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1. 发明授权

US5256720A Polypropylene resin composition 失效
标题翻译：聚丙烯树脂组合物
公开(公告)号：US5256720A
公开(公告)日：1993-10-26
申请号：US888712
申请日：1992-05-27
申请人： Satoshi Kuwata , Toshio Shiobara
发明人： Satoshi Kuwata , Toshio Shiobara
IPC分类号： C08J5/18 , C08K3/22 , C08K3/34 , C08K3/36 , C08L23/10 , C08K9/06
CPC分类号： C08J5/18 , C08K3/22 , C08K3/36 , C08J2323/10
摘要： Disclosed is a novel polypropylene resin composition which is outstandingly free from surface tackiness and still has good transparency so as to be useful as a material of resin films used for wrapping. The resin composition comprises, as a uniform blend, (a) 100 parts by weight of a polypropylene resin, and (b) from 0.01 to 10 parts by weight of an inorganic oxide powder which is a product obtained by the deflagration of an inorganic oxidizable powder, e.g., an elementary silicon powder, in an oxidizing atmosphere such as air. By virtue of the unique method for the preparation of the silicon dioxide powder, the particles have high surface activity so that the surface properties of the resin composition or, in particular, resin films prepared therefrom can be greatly improved even with a relatively small amount of the inorganic oxide powder compounded as an anti-blocking agent not to badly affect the transparency.

2. 发明授权

US08823186B2 Fiber-containing resin substrate, sealed substrate having semiconductor device mounted thereon, sealed wafer having semiconductor device formed thereon, a semiconductor apparatus, and method for manufacturing semiconductor apparatus 有权
标题翻译：含有纤维的树脂基板，其上安装有半导体装置的密封基板，其上形成有半导体装置的密封晶片，半导体装置和半导体装置的制造方法
公开(公告)号：US08823186B2
公开(公告)日：2014-09-02
申请号：US13301035
申请日：2011-11-21
申请人： Susumu Sekiguchi , Toshio Shiobara
发明人： Susumu Sekiguchi , Toshio Shiobara
IPC分类号： H01L23/29
CPC分类号： H01L21/561 , H01L21/568 , H01L23/293 , H01L24/97 , H01L2924/10253 , H01L2924/15788 , H01L2924/181 , Y10T442/2041 , H01L2924/00
摘要： A fiber-containing resin substrate for collectively sealing a semiconductor devices mounting surface of a substrate having the semiconductor devices mounted thereon or a semiconductor devices forming surface of a wafer having semiconductor devices formed thereon, includes: a resin-impregnated fiber base material obtained by impregnating a fiber base material with a thermosetting resin and semi-curing or curing the thermosetting resin; and an uncured resin layer containing an uncured thermosetting resin and formed on one side of the resin-impregnated fiber base material. There can be a fiber-containing resin substrate that enables suppressing warp of a wafer and delamination of semiconductor devices even though a large-diameter wafer or a large-diameter substrate made of a metal and the like is sealed, enables collectively sealing a semiconductor devices mounting surface of the substrate or a semiconductor devices forming surface of the wafer, and has excellent heat resistance or moisture resistance after sealing.
摘要翻译：用于共同密封其上安装有半导体器件的基板的半导体器件安装表面或形成有半导体器件的形成表面的半导体器件的含纤维树脂基板包括：通过浸渍获得的树脂浸渍的纤维基材具有热固性树脂并半固化或固化所述热固性树脂的纤维基材; 以及未固化的树脂层，其含有未固化的热固性树脂，并且在树脂浸渍的纤维基材的一侧上形成。即使由金属等制成的大直径晶片或大直径基板被密封，也可以是能够抑制晶片翘曲和半导体器件分层的含纤维树脂基板，能够集中地密封半导体器件衬底的安装表面或形成晶片表面的半导体器件，并且在密封后具有优异的耐热性或耐湿性。

