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1. 发明授权

US09233849B2 Process for producing fluorine-containing sulfonylimide salt 有权
标题翻译：含氟磺酰亚胺盐的制备方法
公开(公告)号：US09233849B2
公开(公告)日：2016-01-12
申请号：US13985915
申请日：2012-02-28
申请人： Shiro Tsubokura , Toru Suzuki , Michiaki Maruyama , Yasuyuki Aiura
发明人： Shiro Tsubokura , Toru Suzuki , Michiaki Maruyama , Yasuyuki Aiura
IPC分类号： C07C303/40 , C01B21/087 , C01B21/093 , C01B21/086
CPC分类号： C01B21/086 , C01B21/087 , C01B21/093 , C07C303/40 , C07C311/48
摘要： By reacting a fluorine-containing sulfonylimide ammonium salt such as ammonium N,N-di(fluorosulfonyl)imide with an alkali metal hydroxide such as lithium hydroxide, potassium hydroxide or sodium hydroxide under reduced pressure and at a low temperature of approximately 40° C., a fluorine-containing sulfonylimide alkali metal salt such as lithium N,N-di(fluorosulfonyl)imide, potassium N,N-di(fluorosulfonyl)imide or sodium N,N-di(fluorosulfonyl)imide is obtained.
摘要翻译：使N，N-二（氟磺酰基）酰亚胺铵等含氟磺酰亚胺铵盐与碱金属氢氧化物如氢氧化锂，氢氧化钾或氢氧化钠在减压下和约40℃的低温下反应。得到N，N-二（氟磺酰基）酰亚胺锂，N，N-二（氟磺酰基）酰亚胺钾，N，N-二（氟磺酰基）酰亚胺钠等含氟磺酰亚胺碱金属盐。

2. 发明授权

US09096502B2 Production process for fluorosulfonylimide ammonium salt 有权
标题翻译：氟磺酰亚胺铵盐的生产工艺
公开(公告)号：US09096502B2
公开(公告)日：2015-08-04
申请号：US14001547
申请日：2012-02-24
申请人： Shiro Tsubokura , Yasuyuki Aiura , Toru Suzuki , Michiaki Maruyama
发明人： Shiro Tsubokura , Yasuyuki Aiura , Toru Suzuki , Michiaki Maruyama
IPC分类号： C07C311/48 , C07C303/40 , C01B21/093 , H01M10/052 , H01M10/0568 , C01B21/092
CPC分类号： C07C311/48 , C01B21/0923 , C01B21/093 , C07C303/40 , H01M10/052 , H01M10/0568 , Y02E60/122 , Y02P70/54
摘要： A compound [II] such as ammonium N,N-di(fluorosulfonyl)imide is obtained by reacting a compound [I] such as N,N-di(chlorosulfonyl)imide and NH4F (HF)p. A compound [IV] such as an N,N-di(fluorosulfonyl)imide alkali metal salt is obtained by reacting the obtained compound [II] and an alkali metal compound or the like.
摘要翻译：通过使诸如N，N-二（氯磺酰基）酰亚胺和NH 4 F（HF）p的化合物[I]与N，N-二（氟磺酰基）酰亚胺铵形成化合物[II]。通过使所得化合物[II]与碱金属化合物等反应，得到N，N-二（氟磺酰基）酰亚胺碱金属盐等化合物[Ⅳ]。

3. 发明申请

US20130331609A1 PRODUCTION PROCESS FOR FLUOROSULFONYLIMIDE AMMONIUM SALT 有权
标题翻译：氟磺酰胺铵盐的生产工艺
公开(公告)号：US20130331609A1
公开(公告)日：2013-12-12
申请号：US14001547
申请日：2012-02-24
申请人： Shiro Tsubokura , Yasuyuki Aiura , Toru Suzuki , Michiaki Maruyama
发明人： Shiro Tsubokura , Yasuyuki Aiura , Toru Suzuki , Michiaki Maruyama
IPC分类号： C07C311/48
CPC分类号： C07C311/48 , C01B21/0923 , C01B21/093 , C07C303/40 , H01M10/052 , H01M10/0568 , Y02E60/122 , Y02P70/54
摘要： A compound [II] such as ammonium N,N-di(fluorosulfonyl)imide is obtained by reacting a compound [I] such as N,N-di(chlorosulfonyl)imide and NH4F (HF)p. A compound [IV] such as an N,N-di(fluorosulfonyl)imide alkali metal salt is obtained by reacting the obtained compound [II] and an alkali metal compound or the like.
摘要翻译：通过使诸如N，N-二（氯磺酰基）酰亚胺和NH 4 F（HF）p的化合物[I]与N，N-二（氟磺酰基）酰亚胺铵形成化合物[II]。通过使所得化合物[II]与碱金属化合物等反应，得到N，N-二（氟磺酰基）酰亚胺碱金属盐等化合物[Ⅳ]。

