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1. 发明授权

US08598349B2 Method for manufacturing conjugated aromatic compound 有权
标题翻译：共轭芳香族化合物的制造方法
公开(公告)号：US08598349B2
公开(公告)日：2013-12-03
申请号：US13144010
申请日：2010-01-18
申请人： Seiji Oda , Takashi Kamikawa , Akio Tanaka
发明人： Seiji Oda , Takashi Kamikawa , Akio Tanaka
IPC分类号： C07D401/04
CPC分类号： C07C45/72 , C07B37/04 , C07C17/269 , C07C41/30 , C07C67/343 , C07C253/30 , C07C303/30 , C08G61/12 , C08G2261/3442 , C08G2261/3444 , C07C25/18 , C07C49/76 , C07C49/84 , C07C69/76 , C07C43/2055 , C07C315/04
摘要： A method for manufacturing a conjugated aromatic compound comprising reacting an aromatic compound (A) substituted with a halogen as a leaving group with an aromatic compound (A) or an aromatic compound (B) substituted with a halogen as a leaving group and is structurally different from the aromatic compound (A), in the presence of (i) a nickel compound, (ii) a metal reducing agent, (iii) at least one ligand (L1) selected from the group consisting of a 2,2′-bipyridine compound having at least one electron-withdrawing group, and a 1,10-phenanthroline compound having at least one electron-withdrawing group, and (iv) at least one ligand (L2) selected from the group consisting of a 2,2′-bipyridine compound having at least one electron-releasing group, and a 1,10-phenanthroline compound having at least one electron-releasing group.
摘要翻译：一种共轭芳香族化合物的制造方法，其特征在于，包括使被取代为离去基团的卤素的芳香族化合物（A）与作为离去基团的卤素取代的芳香族化合物（A）或芳香族化合物（B）反应，结构不同在芳族化合物（A）中，在（i）镍化合物，（ii）金属还原剂，（iii）至少一种选自2,2'-联吡啶的配体（L1）的存在下，具有至少一个吸电子基团的化合物和具有至少一个吸电子基团的1,10-菲咯啉化合物，和（iv）至少一种选自2,2'- 具有至少一个电子释放基团的联吡啶化合物和具有至少一个电子释放基团的1,10-菲咯啉化合物。

2. 发明申请

US20110275859A1 METHOD FOR MANUFACTURING CONJUGATED AROMATIC COMPOUND 有权
公开(公告)号：US20110275859A1
公开(公告)日：2011-11-10
申请号：US13144010
申请日：2010-01-18
申请人： Seiji Oda , Takashi Kamikawa , Akio Tanaka
发明人： Seiji Oda , Takashi Kamikawa , Akio Tanaka
IPC分类号： C07C315/04
CPC分类号： C07C45/72 , C07B37/04 , C07C17/269 , C07C41/30 , C07C67/343 , C07C253/30 , C07C303/30 , C08G61/12 , C08G2261/3442 , C08G2261/3444 , C07C25/18 , C07C49/76 , C07C49/84 , C07C69/76 , C07C43/2055 , C07C315/04
摘要： A method for manufacturing a conjugated aromatic compound comprising reacting an aromatic compound (A) wherein one or two leaving groups selected from the group consisting of an iodine atom, a bromine atom and a chlorine atom are bonded to an aromatic ring and the aromatic compound (A) does not have (c1) a group represented by the following formula (10): wherein A1 represents a C1-C20 alkoxy group etc.; (g1) a C1-C20 alkyl group which may be substituted with a fluorine atom etc.; and (h1) a C2-C20 acyl group which may be substituted with a fluorine atom etc., at the neighboring carbon atom to the carbon atom to which the leaving group is bonded, with an aromatic compound (A) having the same structure as that of the above-mentioned aromatic compound (A) or an aromatic compound (B) wherein the aromatic compound (B) is structurally different from the above-mentioned aromatic compound (A), one or two leaving groups selected from the group consisting of an iodine atom, a bromine atom and a chlorine atom are bonded to an aromatic ring and the aromatic compound (B) does not have the above-mentioned (c1), (g1) and (h1) at the neighboring carbon atom to the carbon atom to which the leaving group is bonded, in the presence of (i) a nickel compound, (ii) a metal reducing agent, (iii) at least one ligand (L1) selected from the group consisting of a 2,2′-bipyridine compound having at least one electron-withdrawing group and having no substituent at 3-, 6-, 3′- and 6′-positions, and a 1,10-phenanthroline compound having at least one electron-withdrawing group and having no substituent at 2- and 9-positions, and (iv) at least one ligand (L2) selected from the group consisting of a 2,2′-bipyridine compound having at least one electron-releasing group and having no substituent at 3-, 6-, 3′- and 6′-positions, and a 1,10-phenanthroline compound having at least one electron-releasing group and having no substituent at 2- and 9-positions.

