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1. 发明申请

WO2012104365A2 METHOD FOR MANUFACTURING PERFLUOROVINYLETHERS 审中-公开
标题翻译：制备全氟尿嘧啶的方法
公开(公告)号：WO2012104365A2
公开(公告)日：2012-08-09
申请号：PCT/EP2012/051730
申请日：2012-02-02
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.p.A. , MILLEFANTI, Stefano , TORTELLI, Vito , MARCHIONNI, Giuseppe , ALBONETTI, Stefania , GREGORI, Manuel , FORNASARI, Giuseppe
发明人： MILLEFANTI, Stefano , TORTELLI, Vito , MARCHIONNI, Giuseppe , ALBONETTI, Stefania , GREGORI, Manuel , FORNASARI, Giuseppe
IPC分类号： C07C41/42
CPC分类号： C07C41/24 , C07C43/17
摘要： The invention pertains to a process for the manufacture of a perfluorovinylether by hydrodehalogenation of a halofluoroether (HFE) having general formula (l-A) or (l-B): R f O-CR f 'X-CR f "R f "'X' (l-A) wherein Rf represents a C 1 -C 6 perfluoro(oxy)alkyl group; R f ', R f " and R f '", equal or different from each other, independently represent fluorine atoms or C 1 -C 5 perfluoro(oxy)alkyl groups; X and X', equal or different from each other, are independently chosen among CI, Br or I; wherein R f * and R f *', equal or different from each other, independently represent fluorine atoms or C 1 -C 3 perfluoro(oxy)alkyl groups; Y 1 and Y 2 , equal or different from each other, independently represent fluorine atoms or C 1 -C 3 perfluoroalkyl groups; X and X' are as above defined; said process comprising contacting said halofluoroether (HFE) with hydrogen in the presence of a catalyst comprising palladium and at least one transition metal (M) selected from the group consisting of the metals of group VIIIB, other than palladium, and of group IB.
摘要翻译：本发明涉及通过具有通式（1A）或（1B）的卤代氟醚（HFE）的加氢脱卤制备全氟乙烯基醚的方法：RfO-CRf'X-CRf“Rf”'X'（1A）其中Rf代表 C1-C6全氟（氧）烷基; Rf'，Rf“和Rf”“彼此相同或不同，独立地表示氟原子或C1-C5全氟（氧）烷基; X和X'彼此相同或不同，独立地选自CI，Br或I; 其中Rf *和Rf *'彼此相同或不同，独立地表示氟原子或C1-C3全氟（氧）烷基; Y1和Y2彼此相同或不同，独立地表示氟原子或C1-C3全氟烷基; X和X'如上所定义; 所述方法包括在催化剂存在下使所述卤代氟醚（HFE）与氢气接触，所述催化剂包含钯和至少一种选自除钯以外的第VIIIB族金属和IB族的过渡金属（M）。

2. 发明申请

WO2012000853A1 PROCESS FOR THE SYNTHESIS OF TRIFLUOROETHYLENE 审中-公开
标题翻译：三氟乙烯合成方法
公开(公告)号：WO2012000853A1
公开(公告)日：2012-01-05
申请号：PCT/EP2011/060400
申请日：2011-06-22
申请人： SOLVAY SOLEXIS S.p.A. , MILLEFANTI, Stefano , TORTELLI, Vito , MARCHIONNI, Giuseppe
发明人： MILLEFANTI, Stefano , TORTELLI, Vito , MARCHIONNI, Giuseppe
IPC分类号： C07C17/23 , C07C21/18
CPC分类号： B01J23/44 , B01J21/18 , B01J23/42 , B01J35/023 , B01J35/1023 , B01J35/1028 , B01J37/0009 , B01J37/18 , C07C17/23 , C07C21/18
摘要： A catalytic process for the synthesis of trifluoroethylene from chlorotrifluoroethylene which comprises contacting chlorotrifluoroethylene with hydrogen in the presence of a catalyst consisting of palladium or platinum supported on extruded activated carbon.
摘要翻译：用于从三氟氯乙烯合成三氟乙烯的催化方法，其包括在负载在挤出的活性炭上的由钯或铂组成的催化剂存在下使氯三氟乙烯与氢接触。