4. 发明申请

US20130323155A1 PROCESS FOR PRODUCING FLUORINE-CONTAINING SULFONYLIMIDE SALT 有权
标题翻译：生产含氟化物磺酰亚胺盐的方法
公开(公告)号：US20130323155A1
公开(公告)日：2013-12-05
申请号：US13985915
申请日：2012-02-28
申请人： Shiro Tsubokura , Toru Suzuki , Michiaki Maruyama , Yasuyuki Aiura
发明人： Shiro Tsubokura , Toru Suzuki , Michiaki Maruyama , Yasuyuki Aiura
IPC分类号： C01B21/086
CPC分类号： C01B21/086 , C01B21/087 , C01B21/093 , C07C303/40 , C07C311/48
摘要： By reacting a fluorine-containing sulfonylimide ammonium salt such as ammonium N,N-di(fluorosulfonyl)imide with an alkali metal hydroxide such as lithium hydroxide, potassium hydroxide or sodium hydroxide under reduced pressure and at a low temperature of approximately 40° C., a fluorine-containing sulfonylimide alkali metal salt such as lithium N,N-di(fluorosulfonyl)imide, potassium N,N-di(fluorosulfonyl)imide or sodium N,N-di(fluorosulfonyl)imide is obtained.
摘要翻译：使N，N-二（氟磺酰基）酰亚胺铵等含氟磺酰亚胺铵盐与碱金属氢氧化物如氢氧化锂，氢氧化钾或氢氧化钠在减压下和约40℃的低温下反应。得到N，N-二（氟磺酰基）酰亚胺锂，N，N-二（氟磺酰基）酰亚胺钾，N，N-二（氟磺酰基）酰亚胺钠等含氟磺酰亚胺碱金属盐。

5. 发明申请

US20130323154A1 PROCESS FOR PRODUCTION OF FLUOROSULFONYLIMIDE AMMONIUM SALT 有权
标题翻译：生产氟磺酰胺铵盐的方法
公开(公告)号：US20130323154A1
公开(公告)日：2013-12-05
申请号：US13984069
申请日：2012-01-30
申请人： Shiro Tsubokura , Michiaki Maruyama
发明人： Shiro Tsubokura , Michiaki Maruyama
IPC分类号： C01B21/086 , C07C209/00
CPC分类号： C01B21/086 , C01B21/092 , C01B21/093 , C07C209/00 , C07C303/40 , H01M8/1048 , H01M10/0568 , Y02P70/56 , C07C311/48
摘要： A compound [I] such as ammonium N-(chlorosulfonyl)-N-(fluorosulfonyl)imide is reacted with hydrogen fluoride to obtain a compound [II] such as ammonium N,N-di(fluorosulfonyl)imide. The obtained compound [II] is reacted with an alkali metal compound or the like to obtain a compound [IV] such as an N,N-di(fluorosulfonyl)imide alkali metal salt.
摘要翻译：将化合物[I]如N-（氯磺酰基）-N-（氟磺酰基）酰亚胺铵与氟化氢反应，得到N，N-二（氟磺酰基）酰亚胺铵盐等化合物[II]。将所得化合物[II]与碱金属化合物等反应，得到N，N-二（氟磺酰基）酰亚胺碱金属盐等化合物[Ⅳ]。

6. 发明授权

US09242862B2 Process for production of fluorosulfonylimide ammonium salt 有权
标题翻译：氟磺酰亚胺铵盐的制备方法
公开(公告)号：US09242862B2
公开(公告)日：2016-01-26
申请号：US13984069
申请日：2012-01-30
申请人： Shiro Tsubokura , Michiaki Maruyama
发明人： Shiro Tsubokura , Michiaki Maruyama
IPC分类号： C01B21/086 , C07C209/00 , C01B21/092 , C01B21/093 , C07C303/40 , H01M8/10 , H01M10/0568
CPC分类号： C01B21/086 , C01B21/092 , C01B21/093 , C07C209/00 , C07C303/40 , H01M8/1048 , H01M10/0568 , Y02P70/56 , C07C311/48
摘要： A compound [I] such as ammonium N-(chlorosulfonyl)-N-(fluorosulfonyl)imide is reacted with hydrogen fluoride to obtain a compound [II] such as ammonium N,N-di(fluorosulfonyl)imide. The obtained compound [II] is reacted with an alkali metal compound or the like to obtain a compound [IV] such as an N,N-di(fluorosulfonyl)imide alkali metal salt.
摘要翻译：将化合物[I]如N-（氯磺酰基）-N-（氟磺酰基）酰亚胺铵与氟化氢反应，得到N，N-二（氟磺酰基）酰亚胺铵盐等化合物[II]。将所得化合物[II]与碱金属化合物等反应，得到N，N-二（氟磺酰基）酰亚胺碱金属盐等化合物[Ⅳ]。