3. 发明授权

US08497024B2 Organopolysilmethylene-siloxane and a cured product thereof 有权
标题翻译：有机聚硅氧烷 - 硅氧烷及其固化物
公开(公告)号：US08497024B2
公开(公告)日：2013-07-30
申请号：US12860682
申请日：2010-08-20
申请人： Manabu Ueno , Toshio Shiobara , Tsutomu Kashiwagi
发明人： Manabu Ueno , Toshio Shiobara , Tsutomu Kashiwagi
IPC分类号： B32B9/04
CPC分类号： C08G77/50 , C08G77/16 , C08G77/18 , C08G77/24 , C08L83/14 , Y10T428/31663 , C08L83/00
摘要： Organopolysilmethylene-siloxane of the formula (1): wherein each R1 is, independently of one another, an unsubstituted or substituted monovalent hydrocarbon group having 1 to 10 carbon atoms other than an alkenyl group, an alkoxy group, a hydroxy group, and a halogen atom; each R2 is, independently of one another, an unsubstituted or substituted monovalent hydrocarbon group having 1 to 10 carbon atoms other than an alkenyl group, an alkoxy group, a hydroxy group, a halogen atom, and (R1)3SiCH2—, wherein each R3 is, independently of one another, a hydrogen atom and an alkyl group having 1 to 4 carbon atoms; k is an integer of 1 to 100; and n is an integer of 1 to 1000; said organopolysilmethylene-siloxane having, in a molecule, at least two out of alkoxy groups, hydroxy groups, and halogen atoms bonded to one or more silicon atoms.
摘要翻译：式（1）的有机聚硅氧烷 - 硅氧烷：其中每个R 1彼此独立地是除烯基，烷氧基，羟基和卤素以外的未取代或取代的碳原子数1〜10的一价烃基原子; 每个R 2彼此独立地是除烯基，烷氧基，羟基，卤素原子和（R 1）3 SiCH 2 - 以外具有1至10个碳原子的未取代或取代的一价烃基，其中每个R 3 彼此独立地是氢原子和具有1至4个碳原子的烷基; k为1〜100的整数， n为1〜1000的整数。所述有机聚硅氧烷 - 硅氧烷在分子中具有至少两个烷氧基，羟基和与一个或多个硅原子键合的卤素原子。

4. 发明授权

US08455899B2 Resin composition, reflector for light-emitting semiconductor device, and light-emitting semiconductor unit 有权
标题翻译：树脂组合物，发光半导体器件的反射器和发光半导体单元
公开(公告)号：US08455899B2
公开(公告)日：2013-06-04
申请号：US13074317
申请日：2011-03-29
申请人： Yusuke Taguchi , Toshio Shiobara
发明人： Yusuke Taguchi , Toshio Shiobara
IPC分类号： H01L33/00 , H01L23/29 , F21V7/00 , C08K5/00
CPC分类号： H01L33/60 , H01L24/97 , H01L33/486 , H01L33/62 , H01L2224/32245 , H01L2224/45144 , H01L2224/48091 , H01L2224/48247 , H01L2224/73265 , H01L2224/97 , H01L2924/01012 , H01L2924/01029 , H01L2924/10253 , H01L2924/12041 , H01L2924/12042 , H01L2924/15747 , H01L2924/181 , H01L2933/0058 , H01L2924/00014 , H01L2924/00
摘要： Disclosed herein is a resin composition including 100 parts by weight of an organic resin and 50 to 1,000 parts by weight of an inorganic filler, wherein 10 to 100% of the inorganic filler is composed of an oxide of a rare earth element.
摘要翻译：本发明公开了一种树脂组合物，其包含100重量份的有机树脂和50-1000重量份的无机填料，其中10-100重量％的无机填料由稀土元素的氧化物组成。

5. 发明授权

US08440776B2 Lens-forming silicone resin composition and silicone lens 有权
标题翻译：透镜成型硅树脂组合物和硅胶透镜
公开(公告)号：US08440776B2
公开(公告)日：2013-05-14
申请号：US12759293
申请日：2010-04-13
申请人： Tsutomu Kashiwagi , Toshio Shiobara , Katsuyuki Imazawa
发明人： Tsutomu Kashiwagi , Toshio Shiobara , Katsuyuki Imazawa
IPC分类号： C08G77/20
CPC分类号： G02B1/041 , C08G77/12 , C08G77/20 , C08L83/04 , C08L83/00
摘要： Silicone resin compositions comprising (A) an organopolysiloxane containing at least two aliphatic unsaturated bonds and having a viscosity of 100-1,000,000 mPa·s at 25° C., (B) an organohydrogenpolysiloxane having at least three silicon-bonded hydrogen atoms (SiH groups) in the form of HR62SiO—, and (C) a platinum group metal base catalyst cure into colorless transparent parts which are useful lenses.
摘要翻译：硅氧烷树脂组合物，其包含（A）含有至少两个脂族不饱和键并且在25℃下具有100-1,000,000mPa·s粘度的有机聚硅氧烷，（B）具有至少三个与硅键合的氢原子的有机氢聚硅氧烷（SiH基）），（C）铂族金属碱催化剂固化成无色透明部分，这是有用的透镜。

