more monomers which are copolymerizable with the monomers a) to c), wherein copolymers containing vinyl acetate as monomer b) and having a number average molecular weight of from 5,000 to 50,000 are excluded from the scope of the copolymer.
摘要翻译： PCT No.PCT / EP94 / 03179 Sec。 371日期：1996年4月2日 102（e）日期1996年4月2日PCT 1994年9月23日PCT公布。第WO95 / 09877号公报日期1995年04月13日一种适用于矿物油中间馏分的流动改进剂的乙烯基共聚物，由以下组成：a）50-94重量％的乙烯; b）3至30重量％的一种或多种C2-C6-一元羧酸的乙烯基酯; c）3至20重量％的一种或多种式I（I）的氨基烷基丙烯酸酯，其中R 1是氢或甲基，R 2和R 3是相同或不同的并且各自是氢或C 1 -C 6烷基， A1是直链或支链C 2 -C 10 - 亚烷基; 和d）0至10重量％的可与单体a）至c）共聚的一种或多种单体，其中包含乙酸乙烯酯作为单体b）并且数均分子量为5,000至50,000的共聚物被排除从共聚物的范围。

5. 发明授权

US5747616A Ethylene-based copolymers and their use as flow improvers in mineral oil middle distillates 失效
标题翻译：乙烯基共聚物及其在矿物油中间馏分中作为流动改进剂的用途
公开(公告)号：US5747616A
公开(公告)日：1998-05-05
申请号：US869971
申请日：1997-06-05
申请人： Hans-Joachim Muller , Bernd Wenderoth , Albin Berger , Dieter Littmann , Roger Klimesch , Knut Oppenlander , Bernd Lothar Marczinke , Thomas Ruhl , Marc Heider
发明人： Hans-Joachim Muller , Bernd Wenderoth , Albin Berger , Dieter Littmann , Roger Klimesch , Knut Oppenlander , Bernd Lothar Marczinke , Thomas Ruhl , Marc Heider
IPC分类号： C08F10/00 , C08F210/02 , C10L1/22 , C10L1/236 , C10L10/14 , C08F222/40 , C08F216/18
CPC分类号： C10L1/2366 , C08F210/02 , C10L1/2368
摘要： Ethylene-based copolymers which are suitable as flow improvers for mineral oil middle distillates are composed of a) from 50 to 94% by weight of ethylene, b) from 3 to 30% by weight of one or more vinyl esters of C.sub.2 -C.sub.6 -monocarboxylic acids, c) from 3 to 20% by weight of one or more aminoalkyl acrylates of the general formula I ##STR1## where R.sup.1 is hydrogen or methyl, R.sup.2 and R.sup.3 may be identical or different and are each hydrogen or C.sub.1 -C.sub.6 -alkyl and A.sup.1 is straight-chain or branched C.sub.2 -C.sub.10 -alkylene, and d) from 0 to 10% by weight of one or more monomers which are copolymerizable with the monomers a) to c), copolymers in which monomer b) is vinyl acetate and which have a number average molecular weight of from 5000 to 50,000 being excluded, or are composed of a') from 50 to 95.5% by weight of ethylene, b') from 4 to 30% by weight of one or more vinyl esters of C.sub.2 -C.sub.6 -monocarboxylic acids, c') from 0.5 to 20% by weight of one or more vinylimidazoles of the general formula II ##STR2## where R.sup.4, R.sup.5 and R.sup.6 may be identical or different and are each hydrogen or C.sub.1 -C.sub.6 -alkyl, or from 0.5 to 20% by weight of one or more aminoalkyl vinyl ethers of the general formula III R.sup.7 R.sup.8 N--A.sup.2 --O--CR.sup.9 .dbd.CR.sup.10 R.sup.11(III) where R.sup.7 and R.sup.8 are each C.sub.1 -C.sub.6 -alkyl, R.sup.9, R.sup.10 and R.sup.11 are each hydrogen or C.sub.1 -C.sub.6 -alkyl and A.sup.2 is C.sub.2 -C.sub.6 -alkylene, and d') from 0 to 10% by weight of one or more monomers which are copolymerizable with the monomers a') to c').
摘要翻译：适用于矿物油中间馏分的流动改进剂的乙烯基共聚物由以下组成：a）50-94重量％的乙烯，b）3-30重量％的一种或多种C2-C6- 一元羧酸，c）3至20重量％的一种或多种通式I（I）的氨基烷基丙烯酸酯，其中R 1是氢或甲基，R 2和R 3可以相同或不同，各自为氢或C1 -C6-烷基和A1是直链或支链C 2 -C 10 - 亚烷基，和d）0至10重量％的可与单体a）至c）共聚的一种或多种单体，其中单体b ）为乙酸乙烯酯，其数均分子量为5000〜50,000，或者由以下组成：a）50〜95.5重量％的乙烯，b'），4〜30重量％的一种或多种更多的C2-C6-一元羧酸的乙烯基酯，c'）0.5至20重量％的一种或多种通式II的乙烯基咪唑（II）w 这里R 4，R 5和R 6可以相同或不同，各自为氢或C 1 -C 6烷基，或0.5至20重量％的一种或多种通式IIIR7R8N-A2-O-CR9 = CR10R11的氨基烷基乙烯基醚（III）其中R 7和R 8各自为C 1 -C 6烷基，R 9，R 10和R 11各自为氢或C 1 -C 6烷基，且A 2为C 2 -C 6亚烷基，d'）为0至10重量％一种或多种可与单体a'）至c'）共聚的单体。

