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1. 发明授权

US07217836B2 Process for producing (meth)acrolein and/or (meth)acrylic acid 有权
标题翻译：制备（甲基）丙烯醛和/或（甲基）丙烯酸的方法
公开(公告)号：US07217836B2
公开(公告)日：2007-05-15
申请号：US10479228
申请日：2002-05-21
申请人： Seigo Watanabe , Motomu Oh-Kita , Toshihiro Sato
发明人： Seigo Watanabe , Motomu Oh-Kita , Toshihiro Sato
IPC分类号： C07C51/235 , C07C51/16 , C07C45/00
CPC分类号： C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A method for producing (meth)acrolein and/or (meth)acrylic acid by subjecting isobutylene and the like or propylene to a vapor-phase catalytic oxidation with molecular oxygen in the presence of a solid oxidation catalyst in a tubular type of fixed bed reactor, wherein a temperature of a hot-spot zone is sufficiently controlled and (meth)acrolein and (meth)acrylic acid are produced with a high yield.A method for producing (meth)acrolein and/or (meth)acrylic acid by passing a raw material gas comprising isobutylene and the like or propylene and oxygen through a catalyst layer in a tubular type of fixed bed reactor which is filled with a solid oxidation catalyst, which includes passing a gas containing isobutylene and the like or propylene in a concentration lower than that of the raw material gas, and oxygen through the catalyst layer for a period of one hour or more prior to passing the raw material gas through the catalyst layer.
摘要翻译：在管式固定床反应器中，在固体氧化催化剂存在下，使用异丁烯等或丙烯进行气相催化氧化，制造（甲基）丙烯醛和/或（甲基）丙烯酸的方法其中热点区域的温度被充分控制，并以高产率制备（甲基）丙烯醛和（甲基）丙烯酸。通过将包含异丁烯等的原料气体或丙烯和氧气通过催化剂层在管式固定床反应器中进行填充的固体氧化物来生产（甲基）丙烯醛和/或（甲基）丙烯酸的方法催化剂，其包括在原料气体通过催化剂之前使含有异丁烯等的气体或浓度低于原料气体的丙烯和通过催化剂层的氧持续1小时以上层。

2. 发明授权

US06930201B2 Process for producing methacrylic acid 有权
标题翻译：生产甲基丙烯酸的方法
公开(公告)号：US06930201B2
公开(公告)日：2005-08-16
申请号：US10450712
申请日：2001-12-19
申请人： Seigo Watanabe , Motomu Oh-Kita
发明人： Seigo Watanabe , Motomu Oh-Kita
IPC分类号： B01J27/19 , B01J27/199 , C07B61/00 , C07C51/235 , C07C51/25 , C07C57/055 , C07C51/16
CPC分类号： B01J23/002 , B01J27/19 , B01J27/199 , B01J2523/00 , C07C51/252 , C07C57/04 , B01J2523/15 , B01J2523/17 , B01J2523/305 , B01J2523/42 , B01J2523/51 , B01J2523/55 , B01J2523/68 , B01J2523/22 , B01J2523/27 , B01J2523/64 , B01J2523/842
摘要： In a method of producing methacrylic acid by passing a material gas containing methacrolein, oxygen and water vapor through a reactor packed with a catalyst containing as the main component a compound oxide containing molybdenum and phosphorus, a concentration of methacrolein in the material gas is controlled in a range of 4 to 6.5 vol %, a molar ratio of the water vapor to the methacrolein in the material gas is controlled in a range of 1 to 2, and a space velocity of the material gas to the catalyst-packed layer is controlled in a range of 500 to 750 h−1, whereby deterioration of the catalyst is effectively inhibited.
摘要翻译：在通过使包含甲基丙烯醛，氧气和水蒸气的原料气体通过含有含有钼和磷的复合氧化物作为主要成分的催化剂的反应器生产甲基丙烯酸的方法中，控制原料气体中甲基丙烯醛的浓度 4〜6.5体积％范围内的原料气体中的水蒸汽与异丁烯醛的摩尔比控制在1〜2的范围内，并且将材料气体向催化剂填充层的空速控制在 500〜750h -1的范围，有效地抑制了催化剂的劣化。