6. 发明授权

US07985806B2 Diglycidylisocyanuryl-modified organopolysiloxane and composition containing the same 有权
标题翻译：二缩水甘油基异氰脲基改性的有机聚硅氧烷及其组合物
公开(公告)号：US07985806B2
公开(公告)日：2011-07-26
申请号：US12360652
申请日：2009-01-27
申请人： Toshio Shiobara , Tsutomu Kashiwagi , Miyuki Wakao , Manabu Ueno
发明人： Toshio Shiobara , Tsutomu Kashiwagi , Miyuki Wakao , Manabu Ueno
IPC分类号： C08G77/14 , C08L83/06
CPC分类号： C08G77/388 , C08L83/08
摘要： An organopolysiloxane represented by formula (1) shown below and having (3,5-diglycidylisocyanuryl)alkyl groups represented by formula (2) at least at both terminals of the main chain: wherein, each R1 represents, independently, a substituted or unsubstituted monovalent hydrocarbon group of 1 to 20 carbon atoms, R2 is a group represented by formula (2) shown below, X is a group represented by formula (3) shown below, a represents an integer of 0 to 100 and b represents an integer of 0 to 30, provided that 1≦a+b, and c represents an integer of 0 to 10 wherein, R3 represents an alkylene group of 2 to 12 carbon atoms wherein, R1 and R2 are as defined above, d represents an integer of 0 to 30, and e represents an integer of 0 to 30.
摘要翻译：由式（1）表示的由下述式（1）表示的有机聚硅氧烷和至少在主链的两个末端具有由式（2）表示的（3,5-二缩水甘油基异氰脲基）烷基：其中，每个R 1独立地表示取代或未取代的一价 1〜20个碳原子的烃基，R2为下述式（2）所示的基团，X为下述式（3）表示的基团，a表示0〜100的整数，b表示0以下的整数至30，条件是1＆nlE; a + b和c表示0至10的整数，其中R 3表示2至12个碳原子的亚烷基，其中R 1和R 2如上所定义，d表示0至 30，e表示0〜30的整数。

7. 发明授权

US07705093B2 Phosphor-filled curable silicone resin composition and cured product thereof 有权
标题翻译：荧光填充固化性有机硅树脂组合物及其固化物
公开(公告)号：US07705093B2
公开(公告)日：2010-04-27
申请号：US11762445
申请日：2007-06-13
申请人： Tsutomu Kashiwagi , Toshio Shiobara
发明人： Tsutomu Kashiwagi , Toshio Shiobara
IPC分类号： C08G77/04
CPC分类号： C08L83/04 , C08G77/12 , C08G77/20 , C08G77/70 , C08K3/32 , C08L83/00
摘要： A phosphor-containing addition-curable silicone resin composition is provided. The composition is capable of forming a cured product which exhibits excellent crack resistance and shock resistance, and minimal surface tackiness. The composition includes (A) an organopolysiloxane including R1SiO1.5 units (T units), R22SiO units (D units), and R3aR4bSiO(4-a-b)/2 units (wherein, R1, R2 and R3 represent a methyl group or the like, R4 represents a vinyl group or allyl group, a represents an integer from 0 to 2, b represents 1 or 2, and a+b is either 2 or 3), in which the number of repetitions of the D units is within a range from 5 to 300; (B) an Si—H-containing polysiloxane including T units, D units, and R3cHdSiO(4-c-d)/2 units (wherein, c represents an integer from 0 to 2, d represents 1 or 2, and c+d is either 2 or 3), in which the number of repetitions of the D units is within a range from 5 to 300, in sufficient quantity that the molar ratio of Si-bonded hydrogen atoms within (B), relative to vinyl groups or allyl groups within (A), is within a range from 0.1 to 4.0; (C) a catalyst; and (D) a phosphor.
摘要翻译：提供含磷光体的可加成固化的有机硅树脂组合物。该组合物能够形成表现出优异的抗裂性和抗冲击性和最小表面粘性的固化产物。该组合物包含（A）包含R1SiO1.5单元（T单元），R22SiO单元（D单元）和R3aR4bSiO（4-ab）/ 2单元的有机聚硅氧烷（其中，R1，R2和R3表示甲基等，R4表示乙烯基或烯丙基，a表示0〜2的整数，b表示1或2，a + b为2或3），D单元的重复数在从5到300; （B）包含T单元，D单元和R3cHdSiO（4-cd）/ 2单元的Si-H的聚硅氧烷（其中，c表示0至2的整数，d表示1或2，c + d为 2或3），其中D单元的重复数在5至300的范围内，其量足以使（B）内的与Si键合的氢原子相对于乙烯基或烯丙基的摩尔比（A）范围内，为0.1〜4.0; （C）催化剂; 和（D）荧光体。