3. 发明申请

US20110275780A1 METHOD FOR PRODUCING CONJUGATED AROMATIC COMPOUND 审中-公开
标题翻译：生产结合芳族化合物的方法
公开(公告)号：US20110275780A1
公开(公告)日：2011-11-10
申请号：US13144026
申请日：2010-01-18
申请人： Seiji Oda , Takashi Kamikawa
发明人： Seiji Oda , Takashi Kamikawa
IPC分类号： C08G2/06 , C08G75/23 , C08G2/20 , C08G2/16
CPC分类号： C07C45/72 , C07C49/84 , C07C315/04 , C08G61/12 , C08G2261/3442 , C08G2261/3444
摘要： A method for producing a conjugated aromatic compound comprising reacting an aromatic compound (A) represented by the formula (1) wherein n represents 0 or 1, m represents (3-n), R1 represents a C1-C20 alkyl group etc., R2 is independently in each occurrence a hydrogen atom etc., X1 and X3 independently each represent a chlorine atom etc., with an aromatic compound (A) having the same structure as that of the above-mentioned aromatic compound (A) or an aromatic compound (B) wherein the aromatic compound (B) is structurally different from the above-mentioned aromatic compound (A) and one or two leaving groups selected from the group consisting of an iodine atom, a bromine atom and a chlorine atom are bonded to an aromatic ring, in the presence of a nickel compound, a metal reducing agent, and a 2,2′-bipyridine compound having at least one electron-releasing group and having no substituent at 3-, 6-, 3′- and 6′-positions.
摘要翻译：一种共轭芳香族化合物的制造方法，其特征在于，使由式（1）表示的芳香族化合物（A）（其中n表示0或1）表示，m表示（3-n），R1表示C1-C20烷基等，R2 在每种情况下独立地为氢原子等，X1和X3各自独立地表示氯原子等，与具有与上述芳香族化合物（A）相同结构的芳香族化合物（A）或芳香族化合物（B）其中芳族化合物（B）在结构上不同于上述芳香族化合物（A），并且一个或两个离开基团，选自碘原子，溴原子和氯原子结合到芳族环，在镍化合物，金属还原剂和具有至少一个电子释放基团并且在3，6，3'和6'上没有取代基的2,2'-联吡啶化合物存在下，位置。