3. 发明授权

US06346646B1 Process for producing methacrolein and methacrylic acid 有权
标题翻译：甲基丙烯醛和甲基丙烯酸的制备方法
公开(公告)号：US06346646B1
公开(公告)日：2002-02-12
申请号：US09463385
申请日：2000-01-27
申请人： Seigo Watanabe , Motomu Oh-Kita
发明人： Seigo Watanabe , Motomu Oh-Kita
IPC分类号： C07C5125
CPC分类号： C07C51/235 , B01J23/002 , B01J23/8876 , B01J2523/00 , C07C45/35 , C07C45/37 , C07C51/21 , C07C51/252 , C07C47/22 , C07C57/04 , B01J2523/15 , B01J2523/27 , B01J2523/53 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/845
摘要： A process for producing methacrolein and methacrylic acid by catalytically oxidizing isobutylene or tertiary butanol in the presence of a catalyst comprising a compound oxide containing molybdenum, bismuth and iron as the essential components, wherein a catalytic oxidation reaction is started at a temperature of (T−3)° C. or lower wherein T° C. is defined as the boundary temperature of activation energy of a reaction for obtaining methacrolein and methacrylic acid from isobutylene using said catalyst, the reaction is continued while the reaction temperature is increased as the activity of the catalyst decreases, and an activation treatment is conducted for the catalyst at least once before the reaction temperature exceeds the boundary temperature of activation energy.
摘要翻译：在含有以钼，铋和铁为主要成分的复合氧化物的催化剂存在下催化氧化异丁烯或叔丁醇的方法，其中催化氧化反应在（T- 3）℃或更低，其中T℃定义为使用所述催化剂从异丁烯获得异丁烯醛和甲基丙烯酸的反应的活化能的边界温度，反应继续，同时反应温度随着催化剂减少，并且在反应温度超过活化能的边界温度之前，对催化剂进行至少一次的活化处理。

4. 发明授权

US5349092A Process for producing catalysts for synthesis of unsaturated aldehydes and unsaturated carboxylic acids 失效
标题翻译：制备用于合成不饱和醛和不饱和羧酸的催化剂的方法
公开(公告)号：US5349092A
公开(公告)日：1994-09-20
申请号：US22648
申请日：1993-02-25
申请人： Seigo Watanabe , Motomu Oh-Kita
发明人： Seigo Watanabe , Motomu Oh-Kita
IPC分类号： B01J23/88 , B01J23/31 , B01J27/192 , B01J37/08 , C07B61/00 , C07C27/14 , C07C45/35 , C07C45/37 , C07C47/22 , C07C51/23 , C07C51/25 , C07C57/05 , C07C57/055 , C07C45/34 , B01J27/28
CPC分类号： C07C51/23 , B01J23/31 , C07C45/35 , C07C45/37 , C07C51/252
摘要： Disclosed is a process for producing a multicomponent catalyst containing molybdenum and bismuth and used for synthesis of unsaturated aldehydes and unsaturated carboxylic acids, characterized in that dried starting materials for the catalyst are calcinated in an atmosphere containing 1 vol % or more of a nitrogen oxide and 0.5 vol % or more of oxygen.
摘要翻译：公开了一种含有钼和铋的多组分催化剂的制备方法，用于合成不饱和醛和不饱和羧酸，其特征在于将干燥的催化剂原料在含有1体积％或更多氮氧化物的气氛中煅烧， 0.5体积％以上的氧气。

5. 发明授权

US5532199A Carrier-supported catalyst for the synthesis of unsaturated aldehydes and unsaturated carboxylic acids and process for preparing the same 失效
标题翻译：用于合成不饱和醛和不饱和羧酸的载体载体催化剂及其制备方法
公开(公告)号：US5532199A
公开(公告)日：1996-07-02
申请号：US359430
申请日：1994-12-20
申请人： Seigo Watanabe , Motomu Oh-Kita
发明人： Seigo Watanabe , Motomu Oh-Kita
IPC分类号： B01J23/31 , B01J23/887 , B01J35/06 , B01J37/02 , C07C45/35 , C07C45/37 , C07C51/25
CPC分类号： C07C45/37 , B01J23/002 , B01J23/31 , B01J23/8876 , B01J35/06 , C07C45/35 , C07C51/252 , B01J2523/00 , B01J37/0223
摘要： A carrier-supported catalyst for the synthesis of unsaturated aldehydes and unsaturated carboxylic acids, comprising a catalyst active substance comprising at least molybdenum and bismuth as its components, glass fiber having an average diameter in a range of more than 5 .mu.m and not more than 200 .mu.m and an average length in a range of from 50 .mu.m to 1 mm, which is used as a carrier assistant in an amount of 0.5-50% by weight based on the catalyst active substance, and a carrier. The carrier-supported catalyst of this invention suffers no release or fall-off of the catalyst active substance from the carrier even if the catalyst supporting rate is increased. It also has high mechanical strength and is helpful for providing the objective product in a high yield. Further, the carrier-supported catalyst preparation process of this invention is capable of producing a carrier-supported catalyst having excellent mechanical strength and enabling high-yield production of an objective product, with ease and good reproducibility.
摘要翻译：用于合成不饱和醛和不饱和羧酸的载体负载催化剂，其包含至少包含钼和铋作为其组分的催化剂活性物质，平均直径在5μm以上且不大于 200μm，平均长度为50μm〜1mm，作为载体助剂，其用量为催化剂活性物质的0.5〜50wt％，载体为载体。本发明的载体负载型催化剂即使催化剂支持率提高，也不会使催化剂活性物质从载体中释放或脱落。它还具有很高的机械强度，有助于以高产量提供目标产品。此外，本发明的载体负载型催化剂制备方法能够以容易且良好的再现性制造具有优异的机械强度且能够高产率生产目标产物的载体负载型催化剂。

