会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 7. 发明申请
    • PRESSURE STEPPED MICROWAVE ASSISTED DIGESTION
    • 压力微波辅助消毒
    • US20110036705A1
    • 2011-02-17
    • US12541262
    • 2009-08-14
    • David A. BarclayJoseph J. LambertWilliam E. JenningsDavid L. Herman
    • David A. BarclayJoseph J. LambertWilliam E. JenningsDavid L. Herman
    • B01J19/12H05B6/64B65D51/16
    • G01N1/44B01J19/126B01J2219/0801B01J2219/0871B01J2219/0877B01J2219/089B01J2219/1215B01J2219/1233B01J2219/1236B01J2219/1242B01J2219/1275H05B6/6447H05B6/806
    • An instrument and method for high pressure microwave assisted chemistry are disclosed. The method includes the steps of applying microwave radiation to a sample in a sealed vessel while measuring the temperature of the sample and measuring the pressure generated inside the vessel and until the measured pressure reaches a designated set point, opening the vessel to release gases until the pressure inside the vessel reaches a lower designated set point, closing the vessel, and repeating the steps of opening the vessel at designated pressure set points and closing the vessel at designated pressure set points to the sample until the sample reaction reaches a designated high temperature. The designated set points can controllably differ from one another as the reaction proceeds. Microwave energy can be applied continuously or intermittently during the opening and closing steps. The apparatus includes a microwave cavity, a microwave transparent pressure resistant reaction vessel in the cavity, a cap on the reaction vessel, a pressure sensor for measuring pressure in the vessel, a temperature sensor, and means for opening and closing the cap at predetermined pressure set points measured by the pressure sensor to release pressure from the vessel.
    • 公开了一种用于高压微波辅助化学的仪器和方法。 该方法包括以下步骤:在测量样品的温度并测量容器内部产生的压力并直到测量的压力达到指定的设定点,将微波辐射施加到密封容器中的样品中,打开容器释放气体直至 容器内的压力达到下指定设定点,关闭容器,并重复在指定压力设定点打开容器的步骤,并在指定的压力设定点关闭容器至样品,直到样品反应达到指定的高温。 当反应进行时,指定的设定点可以彼此可控地不同。 微波能量可以在打开和关闭步骤期间连续或间歇地施加。 该装置包括微波空腔,空腔中的微波透明耐压反应容器,反应容器上的盖,用于测量容器压力的压力传感器,温度传感器以及用于以预定压力打开和关闭盖的装置 由压力传感器测量的设定点以释放来自容器的压力。