8. 发明授权

US07563854B2 Method of producing high molecular weight organopolysiloxane, composition comprising the high molecular weight organopolysiloxane, and optical semiconductor device sealed with cured product thereof 有权
标题翻译：生产高分子量有机聚硅氧烷的方法，包含高分子量有机聚硅氧烷的组合物和用其固化产物密封的光学半导体器件
公开(公告)号：US07563854B2
公开(公告)日：2009-07-21
申请号：US11586525
申请日：2006-10-26
申请人： Hisashi Shimizu , Toshio Shiobara , Tsutomu Kashiwagi
发明人： Hisashi Shimizu , Toshio Shiobara , Tsutomu Kashiwagi
IPC分类号： C08G77/06
CPC分类号： C08G77/04 , C08G77/06 , C08G77/08 , C08G77/14 , Y10T428/31663
摘要： Provided is a method of producing a high molecular weight organopolysiloxane with a polystyrene equivalent weight average molecular weight of at least 5×104, comprising the steps of producing an organopolysiloxane by subjecting a silane compound having a hydrolyzable group to a first hydrolysis and condensation, and then subjecting that organopolysiloxane to an additional second hydrolysis and condensation. The high molecular weight organopolysiloxane is stable, resistant to gelling, and resistant to cracking even when formed as a thick film. A resin composition comprising the high molecular weight organopolysiloxane and a condensation catalyst is useful for sealing an optical element and for producing an optical semiconductor device.
摘要翻译：本发明提供一种聚苯乙烯换算重均分子量为5×10 4以上的高分子量有机聚硅氧烷的制造方法，其特征在于，包括使具有水解性基团的硅烷化合物进行第一次水解缩合而制造有机聚硅氧烷的工序，该有机聚硅氧烷再次进行水解和缩合。高分子量有机聚硅氧烷是稳定的，耐胶凝的，即使形成厚膜也能耐裂纹。包含高分子量有机聚硅氧烷和缩合催化剂的树脂组合物可用于密封光学元件并用于制造光学半导体器件。