4. 发明申请

US20090326188A1 Method for producing polyarylene 审中-公开
标题翻译：聚亚芳基的制备方法
公开(公告)号：US20090326188A1
公开(公告)日：2009-12-31
申请号：US12310997
申请日：2007-08-31
申请人： Seiji Oda , Takashi Kamikawa
发明人： Seiji Oda , Takashi Kamikawa
IPC分类号： C08G61/10
CPC分类号： C08G61/10 , C08G61/12 , C08G2261/1452 , C08G2261/31 , C08G2261/312 , C08G2261/3442 , C08G2261/412 , H01B1/122 , H01M8/1025 , H01M8/1027 , H01M8/1032 , H01M8/1039 , H01M8/1072 , H01M2300/0082 , Y02P70/56
摘要： A method for producing a polyarylene comprising polymerizing only a dihalobiphenyl compound represented by the formula (1): wherein A represents a C1-C20 alkoxy group etc., R1 represents a fluorine atom etc., X1 represents a chlorine atom etc., and k represents an integer of 0 to 3, or a dihalobiphenyl compound represented by the formula (1) with an aromatic compound represented by the formula (2): or an aromatic compound represented by the formula (3): X3-Ar5-X3 (3) wherein a, b and c represents 0 or 1, n represents an integer of 5 or more, Ar1, Ar2, Ar3 and Ar4 represents a divalent aromatic group etc., Y1 and Y2 represents a single bond etc., Z1 and Z2 represents —O— or —S—, and X2 and X3 represent a chlorine atom etc., in the presence of catalytic amounts of a divalent nickel compound, a trivalent phosphorus ligand and zinc.
摘要翻译：聚亚芳基的制造方法，其仅包含式（1）表示的二卤代联苯化合物：其中A表示C1-C20烷氧基等，R1表示氟原子等，X1表示氯原子等，k表示（3）表示的芳香族化合物或式（3）所示的芳香族化合物：式（3）表示的芳香族化合物：式（3）表示的芳香族化合物：X3-Ar5-X3 ）其中a，b和c表示0或1，n表示5或更大的整数，Ar 1，Ar 2，Ar 3和Ar 4表示二价芳基等，Y1和Y2表示单键等，Z1和Z2表示 -O-或-S-，X2和X3表示氯原子等，在催化量的二价镍化合物，三价磷配体和锌的存在下。

5. 发明申请

US20090036632A1 Polyarylene and Process for Producing the Same 失效
标题翻译：聚亚芳基及其制备方法
公开(公告)号：US20090036632A1
公开(公告)日：2009-02-05
申请号：US12224672
申请日：2006-09-06
申请人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Katsuhiro Suenobu
发明人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Katsuhiro Suenobu
IPC分类号： C08G75/23 , C07C317/16 , C08G75/30 , C08G8/02
CPC分类号： C08G61/02 , C07C309/73 , C07C311/16 , C08G61/10 , C08G65/4012 , C08G75/23 , C08G2261/122 , C08G2261/1452 , C08G2261/312 , C08G2261/516
摘要： A dihalobiphenyl compound represented by the formula (1): wherein A represents an amino group substituted with one or two C1-C20 hydrocarbon groups or a C1-C20 alkoxy group, R1 represents a fluorine atom, a C1-C20 alkyl group, etc., X1 represents a chlorine atom, a bromine atom or an iodine atom, an k represents an integer of 0 to 3, and a polyarylene comprising a repeating unit represented by the formula (2): wherein A, R1 and k represent the same meanings as defined above.
摘要翻译：由式（1）表示的二卤代联苯化合物：其中A表示被一个或两个C 1 -C 20烃基或C 1 -C 20烷氧基取代的氨基，R 1表示氟原子，C 1 -C 20烷基等。 X1表示氯原子，溴原子或碘原子，k表示0〜3的整数，以及含有由式（2）表示的重复单元的聚亚芳基：其中，A，R1和k表示相同的含义如上所述。

6. 发明授权

US08236920B2 Polyarylene and process for producing the same 失效
标题翻译：聚亚芳基及其制备方法
公开(公告)号：US08236920B2
公开(公告)日：2012-08-07
申请号：US12224672
申请日：2006-09-06
申请人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Katsuhiro Suenobu
发明人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Katsuhiro Suenobu
IPC分类号： C08G75/20 , C08G75/23 , C08G8/02 , C07C317/16
CPC分类号： C08G61/02 , C07C309/73 , C07C311/16 , C08G61/10 , C08G65/4012 , C08G75/23 , C08G2261/122 , C08G2261/1452 , C08G2261/312 , C08G2261/516
摘要： A dihalobiphenyl compound represented by the formula (1): wherein A represents an amino group substituted with one or two C1-C20 hydrocarbon groups or a C1-C20 alkoxy group, R1 represents a fluorine atom, a C1-C20 alkyl group, etc., X1 represents a chlorine atom, a bromine atom or an iodine atom, an k represents an integer of 0 to 3, and a polyarylene comprising a repeating unit represented by the formula (2): wherein A, R1 and k represent the same meanings as defined above.
摘要翻译：由式（1）表示的二卤代联苯化合物：其中A表示被一个或两个C 1 -C 20烃基或C 1 -C 20烷氧基取代的氨基，R 1表示氟原子，C 1 -C 20烷基等。 X1表示氯原子，溴原子或碘原子，k表示0〜3的整数，以及含有由式（2）表示的重复单元的聚亚芳基：其中，A，R1和k表示相同的含义如上所述。