3. 发明申请

WO2009150091A1 METHOD FOR MANUFACTURING PERFLUOROVINYLETHERS 审中-公开
标题翻译：制备全氟尿嘧啶的方法
公开(公告)号：WO2009150091A1
公开(公告)日：2009-12-17
申请号：PCT/EP2009/056858
申请日：2009-06-04
申请人： SOLVAY SOLEXIS S.P.A. , MILLEFANTI, Stefano , TORTELLI, Vito , MARCHIONNI, Giuseppe
发明人： MILLEFANTI, Stefano , TORTELLI, Vito , MARCHIONNI, Giuseppe
IPC分类号： C07C17/35 , C07C17/00 , C07C19/08
CPC分类号： C07C41/24 , C07D317/34 , C07C43/17
摘要： The invention pertains to a process for the manufacture of a perfluorovinylether by hydrodehalogenation of a halofluoroether (HFE) having general formula (I-A) or (I-B): R f O-CR f 'X-CR f ''R f '''X' (I-A) wherein R f represents a C 1 -C 6 perfluoro(oxy)alkyl group; R f ', R f " and R f "' equal or different from each other, independently represent fluorine atoms or C 1 -C 5 perfluoro(oxy)alkyl groups; X and X', equal or different from each other, are independently chosen among Cl, Br or I; formula (I-B); wherein R f * and R f *', equal or different from each other, independently represent fluorine atoms or C 1 -C 3 perfluoro(oxy)alkyl groups; Y 1 and Y 2 , equal or different from each other, independently represent fluorine atoms or C 1 -C 3 perfluoroalkyl groups; X and X' are as above defined; said process comprising contacting said halofluoroether (HFE) with hydrogen in the presence of a catalyst comprising at least one transition metal of group VIII B at a temperature of at most 340°C.
摘要翻译：本发明涉及通过具有通式（IA）或（IB）的卤代氟醚（HFE）的加氢脱卤制备全氟乙烯基醚的方法：RfO-CRf'X-CRf''Rf“'X'（IA），其中 Rf表示C1-C6全氟（氧）烷基; Rf'，Rf“和Rf”'彼此相同或不同，独立地表示氟原子或C1-C5全氟（氧）烷基; X和X'彼此相同或不同，独立地选自Cl，Br或I; 式（I-B）; 其中Rf *和Rf *'彼此相同或不同，独立地表示氟原子或C1-C3全氟（氧）烷基; Y1和Y2彼此相同或不同，独立地表示氟原子或C1-C3全氟烷基; X和X'如上所定义; 所述方法包括在包含至少一种第ⅧB族过渡金属的催化剂存在下，在至多340℃的温度下使所述卤代氟醚（HFE）与氢气接触。

4. 发明申请

WO2012080098A1 FOAMABLE FLUOROPOLYMER COMPOSITIONS 审中-公开
标题翻译：可泡沫氟聚合物组合物
公开(公告)号：WO2012080098A1
公开(公告)日：2012-06-21
申请号：PCT/EP2011/072260
申请日：2011-12-09
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A. , COLAIANNA, Pasqua , BESANA, Giambattista , DI NICOLO, Emanuele , BRAGANTE, Letanzio , MARCHIONNI, Giuseppe , BRINATI, Giulio
发明人： COLAIANNA, Pasqua , BESANA, Giambattista , DI NICOLO, Emanuele , BRAGANTE, Letanzio , MARCHIONNI, Giuseppe , BRINATI, Giulio
IPC分类号： C08J9/00
CPC分类号： C08K5/42 , C08J9/0019 , C08J2327/12
摘要： The invention pertains to foamable thermoplastic fluoropolymer composition comprising: - at least one fluoropolymer [polymer (A)]; and - at least one perfluoroalkoxysulphonic derivative of either of formulae: (X n+ ) 1/n -O 3 S-CF 2 CF 2 O-R d f -OCF 2 CF 2 -SO 3 -(X n+ ) 1/n and R m f -OCF 2 CF 2 -SO 3 -(X n+ ) 1/n wherein R d f is a divalent C 1 -C 12 perfluorocarbon group, possibly comprising one or more ethereal oxygen atom; Rmf is a monovalent C 1 -C 12 perfluorocarbon group, possibly comprising one or more ethereal oxygen atom, optionally comprising heteroatoms, generally selected from S, N, P; X = H, a metal cation, or an ammonium group; n is the valence of the cation X, preferably 1 or 2.
摘要翻译：本发明涉及可发泡热塑性含氟聚合物组合物，其包含： - 至少一种含氟聚合物[聚合物（A）]; 和（Xn +）1 / n -O3S-CF2CF2O-Rdf-OCF2CF2-SO3-（Xn +）1 / n和Rmf-OCF2CF2-SO3-（Xn +）1 / n的至少一种全氟代烷氧基磺酸衍生物其中Rd f是可能包含一个或多个醚类氧原子的二价C1-C12全氟化碳基团; Rmf是单价C1-C12全氟化碳基团，可能包含一个或多个醚性氧原子，任选地包含杂原子，通常选自S，N，P; X = H，金属阳离子或铵基; n是阳离子X的化合价，优选1或2。