9. 发明授权

US07550204B2 Resin composition for sealing optical device, cured product thereof, and method of sealing semiconductor element 有权
标题翻译：用于密封光学元件的树脂组合物，其固化产物，以及密封半导体元件的方法
公开(公告)号：US07550204B2
公开(公告)日：2009-06-23
申请号：US11586564
申请日：2006-10-26
申请人： Hisashi Shimizu , Toshio Shiobara , Tsutomu Kashiwagi
发明人： Hisashi Shimizu , Toshio Shiobara , Tsutomu Kashiwagi
IPC分类号： B32B9/04 , C08G77/18
CPC分类号： C08L83/04 , C08G77/14 , C08G77/18 , C08G77/20 , C08G77/70 , C08J7/047 , C08J2483/00 , C08K5/0091 , H01L23/296 , H01L2924/0002 , Y10T428/31663 , H01L2924/00
摘要： The present invention provides a composition for sealing an optical device comprising (i) a silylated organopolysiloxane with a polystyrene equivalent weight average molecular weight of 5×104 or greater, represented by an average composition formula: R1a(OX)bSiO(4−a−b)/2 (wherein, R1 represents an alkyl group, alkenyl group, or aryl group; X represents a combination of a group represented by a formula —SiR2R3R4 (wherein, RE to R4 are monovalent hydrocarbon groups), and an alkyl group, alkenyl group, alkoxyalkyl group or acyl group; a represents a number within a range from 1.00 to 1.5; b represents a number that satisfies 0 b 2, and a+b satisfies 1.00 a+b 2), and (ii) a condensation catalyst, as well as a transparent cured product obtained by curing the composition, and a method of sealing a semiconductor element that comprises a step of applying the composition to a semiconductor element, and a step of curing the composition that has been applied to the semiconductor element. The composition can form a coating film that exhibits excellent levels of heat resistance, ultraviolet light resistance, optical transparency, toughness and adhesion.
摘要翻译：本发明提供了一种用于密封光学装置的组合物，其包含（i）聚苯乙烯换算的重均分子量为5×10 4或更大的甲硅烷基化有机聚硅氧烷，其平均组成式为：<？in-line-formula description =“In- 线形式“end =”lead“→> R1a（OX）bSiO（4-ab）/ 2 <？in-line-formula description =”In-line Formulas“end =”tail“？>（其中，R1表示烷基，烯基或芳基; X表示由式-SiR 2 R 3 R 4表示的基团（其中，RE至R 4为一价烃基）和烷基，烯基，烷氧基烷基或酰基的组合; 表示在1.00〜1.5的范围内的数字; b表示满足0 b 2的数，a + b满足1.00 a + b 2），（ii）缩合催化剂，以及由固化组合物，以及密封半导体元件的方法，其包括施加组合物的步骤涉及半导体元件，以及固化已经施加到半导体元件上的组合物的步骤。该组合物可以形成表现出优异的耐热性，耐紫外线性，光学透明性，韧性和粘附性的涂膜。

10. 发明申请

US20070249790A1 Silicone lens and silicone resin composition for molding lens 有权
标题翻译：硅胶透镜和用于成型镜片的硅树脂组合物
公开(公告)号：US20070249790A1
公开(公告)日：2007-10-25
申请号：US11785791
申请日：2007-04-20
申请人： Tsutomu Kashiwagi , Toshio Shiobara
发明人： Tsutomu Kashiwagi , Toshio Shiobara
IPC分类号： C08L83/04 , C08G77/00
CPC分类号： C08L83/04 , C08G77/12 , C08G77/16 , C08G77/20 , C08G77/70 , C08G77/80 , C08K5/56 , C08L83/00
摘要： A colorless transparent silicone lens produced by thermally curing a silicone resin composition comprising (A) an organopolysiloxane having a resin structure comprising R1SiO1.5 unit, R22SiO unit, and R3aR4bSiO(4-a-b)/2 unit wherein R1, R2, and R3 are independently methyl group, ethyl group, propyl group, cyclohexyl group, or phenyl group, R4 is vinyl group or allyl group, a is 0, 1, or 2, b is 1 or 2, and a+b is 2 or 3, and wherein number of repetition of the R22SiO unit is 5 to 300, (B) an organohydrogen polysiloxane having a resin structure comprising R1SiO1.5 unit, R22SiO unit, and R3cHdSiO(4-c-d)/2 unit wherein c is 0, 1, or 2, d is 1 or 2, and c+d is 2 or 3, and wherein number of repetition of the R22SiO unit is 5 to 300, the component, and (C) a platinum group catalyst. A silicone lens having excellent flexibility, transparency, and moldability as well as reduced surface tackiness is provided.
摘要翻译：通过热固化有机硅树脂组合物制得的无色透明硅氧烷透镜，该有机硅树脂组合物包含（A）具有包含R 1 SiO 1/2单元的树脂结构的有机聚硅氧烷，R 2， SiO 2单元和R 3 SiO 2 SiO 2 SiO 2单元和/或SiO 2 其中R 1，R 2和R 3独立地是（4-ab）/ 2单元独立地是甲基乙基，丙基，环己基或苯基，R 4是乙烯基或烯丙基，a是0,1或2，b是1或2，a + b是 2或3，其中R 2 SiO 2 SiO单元的重复次数为5〜300，（B）具有包含R 2 SiO 2的树脂结构的有机氢聚硅氧烷， 1个SiO 1单元，R 2 O 2 SiO单元和R 3 -S 3单元其中c为0,1或2，d为1或2，c + d为（4-cd）/ 2单元 2或3，其中R 2 O 2 SiO单元的重复次数为5〜300，该成分为（C）铂族催化剂。提供了具有优异的柔性，透明性和成型性以及降低的表面粘性的硅氧烷透镜。

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