7. 发明申请

US20100292481A1 METHOD FOR PRODUCING CONJUGATED AROMATIC COMPOUND 审中-公开
标题翻译：生产结合芳族化合物的方法
公开(公告)号：US20100292481A1
公开(公告)日：2010-11-18
申请号：US12809254
申请日：2008-12-17
申请人： Seiji Oda , Takashi Kamikawa
发明人： Seiji Oda , Takashi Kamikawa
IPC分类号： C07D401/04 , C07C303/26 , C07C45/00 , C07C249/00 , C07C25/13 , C07C39/12 , C07C319/00 , C07C1/00
CPC分类号： C07C303/30 , C07B37/04 , C07C1/26 , C07C17/269 , C07C41/30 , C07C45/72 , C07C49/84 , C07C253/30 , C07C303/40 , C07C2603/18 , C07D215/06 , C07D333/10 , C08G61/02 , C08G61/10 , C08G61/12 , C08G2261/1452 , C08G2261/312 , C08G2261/3142 , C08G2261/3442 , C08G2261/3444 , C08G2261/516 , C07C15/14 , C07C25/18 , C07C311/16 , C07C255/51 , C07C309/73 , C07C43/2055
摘要： A method for producing a conjugated aromatic compound comprising reacting an aromatic compound (A) wherein one or two leaving groups are bonded to an aromatic ring with an aromatic compound (A) having the same structure as that of the above-mentioned aromatic compound (A) or an aromatic compound (B) being structurally different from the above-mentioned aromatic compound (A) and having one or two leaving groups bonded to an aromatic ring, in the presence of a nickel compound, a ligand, a manganese salt and a metal reducing agent.
摘要翻译：一种共轭芳香族化合物的制造方法，其特征在于，使芳香族化合物（A）与芳香族化合物（A）结合的芳香族化合物（A）与上述芳香族化合物（A ）或与上述芳族化合物（A）在结构上不同的具有一个或两个与芳环键合的离去基团的芳族化合物（B），在镍化合物，配体，锰盐和金属还原剂。

8. 发明申请

US20090048413A1 Method for Production of Conjugated Polymer 审中-公开
标题翻译：共轭聚合物的制备方法
公开(公告)号：US20090048413A1
公开(公告)日：2009-02-19
申请号：US12224834
申请日：2007-03-09
申请人： Seiji Oda , Takashi Kamikawa
发明人： Seiji Oda , Takashi Kamikawa
IPC分类号： C08G79/08
CPC分类号： C08G61/123 , C08G61/02 , C08G61/10 , C08G61/126
摘要： A method for production of a conjugated polymer comprising contacting (A) an aromatic monomer having at least two boron-containing functional groups with an aromatic monomer having at least two reactive functional groups or (B) aromatic monomers having at least one boron-containing functional group and at least one reactive functional group with each other, both in an ether solvent in the presence of a palladium catalyst wherein a phosphine compound is coordinated to palladium, cesium carbonate and 1 to 100 moles of water per 1 mole of the boron-containing functional group of the above-mentioned aromatic monomer.
摘要翻译：一种制备共轭聚合物的方法，包括使（A）具有至少两个含硼官能团的芳族单体与具有至少两个反应性官能团的芳族单体或（B）具有至少一个含硼官能团的芳族单体基团和至少一个反应性官能团彼此，在醚溶剂中，在钯催化剂的存在下，其中膦化合物与钯配位，碳酸铯和每100摩尔含硼的1至100摩尔水上述芳香族单体的官能团。