5. 发明申请

WO2012084749A1 THERMOPROCESSABLE PER(HALO)FLUOROPOLYMER COMPOSITION 审中-公开
标题翻译：（HALO）氟聚合物组合物
公开(公告)号：WO2012084749A1
公开(公告)日：2012-06-28
申请号：PCT/EP2011/073146
申请日：2011-12-16
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A. , COLAIANNA, Pasqua , AVATANEO, Marco , DI NICOLO, Emanuele , BESANA, Giambattista , MARCHIONNI, Giuseppe
发明人： COLAIANNA, Pasqua , AVATANEO, Marco , DI NICOLO, Emanuele , BESANA, Giambattista , MARCHIONNI, Giuseppe
IPC分类号： C08L71/02 , C08G65/00 , C08L27/00
CPC分类号： C08L53/00 , C08G65/007 , C08G2650/48 , C08K3/04 , C08K2003/3045 , C08L27/00 , C08L27/18 , C08L71/02 , C08L2666/04
摘要： The invention pertains to a thermoprocessable composition comprising: - at least one thermoprocessable per(halo)fluoropolymer [polymer (A)]; - at least one inorganic filler [filler (I)]; and - at least one perfluoropolyether block copolymer [polymer (E)] comprising: A) one or more (per)fluoropolyoxyalkylene segment (chain R f ), that is to say a segment comprising recurring units having at least one catenary ether bond and at least one fluorocarbon moiety, and B) one or more polyalkylene segment (chain R a ) comprising recurring units of formula: -(CR 1 R 2 -CR 3 R 4 )- wherein R 1 , R 2 , R 3 , R 4 , equal to or different from each other, are selected from the group consisting of H, halogens (preferably F, CI); C 1 -C 6 (hydro)carbon groups, optionally containing fluorine or other heteroatoms, preferably perfluoroalkyi or (per)fluorooxyalkyl.
摘要翻译：本发明涉及一种热可加工组合物，其包含： - 至少一种热可加工的每（卤）含氟聚合物[聚合物（A）]; - 至少一种无机填料[填料（I）]; 和 - 至少一种全氟聚醚嵌段共聚物[聚合物（E）]，其包含：A）一个或多个（全）氟聚氧亚烷基链段（链Rf），也就是说包含具有至少一个链中键的重复单元的链段和至少一个碳氟化合物部分，和B）包含式： - （CR 1 R 2 -CR 3 R 4） - 的重复单元的一个或多个聚亚烷基链段（链Ra） - 其中R 1，R 2，R 3，R 4彼此相同或不同，选自由H，卤素（优选F，Cl）组成的组; 任选地含有氟或其它杂原子的C 1 -C 6（氢）碳基团，优选全氟烷基或（全）氟氧烷基。

6. 发明申请

WO2012072538A1 FUEL CELL MODULES 审中-公开
标题翻译：燃料电池模块
公开(公告)号：WO2012072538A1
公开(公告)日：2012-06-07
申请号：PCT/EP2011/071114
申请日：2011-11-28
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A. , ARCELLA, Vincenzo , MARCHIONNI, Giuseppe , DE PATTO, Ugo , GUARDA, Pier, Antonio
发明人： ARCELLA, Vincenzo , MARCHIONNI, Giuseppe , DE PATTO, Ugo , GUARDA, Pier, Antonio
IPC分类号： H01M8/10 , H01M8/02
CPC分类号： H01M8/1006 , H01M8/0232 , H01M8/0254 , H01M8/1004 , H01M2008/1095
摘要： A method for the preparation of corrugated fuel cell units from a composite laminate comprising an ion conductive membrane having first and second surface; a first electrocatalyst layer in contact with the first surface of the membrane; a second electrocatalyst layer in contact with the second surface of the membrane; a first metallic mesh in contact with said first electrocatalyst layer and a second metallic mesh in contact with said second electrocatalyst layer.
摘要翻译：一种由复合层压制备波纹燃料电池单元的方法，包括具有第一和第二表面的离子传导膜; 与膜的第一表面接触的第一电催化剂层; 与所述膜的第二表面接触的第二电催化剂层; 与所述第一电催化剂层接触的第一金属网和与所述第二电催化剂层接触的第二金属网。