7. 发明申请

US20090275753A1 ORTHO-SUBSTITUTED ANILINE DERIVATIVE AND ANTIOXIDANT DRUG 审中-公开
标题翻译： ORTHO替代苯胺衍生物和抗氧化剂药物
公开(公告)号：US20090275753A1
公开(公告)日：2009-11-05
申请号：US12092294
申请日：2006-11-06
申请人： Shiro Tsubokura , Nobuhiro Umeda , Seiichi Uchida
发明人： Shiro Tsubokura , Nobuhiro Umeda , Seiichi Uchida
IPC分类号： C07D405/14 , C07D307/87 , C07D405/12
CPC分类号： C07D307/79 , C07D405/06 , C07D405/12 , C07D405/14 , C07D413/12 , C07D417/12 , C07D471/08
摘要： A compound represented by formula (1) or a salt thereof, and an antioxidant drug containing the compound or the salt as an active ingredient, are provided. The compound or salt exhibits effective antioxidant activity in treating ischemic organ disorders and diseases caused by oxidative cell damage, and in inhibiting retinal lesions caused by oxidation due to the effects of light. In formula (1): a represents either 1 or 2, R0 represents an unsubstituted or substituted amino group, R1 to R4 each represent, independently, a hydrogen atom or an alkyl group, E represents an unsubstituted or substituted alkylene chain, D represents a single bond, oxygen atom, unsubstituted or substituted nitrogen atom, sulfur atom, sulfinyl group, sulfonyl group, carbonyl group, carbonylamino group or aminocarbonyl group, and A represents an unsubstituted or substituted aromatic hydrocarbon group, unsubstituted or substituted heterocyclic group, unsubstituted or substituted aralkyl group, or unsubstituted or substituted heteroaralkyl group.
摘要翻译：提供由式（1）表示的化合物或其盐，以及含有该化合物或其盐作为活性成分的抗氧化剂。化合物或盐在治疗缺血性器官障碍和由氧化性细胞损伤引起的疾病中以及由于光的影响而抑制氧化引起的视网膜损伤中表现出有效的抗氧化活性。在式（1）中：a表示1或2，R 0表示未取代或取代的氨基，R 1至R 4各自独立地表示氢原子或烷基，E表示未取代或取代的亚烷基链，D表示单键，氧原子，未取代或取代的氮原子，硫原子，亚磺酰基，磺酰基，羰基，羰基氨基或氨基羰基，A表示未取代或取代的芳族烃基，未取代或取代的杂环基，未取代或取代的芳烷基或未取代或取代的杂芳烷基。

8. 发明申请

US20060247228A1 Phenylazole compounds production process and antioxidants 失效
标题翻译：苯唑化合物生产工艺及抗氧化剂
公开(公告)号：US20060247228A1
公开(公告)日：2006-11-02
申请号：US10566820
申请日：2004-07-30
申请人： Nobuhiro Umeda , Nobuo Mochizuki , Seiichi Uchida , Mitsumasa Takada , Shiro Tsubokura , Yasuyuki Shiinoki , Fumie Shirato , Hiroko Moroe
发明人： Nobuhiro Umeda , Nobuo Mochizuki , Seiichi Uchida , Mitsumasa Takada , Shiro Tsubokura , Yasuyuki Shiinoki , Fumie Shirato , Hiroko Moroe
IPC分类号： A61K31/551 , A61K31/496 , A61K31/4745 , A61K31/454 , C07D471/02 , C07D403/02
CPC分类号： C07D471/04 , C07D405/12 , C07D405/14
摘要： The present invention is directed to compounds represented by the formula (1): B-D-Z (1) [wherein B represent the following formula (B-1), (B-2) or (B-3); A represents an optionally substituted imidazole or pyrazole group; E represents the following formula (1a): X represents an oxygen atom, the formula: SOu, or the formula: N—R9; Y represents a carbon atom or a nitrogen atom; D represents an oxygen atom, a sulfur atom or the formula (1a); Z represents (a chroman-2-yl group, a chroman-4-yl group, a 2,3-dihydrobenzofuran-2-yl group, a 2,3-dihydrobenzofuran-3-yl group, etc.) which is substituted with NHR10 or OR11)] or pharmaceutically acceptable salts thereof, and to antioxidants, therapeutic agents for kidney diseases or cerebrovascular disorder, and retinal oxidative damage inhibitors, which include the compounds as the active ingredient.
摘要翻译：本发明涉及由式（1）表示的化合物：<？in-line-formula description =“In-line formula”end =“lead”？> BDZ（1）<？in-line-formula description = “其中，B表示下述式（B-1），（B-2）或（B-3）表示的化合物。 A表示任选取代的咪唑或吡唑基; E表示下式（1a）：X表示氧原子，式：SOu，或下式：N-R 9; Y表示碳原子或氮原子; D表示氧原子，硫原子或式（1a）; Z表示（苯并二氢吡喃-2-基，苯并二氢吡喃-4-基，2,3-二氢苯并呋喃-2-基，2,3-二氢苯并呋喃-3-基等），其被 NHR 10或OR 11）]或其药学上可接受的盐，以及抗氧化剂，肾脏疾病或脑血管障碍的治疗剂和视网膜氧化损伤抑制剂，其包括化合物作为活性成分。