6. 发明授权

US06562915B2 Method for carrying out radical ethylene high-pressure polymerization while preventing undesired polymer deposits 有权
标题翻译：进行自由基乙烯高压聚合同时防止不期望的聚合物沉积物的方法
公开(公告)号：US06562915B2
公开(公告)日：2003-05-13
申请号：US10182563
申请日：2002-07-31
申请人： Frank-Olaf Mähling , Andreas Deckers , Dieter Littmann , Heinz Friedrich Sutoris , Kaspar Evertz
发明人： Frank-Olaf Mähling , Andreas Deckers , Dieter Littmann , Heinz Friedrich Sutoris , Kaspar Evertz
IPC分类号： C08F240
CPC分类号： C08F297/08 , C08F110/02 , C08F2/40 , C08F2/00 , C08F4/34 , C08F2/005 , C08F2500/26
摘要： In a process for the polymerization or copolymerization of ethylenically unsaturated monomers in the presence of polymerization initiators which decompose to form free radicals in a continuously operated polymerization apparatus comprising a fresh gas feed line, a precompressor, a postcompressor, a reactor, a pressure maintenance valve, a high-pressure circuit having a high-pressure product separator and a high-pressure circulation gas return line, a product valve and a low-pressure circuit having a low-pressure product separator and a low-pressure circulation gas return line, nitrogen monoxide or oxygen is introduced as inhibitor into the high-pressure circuit, into the low-pressure circuit and/or the precompressor.
摘要翻译：在用于在连续操作的聚合装置中分解形成自由基的聚合引发剂存在下烯键式不饱和单体的聚合或共聚的方法中，所述聚合引发剂包括新鲜气体进料管线，预压缩机，后压缩机，反应器，压力维持阀具有高压产品分离器和高压循环气体返回管路的高压回路，具有低压产品分离器和低压循环气体返回管路的产品阀和低压回路，氮气将一氧化碳或氧气作为抑制剂引入高压回路中，进入低压回路和/或预压缩机。

7. 发明授权

US08273835B2 Method for ethylene polymerization in a tubular reactor with reduced output 有权
标题翻译：在具有降低的产量的管式反应器中进行乙烯聚合的方法
公开(公告)号：US08273835B2
公开(公告)日：2012-09-25
申请号：US13144355
申请日：2010-01-14
申请人： Dieter Littmann , Andre-Armand Finette , Hans Joachim Meinke
发明人： Dieter Littmann , Andre-Armand Finette , Hans Joachim Meinke
IPC分类号： C08F2/00 , C08F10/02 , B01J19/24
CPC分类号： B01J19/2415 , B01J4/008 , C08F10/02 , C08F2/38 , C08F4/38 , C08F2/00
摘要： Process for the preparation of ethylene homopolymers or copolymers in the presence of free-radical polymerization initiators at from 100° C. to 350° C. and pressures in the range of from 160 MPa to 350 MPa in a tubular reactor with at least two spatially separated initiator injection points, wherein injecting initiator rises the temperature of the reaction mixture in the reaction zone following the injection point, and the first initiator injection point of the tubular reactor is not provided with initiator or is provided with so little initiator that the temperature of the reaction mixture does not rise more than 20° C. in the first reaction zone and method for reducing the output of a high pressure tubular reactor for the homo- or copolymerization of ethylene in the presence of free-radical polymerization initiators with at least two initiator injection points, wherein feeding of free-radical polymerization initiator to the first initiator injection point is discontinued or reduced to a level that the temperature of the reaction mixture in the first reaction zone does not rise more than 20° C.
摘要翻译：在自由基聚合引发剂存在下，在100℃至350℃下制备乙烯均聚物或共聚物的方法，并且在具有至少两个空间位置的管式反应器中在160MPa至350MPa范围内的压力分离的引发剂注入点，其中注射引发剂在注射点之后升高反应区域中的反应混合物的温度，并且管式反应器的第一引发剂注入点不具有引发剂，或者设置有少量引发剂，反应混合物在第一反应区域中不会升高超过20℃，并且在自由基聚合引发剂存在下，降低高压管式反应器用于乙烯均聚或共聚的产物的方法与至少两种引发剂注入点，其中自由基聚合引发剂向第一引发剂注入点的进料停止或减少 d达到第一反应区中的反应混合物的温度不升高超过20℃的水平。