7. 发明申请

WO2012168130A1 STABLE ION EXCHANGE FLUORINATED POLYMERS AND MEMBRANES OBTAINED THEREFROM 审中-公开
标题翻译：稳定的离子交换荧光聚合物和其获得的膜
公开(公告)号：WO2012168130A1
公开(公告)日：2012-12-13
申请号：PCT/EP2012/060212
申请日：2012-05-31
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.p.A. , AVATANEO, Marco , OLDANI, Claudio , MARCHIONNI, Giuseppe
发明人： AVATANEO, Marco , OLDANI, Claudio , MARCHIONNI, Giuseppe
IPC分类号： H01M8/10 , C08J5/22
CPC分类号： H01M8/1039 , B01D71/32 , C08J5/225 , C08J2327/18 , C08K5/1565 , H01M8/1018 , H01M2300/0082 , H01M2300/0091 , Y02E60/521
摘要： A composition comprising at least one fluorinated polymer comprising -SO 2 X functional groups, wherein X is selected from X' or from OM and wherein X' is selected from the group consisting of F, CI, Br, I and M is selected from the group consisting of H, alkaline metals, NH4, and at least one fluorinated aromatic compound. Ion conducting membranes comprising the composition have improved resistance towards radical degradation in fuel cell applications.
摘要翻译：一种组合物，其包含至少一种包含-SO 2 X官能团的氟化聚合物，其中X选自X'或选自OM，并且其中X'选自F，Cl，Br，I和M，其选自的H，碱金属，NH 4和至少一种氟化芳族化合物。包含该组合物的离子导电膜对燃料电池应用中的自由基降解具有改进的抗性。

8. 发明申请

WO2012098146A1 LIQUID COMPOSITIONS OF FLUORINATED ANION EXCHANGE POLYMERS 审中-公开
标题翻译：氟化阴离子交换聚合物的液体组合物
公开(公告)号：WO2012098146A1
公开(公告)日：2012-07-26
申请号：PCT/EP2012/050687
申请日：2012-01-18
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A. , PETRICCI, Silvia , GUARDA, Pier Antonio , OLDANI, Claudio , MARCHIONNI, Giuseppe
发明人： PETRICCI, Silvia , GUARDA, Pier Antonio , OLDANI, Claudio , MARCHIONNI, Giuseppe
IPC分类号： C09D127/12 , C08F8/32 , C08F8/44 , C08J3/09 , C08J3/11
CPC分类号： C08L29/10 , B01J31/08 , C08F8/44 , C08J5/20 , C08J5/2237 , C08J5/225 , C08J2327/12 , C09D127/12
摘要： A liquid composition comprising: - a liquid medium comprising at least one aprotic polar organic solvent and less than 25 wt% based on the total weight of the composition of an alcohol; and - at least 5 wt% based on the total weight of the composition of at least one fluorinated anion exchange polymer comprising a fluorocarbon backbone and side-chains covalently attached to the backbone having terminal groups of formula (I): -SO 2 NR 1 Q + X - , wherein Q + is a group comprising at least one quaternary nitrogen atom, and R 1 is H or a C 1 -C 20 alkyl group, or forms a ring together with a group in Q + , wherein the ring contains 2 to 10 carbon atoms and, optionally, up to 4 heteroatoms; and X - is an anion selected among the group consisting of organic anions and lipophilic inorganic anions is disclosed. The liquid composition is suitable for the preparation of ion exchange membranes and as binders for electrocatalytic layers for use in electrochemical applications.
摘要翻译：一种液体组合物，其包含：液体介质，其包含至少一种非质子极性有机溶剂，并且基于所述组合物的总重量小于25重量％; 和 - 至少5重量％，基于组合物的至少一种氟化阴离子交换聚合物的总重量，所述氟化阴离子交换聚合物包含氟碳骨架和共价连接到具有式（I）的端基的主链的侧链：-SO 2 NR1Q + X - 其中Q +是包含至少一个季氮原子的基团，并且R 1是H或C 1 -C 20烷基，或与Q +中的基团一起形成环，其中所述环含有2至10个碳原子，并且任选地为上至4个杂原子; 并且X-是选自有机阴离子和亲脂性无机阴离子的阴离子。液体组合物适用于制备离子交换膜和用作电化学应用中的电催化层的粘合剂。