6. 发明授权

US06969774B2 Method for producing methacrylic acid 有权
标题翻译：生产甲基丙烯酸的方法
公开(公告)号：US06969774B2
公开(公告)日：2005-11-29
申请号：US10148171
申请日：2000-12-07
申请人： Seigo Watanabe , Motomu Oh-Kita
发明人： Seigo Watanabe , Motomu Oh-Kita
IPC分类号： C07C51/25 , C07C57/055 , C07C51/235
CPC分类号： C07C51/252 , C07C57/04
摘要： In a method for synthesizing methacrylic acid by using a fixed bed tube type reactor provided with a catalyst bed into which a solid oxidation catalyst is filled and with a heat medium bath and by flowing a raw material gas containing methacrolein and oxygen through the catalyst bed, the catalyst bed does not have any sections in which a temperature difference between the heat medium bath and the catalyst bed (ΔT) exceeds 35° C., and two or more high temperature zones in which each ΔT is 15 to 35° C. are provided. According to this method, mathacrylic acid can be manufactured in higher yields.
摘要翻译：在通过使用固体床管式反应器合成甲基丙烯酸的方法中，所述反应器设置有填充有固体氧化催化剂的催化剂床和热介质浴，并且使含有甲基丙烯醛和氧气的原料气体通过催化剂床流动，催化剂床不具有其中热介质浴和催化剂床（DeltaT）之间的温差超过35℃的任何部分，并且其中每个DeltaT为15至35℃的两个或更多个高温区域为提供。根据该方法，能够以较高的收率制造数学丙烯酸。

7. 发明申请

US20060194693A1 Catalyst for acrylonitrile synthesis 有权
标题翻译：丙烯腈合成催化剂
公开(公告)号：US20060194693A1
公开(公告)日：2006-08-31
申请号：US10553200
申请日：2004-04-14
申请人： Seigo Watanabe , Koichi Mizutani , Motoo Yanagita , Jinko Izumi
发明人： Seigo Watanabe , Koichi Mizutani , Motoo Yanagita , Jinko Izumi
IPC分类号： B01J23/28
CPC分类号： C07C253/26 , B01J21/08 , B01J23/002 , B01J23/8876 , B01J27/192 , B01J2523/00 , Y02P20/52 , B01J2523/13 , B01J2523/14 , B01J2523/22 , B01J2523/3712 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/845 , B01J2523/847 , B01J2523/305 , B01J2523/51 , B01J2523/53 , C07C255/08
摘要： A catalyst for acrylonitrile synthesis is disclosed which is composed of particles containing silica and a composite oxide including at least molybdenum. When the Mo/Si atomic ratio in bulk composition of the catalyst is represented by A and the Mo/Si atomic ratio in surface composition of the particles is represented by B, B/A is not more than 0.6.
摘要翻译：公开了一种用于丙烯腈合成的催化剂，其由含有二氧化硅和至少包含钼的复合氧化物的颗粒组成。当催化剂的本体组成中的Mo / Si原子比由A表示，并且颗粒的表面组成中的Mo / Si原子比由B表示时，B / A不大于0.6。

8. 发明申请

US20060078165A1 Motion detection apparatus and motion detection method 有权
公开(公告)号：US20060078165A1
公开(公告)日：2006-04-13
申请号：US11146041
申请日：2005-06-07
申请人： Seigo Watanabe
发明人： Seigo Watanabe
IPC分类号： G06K9/00
CPC分类号： G06T7/248 , G06T7/73 , G06T2207/10016 , G06T2207/30241 , G06T2207/30248
摘要： A motion detection device includes a feature extracting section 2 extracting a feature area of an object from among frame images clipped by an image pickup section 1, a feature standardizing section 3 standardizing a size of a feature area extracted by the feature extracting section 2, a balloting section 4 counting up a ballot value of an image area on a frame image located in a standardized pattern that is standardized by the feature standardizing section 3, and a shift speed detecting section 5 calculating a gradient of a counted-up ballot value and calculating a shift direction, a shift speed and position of a feature area based on the gradient.