8. 发明授权

US4925769A Light-sensitive photopolymerizable laminate material 失效
标题翻译：光敏光聚合层压材料
公开(公告)号：US4925769A
公开(公告)日：1990-05-15
申请号：US324709
申请日：1989-03-17
申请人： Wolfgang Huemmer , Bernd Bronstert , Dieter Littmann , Manfred Zuerger
发明人： Wolfgang Huemmer , Bernd Bronstert , Dieter Littmann , Manfred Zuerger
IPC分类号： G03F7/027 , C08F2/50 , G03F7/00 , G03F7/095 , G03F7/11
CPC分类号： G03F7/0955 , G03F7/11
摘要： Photopolymerizable laminates suitable for producing printing plates have on a dimensionally stable base at least one intermediate layer and on top thereof a photopolymerizable relief-forming layer, the intermediate layer containing aryl glycidyl (meth)acrylate in an at least partially polymerized state.
摘要翻译：适用于生产印版的可光聚合层压板在至少一个中间层的尺寸稳定的基底上，在其顶部上具有至少部分聚合的状态的中间层（甲基）丙烯酸芳基缩水甘油酯。

9. 发明授权

US4960673A Photopolymerizable laminate suitable for producing printing plates 失效
标题翻译：适用于生产印版的可光聚合层压板
公开(公告)号：US4960673A
公开(公告)日：1990-10-02
申请号：US324829
申请日：1989-03-17
申请人： Erich Beck , Bernd Bronstert , Wolfgang Huemmer , Dieter Littmann
发明人： Erich Beck , Bernd Bronstert , Wolfgang Huemmer , Dieter Littmann
IPC分类号： C08F2/50 , G03F7/00 , G03F7/027 , G03F7/033 , G03F7/095 , G03F7/11
CPC分类号： G03F7/11 , G03F7/027 , G03F7/0955 , Y10S430/106 , Y10S430/109 , Y10S430/11
摘要： Photopolymerizable laminates suitable for producing flexible and resilient printing plates carry on a dimensionally stable base at least one intermediate layer and on top thereof a photopolymerizable layer which consists essentially of a mixture of a water-soluble copolymer or derivative of polyvinyl alcohol, a specific copolymerizable mono-functional (meth)acrylate, a photoinitiator and a thermal polymerization inhibitor.
摘要翻译：适用于生产柔性和弹性印版的可光聚合层压板在至少一个中间层上承载尺寸稳定的基底，并且在其顶部上可光聚合层，其基本上由水溶性共聚物或聚乙烯醇衍生物，特定的可共聚单体官能（甲基）丙烯酸酯，光引发剂和热聚合抑制剂。

10. 发明授权

US09238700B2 Process for the preparation of ethylene copolymers in the presence of free-radical polymerization initiator by copolymerizing ethylene, a bi- or multifunctional comonomer and optionally further comonomers 有权
标题翻译：在自由基聚合引发剂存在下通过共聚乙烯，双或多官能共聚单体和任选的其它共聚单体制备乙烯共聚物的方法
公开(公告)号：US09238700B2
公开(公告)日：2016-01-19
申请号：US13996415
申请日：2011-12-19
申请人： Dieter Littmann , Dieter Lilge , Barbara Gall , Iakovos Vittorias , Gerd Mannebach , Markus Busch , Thomas Herrmann
发明人： Dieter Littmann , Dieter Lilge , Barbara Gall , Iakovos Vittorias , Gerd Mannebach , Markus Busch , Thomas Herrmann
IPC分类号： B05D3/02 , C08F210/02 , C08F2/38
CPC分类号： C08F210/02 , C08F2/38 , C08F2/00 , C08F220/28
摘要： Process for preparing ethylene copolymers in the presence of free-radical polymerization initiator at pressures in the range of from 160 MPa to 350 MPa and temperatures in the range of from 100° C. to 350° C. in a tubular reactor by copolymerizing ethylene, a bi- or multifunctional comonomer and optionally further comonomers, wherein the bi- or multifunctional comonomer bears at least two different functional groups, of which at least one is a unsaturated group, which can be incorporated into the growing polymer chain, and at least another functional group can act as chain transfer agent in radical ethylene polymerization, ethylene copolymers obtainable by such a process, the use of the ethylene copolymers for extrusion coating and a process for extrusion coating a substrate selected from the group consisting of paper, paperboard, polymeric film, and metal, with such ethylene copolymers.
摘要翻译：在自由基聚合引发剂存在下，在160MPa至350MPa的压力范围内制备乙烯共聚物的方法，在管式反应器中通过共聚乙烯制备温度在100℃至350℃的方法，双功能或多功能共聚单体和任选的其它共聚单体，其中双官能或多功能共聚单体具有至少两个不同的官能团，其中至少一个是不饱和基团，其可以并入生长的聚合物链中，并且至少另一个官能团可以作为自由基乙烯聚合中的链转移剂，可通过这种方法获得的乙烯共聚物，使用乙烯共聚物进行挤出涂布，以及用于挤出涂布选自纸，纸板，聚合物膜，和金属，与这种乙烯共聚物。

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