9. 发明申请

WO2012041821A1 A COMPOSITE POLYMERIZATION INITIATOR AND POLYMER BRUSH COMPOSITE OBTAINED THEREFROM 审中-公开
标题翻译：复合聚合反应器和聚合物刷组合物
公开(公告)号：WO2012041821A1
公开(公告)日：2012-04-05
申请号：PCT/EP2011/066708
申请日：2011-09-27
申请人： SOLVAY SPECIALTY POLYMERS ITALY S.P.A. , AVATANEO, Marco , MARCHIONNI, Giuseppe , DENISOV, Evgeny , LIN, Shiow-Ching , SPADA, Fabrizio , KENT, Bradley, Lane
发明人： AVATANEO, Marco , MARCHIONNI, Giuseppe , DENISOV, Evgeny , LIN, Shiow-Ching , SPADA, Fabrizio , KENT, Bradley, Lane
IPC分类号： C07F7/12 , C08F220/14
CPC分类号： C07F19/00 , C07B2200/11 , C07F7/12 , C08F14/22 , C08F20/14
摘要： Composite polymerization initiators are disclosed suitable to prepare polymer brush composites. The composite initiators comprise groups of formula (1): -(L) n -CR 2 -B(R B1 ) 2 covalently anchored to the surface of a solid substrate. Disclosed are also a process for the preparation of the composite polymerization initiator as well as the polymerization process providing a polymer brush composite from said composite initiator.
摘要翻译：公开了适用于制备聚合物刷复合材料的复合聚合引发剂。复合引发剂包括共价键合到固体底物表面的式（1）基团： - （L）n-CR 2 -B（RB 1）2。还公开了制备复合聚合引发剂的方法以及从所述复合引发剂提供聚合物刷复合物的聚合方法。

10. 发明申请

WO2010003931A1 PROCESS FOR THE MANUFACTURE OF FLUOROSURFACTANTS 审中-公开
标题翻译：制造氟化物的方法
公开(公告)号：WO2010003931A1
公开(公告)日：2010-01-14
申请号：PCT/EP2009/058536
申请日：2009-07-07
申请人： SOLVAY SOLEXIS S.p.A. , MARCHIONNI, Giuseppe , TORTELLI, Vito
发明人： MARCHIONNI, Giuseppe , TORTELLI, Vito
IPC分类号： C07C59/135 , C07C51/04
CPC分类号： C07C51/04 , C07C51/367 , C07C51/412 , C07C51/58 , C07C59/135
摘要： This invention pertains to a novel process for the manufacture of a perfluorooxycarboxylate of formula (I): R f O-CF 2 CF 2 -O-CF 2 -COOX a (I) wherein R f is a perfluoro(oxy)alkyl group, and Xa is H, a monovalent metal or an ammonium group of formula NR N 4 , with R N , equal or different at each occurrence, being H or a C 1-6 hydrocarbon group, said process comprising: (A) reacting a perfluorovinylether of formula R f -O-CF=CF 2 with an ethylene glycol derivative selected among ethylene glycol (HO-CH 2 CH 2 -OH), glycolic acid (HO-CH 2 -COOH), glycolaldheyde (HO-CH 2 -CHO) and protected derivatives thereof, so as to yield the corresponding addition product of formula R f -O-CFH-CF 2 -O-CH 2 -E, with R f having the same meaning as above detailed, and E being selected among -CH 2 OH, -COOH and -CHO; (B) optionally protecting functional group E with suitable chemistry; (C) fluorinating said (protected) addition product to yield the corresponding perfluorinated addition product; (D) optionally deprotecting said perfluorinated addition product to yield corresponding acyl fluoride of formula R f -O-CF 2 -CF 2 -O-CF 2 -C(O)F; (E) hydrolyzing and, optionally, neutralizing, said acyl fluoride for yielding the perfluorooxycarboxylate of formula (I).
摘要翻译：本发明涉及制备式（I）的全氟氧化羧酸酯的新方法：RfO-CF 2 CF 2 -O-CF 2 -COOa（I）其中Rf是全氟（氧）烷基，Xa是H，一价金属或NRN 4的铵基团，其中RN在每次出现时相同或不同，为H或C 1-6烃基，所述方法包括：（A）使式Rf-O-CF = CF 2的全氟乙烯基醚与选自乙二醇（HO-CH 2 CH 2 -OH），乙醇酸（HO-CH 2 -COOH），乙二醇醛（HO-CH2-CHO）及其保护的衍生物的乙二醇衍生物，得到相应的式Rf- O-CFH-CF2-O-CH2-E，其Rf具有与上述相同的含义，E选自-CH 2 OH，-COOH和-CHO; （B）任选地用合适的化学保护官能团E; （C）氟化所述（保护）加成产物以产生相应的全氟化加成产物; （D）任选地使所述全氟化加成产物脱保护，得到相应的式Rf-O-CF2-CF2-O-CF2-C（O）F的酰基氟; （E）水解和任选地中和所述酰氟以产生式（I）的全氟氧基羧酸酯。

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