9. 发明申请

US20080287646A1 Polyarylene and Method for Producing the Same 审中-公开
标题翻译：聚亚芳基及其制备方法
公开(公告)号：US20080287646A1
公开(公告)日：2008-11-20
申请号：US12083336
申请日：2006-09-06
申请人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Toru Onodera
发明人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Toru Onodera
IPC分类号： C08G75/24 , C08G75/30 , C07C309/39
CPC分类号： C08G61/10 , C07C309/73 , C07C311/16 , C07C2601/14 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M8/1072 , H01M2300/0082 , Y02P70/56
摘要： A dihalobenzene compound represented by the formula (1): wherein A represents a C3-C20 alkoxy group etc., R1 represents a hydrogen atom, a fluorine atom, a C1-C20 alkyl group, etc., X1 represents a chlorine atom, etc., m represents 1 or 2, and k represents 4-m, and a polyarylene comprising a repeating unit represented by the formula (2): wherein A, R1, m and k represent the same meanings as defined above.
摘要翻译：由式（1）表示的二卤苯化合物：其中A表示C 3 -C 20烷氧基等，R 1表示氢原子，氟原子，C 1 -C 20烷基等，X 1表示氯原子等，m表示1或2，k表示4-m，并且包含由式（2）表示的重复单元的聚亚芳基：其中A，R m和k表示与上述相同的含义。

10. 发明申请

US20060111593A1 Coupling catalyst and process using the same 审中-公开
标题翻译：偶联催化剂和工艺使用相同
公开(公告)号：US20060111593A1
公开(公告)日：2006-05-25
申请号：US11327382
申请日：2006-01-09
申请人： Tamon Itahashi , Takashi Kamikawa
发明人： Tamon Itahashi , Takashi Kamikawa
IPC分类号： C07C43/20
CPC分类号： B01J31/181 , B01J23/755 , B01J31/1805 , B01J31/1815 , B01J31/1825 , B01J31/184 , B01J31/2295 , B01J2231/4211 , B01J2531/847 , C07B37/04 , C07D213/06 , C07D213/16
摘要： There are disclosed a process for producing a coupling compound of formula (1): (Y-)n-1)R1-R2-(R1)(n′-1) (1), wherein R1 and R2 independently represent a substituted or unsubstituted aryl group, which process is characterized by reacting an unsaturated organic compound of formula (2): n′(R1X1n) (2) wherein n, n′, and R1 are the same as defined above, and X1 is the same or different and independently represents a leaving group and bonded with a sp2 carbon atom of R1 group, with a boron compound of formula (3): m{R2(BX22)n′} (3) wherein R2 and n′ are the same as defined above, X2 represents a hydroxy group, an alkoxy group, in the presence of a catalyst containing (A) a nickel compound, and (B) a nitrogen-containing cyclic compound, and the catalyst.
摘要翻译：公开了制备式（1）的偶联化合物的方法：<？in-line-formula description =“In-line Formulas”end =“lead”→（Y-）n-1）（n'-1）（1）（1）（1）（1）其中R 1和R 2独立地表示取代或未取代的芳基，其中R 1和R 2独立地表示取代或未取代的芳基该方法的特征在于使式（2）的不饱和有机化合物：<？in-line-formula description =“In-line Formulas”end =“lead”→n'（R 1> （2）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中n，n' 和R 1与上述定义相同，X 1相同或不同，并且独立地表示离去基团并且与R SUP的sp2碳原子键合具有式（3）的硼化合物：<？in-line-formula description =“In-line Formulas”end =“lead”？> m {R 2 SUP / >（BX 2 其中R＆lt; 2和n'与上述定义相同，X 2表示羟基，烷氧基，在含有（A）镍化合物的催化剂和（B ）含氮环状化合物和催化剂。

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