9. 发明授权

US5191817A Machining method for the use of a complex machining machine tool 失效
标题翻译：使用复杂加工机床的加工方法
公开(公告)号：US5191817A
公开(公告)日：1993-03-09
申请号：US439939
申请日：1989-11-21
申请人： Hiroshi Kojima , Keikichi Sakata , Seigo Watanabe , Yukio Mitsukuchi , Shuichi Hashimoto , Choji Kato , Mikiro Teshigawara , Ryoichi Furuhashi , Shoji Momoi , Toshihiko Inoue , Kazuki Uemura , Katsushi Oshima
发明人： Hiroshi Kojima , Keikichi Sakata , Seigo Watanabe , Yukio Mitsukuchi , Shuichi Hashimoto , Choji Kato , Mikiro Teshigawara , Ryoichi Furuhashi , Shoji Momoi , Toshihiko Inoue , Kazuki Uemura , Katsushi Oshima
IPC分类号： B23B3/06 , B23B3/16 , B23B3/30 , B23Q1/01 , B23Q7/00 , B23Q7/04 , B23Q39/04 , G05B19/18 , G05B19/4061 , G05B19/4093 , G05B19/414
CPC分类号： G05B19/4093 , B23B3/06 , B23B3/167 , B23B3/30 , B23Q1/01 , B23Q39/048 , B23Q7/001 , B23Q7/04 , B23Q7/043 , B23Q7/045 , G05B19/182 , G05B19/4061 , G05B19/414 , G05B2219/31407 , G05B2219/33263 , G05B2219/36338 , G05B2219/42104 , G05B2219/45125 , G05B2219/49143 , G05B2219/50001 , G05B2219/50003 , G05B2219/50004 , G05B2219/50219 , G05B2219/50235 , G05B2219/50382 , G05B2219/50387 , Y02P90/265 , Y10T82/10
摘要： A complex machine tool has a single frame having a chip collecting space at a center portion thereof, first and second spindle stocks on the frame, relatively free to move and drive in a Z axis direction and holding the chip collecting space therebetween, workpiece spindles on the spindle stocks free to rotate and drive and facing each other, and tool rests. The tool rests have turrets and can assume various kinds of movement. Complicated and varied types of machining can be performed combining the rotation control of the workpiece spindles and the spindle stocks.
摘要翻译：复杂的机床具有在其中心部分具有芯片收集空间的单个框架，框架上的第一和第二主轴架，相对自由地沿Z轴方向移动和驱动，并且在其间保持芯片收集空间，工件主轴在主轴库存自由旋转并相互驱动并相互对置，刀具支架。刀具具有炮塔，可以承担各种运动。可以结合工件主轴的旋转控制和主轴库存进行复杂多样的加工。

10. 发明授权

US5168609A Workpiece support for a turret on a opposed spindle lathe 失效
标题翻译：工件支撑在相对的主轴车床上的转塔
公开(公告)号：US5168609A
公开(公告)日：1992-12-08
申请号：US634550
申请日：1990-12-27
申请人： Hiroshi Kojima , Keikichi Sakata , Seigo Watanabe , Yukio Mitsukuchi
发明人： Hiroshi Kojima , Keikichi Sakata , Seigo Watanabe , Yukio Mitsukuchi
IPC分类号： B23B3/06 , B23B3/16 , B23B3/30 , B23Q7/00 , B23Q7/04 , B23Q39/04 , G05B19/18
CPC分类号： G05B19/182 , B23B3/06 , B23B3/167 , B23B3/30 , B23Q39/048 , B23Q7/001 , B23Q7/04 , B23Q7/043 , B23Q7/045 , G05B2219/45125 , Y10T29/5109 , Y10T82/2593
摘要： A complex machine tool has a single frame having a chip collecting space at a center portion thereof, first and second spindle stocks on the frame, relatively free to move and drive in a Z axis direction and holding the chip collecting space therebetween, workpiece spindles on the spindle stocks free to rotate and drive and facing each other, and tool rests. The tool rests have turrets and can assume various kinds of movement. Complicated and varied types of machining can be performed combining the rotation control of the workpiece spindles and the spindle stocks.
摘要翻译：复杂的机床具有在其中心部分具有芯片收集空间的单个框架，框架上的第一和第二主轴架，相对自由地沿Z轴方向移动和驱动，并且在其间保持芯片收集空间，工件主轴在主轴库存自由旋转并相互驱动并相互对置，刀具支架。刀具具有炮塔，可以承担各种运动。可以结合工件主轴的旋转控制和主轴库存进行复杂多样的加工。

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