9. 发明授权

US08841458B2 Compound containing pyridine ring and method for producing halogenated picoline derivative and tetrazolyloxime derivative 有权
标题翻译：含有吡啶环的化合物及卤代甲基吡啶衍生物和四唑基肟衍生物的制备方法
公开(公告)号：US08841458B2
公开(公告)日：2014-09-23
申请号：US13583733
申请日：2011-03-11
申请人： Hidekazu Miyazaki , Satoru Yanaka , Shiro Tsubokura , Tadashi Sugiura , Kaoru Noda , Kengo Suzuki
发明人： Hidekazu Miyazaki , Satoru Yanaka , Shiro Tsubokura , Tadashi Sugiura , Kaoru Noda , Kengo Suzuki
IPC分类号： C07D213/75 , C07D401/12 , C07D405/12
CPC分类号： C07D213/75 , C07D401/12 , C07D405/12
摘要： Disclosed is a compound containing a pyridine ring that can be synthesized in an industrially advantageous manner, and is useful as an intermediate for producing tetrazolyloxime derivatives that exhibit fungicidal activity (wherein R0 represents a C1-6 alkoxy group, C1-6 alkoxy-C1-6 alkoxy group or the like, R1 represents a C1-2 alkoxycarbonyl group, acetyl group or the like, Z represents a halogen atom, cyano group or the like, X represents a halogen atom, and n represents an integer of 0 to 3), and industrially advantageous production methods for producing 2-substituted amino-6-halomethylpyridine derivatives and tetrazolyloxime derivatives.
摘要翻译：公开了含有可以工业上有利的方式合成的吡啶环的化合物，可用作生产具有杀真菌活性的四唑基肟衍生物的中间体（其中R 0表示C1-6烷氧基，C1-6烷氧基C1- 6烷氧基等，R 1表示C 1-2烷氧基羰基，乙酰基等，Z表示卤素原子，氰基等，X表示卤素原子，n表示0〜3的整数）以及用于生产2-取代的氨基-6-卤甲基吡啶衍生物和四唑基肟衍生物的工业上有利的制备方法。

10. 发明授权

US08703959B2 Nitrogen-containing heterocyclic compound and method for producing same 有权
公开(公告)号：US08703959B2
公开(公告)日：2014-04-22
申请号：US13638700
申请日：2011-03-28
申请人： Koichi Kutose , Hiroki Inoue , Shiro Tsubokura
发明人： Koichi Kutose , Hiroki Inoue , Shiro Tsubokura
IPC分类号： C07D213/00
CPC分类号： C07D213/89 , C07D213/75
摘要： There are provided a nitrogen-containing heterocyclic compound such as a substituted amino-pyridine-N-oxide compound represented by formula (1), which is useful as a synthetic intermediate for an agrochemical and the like; and a method for producing the nitrogen-containing heterocyclic compound. (In formula (1), R1 and R2 each represents a hydrogen atom or an unsubstituted or substituted alkyl group; R3 represents a hydrogen atom, an unsubstituted or substituted alkylcarbonyl group or the like; R4 represents an unsubstituted or substituted alkylcarbonyl group, an unsubstituted or substituted arylcarbonyl group or the like; A represents a hydroxyl group, a thiol group or the like; m represents any one of integers of 1 to 4; k represents any one of integers of 0 to 3; and k+m≦4.)

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