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1. 发明申请

US20070240609A1 Photoinitiators 有权
公开(公告)号：US20070240609A1
公开(公告)日：2007-10-18
申请号：US11578595
申请日：2005-04-11
申请人： Rinaldo Husler , Thomas Horni , Andre Fuchs , Tunja Jung , Reinhard Sommerlade
发明人： Rinaldo Husler , Thomas Horni , Andre Fuchs , Tunja Jung , Reinhard Sommerlade
IPC分类号： D21H17/07 , C08F2/48 , C08J3/28
CPC分类号： C07C45/46 , B33Y70/00 , C07C45/58 , C07C45/63 , C07C45/64 , C07C45/71 , C07C45/74 , C07C49/792 , C07C49/82 , C07C49/83 , C07C49/84 , C07C69/96 , C07C271/12 , C07C317/24 , C07D295/108 , C07D295/112 , C07D493/08 , C08F2/50 , C07C49/76 , C07C49/80 , C07C49/813
摘要： The invention relates to novel photoinitators of formulae (V), (II), (III), (IV), (V) and (VI) wherein R1 and R2 are each independently of the other C1-C8alkyl; C1-C4alkyl substituted by OH, C1-C4alkoxy, —COO(C1-C8alkyl), (C1-C4alkyl)-COO—, —CN, benzyl, phenyl or by —N(R15)(R16); C3-C6alkerlyl, benzyl, —CH2—C6H4—(C1-C4alkyl) or phenyl; or R1 and R2 together are unbranched or branched C2-C9alkylene or C3-C6-oxa- or -azaalkylene; R3, R4, R5 and R6 are each independently of the others hydrogen, C1-C8alkyl, C3-C6alkenyl, benzyl, —CH2—C6H4—(C1-C4alkyl) or phenyl; R3 and R4 together and/or R5 and R6 together are unbranched or branched C2-C9alkylene; A is Cl, Br, —O—R9, —N(R11)(R12) or —S—R18, A′ is —O—, —NH— or —NR11—; A″ is Cl, Br, —O—R9, —N(R11)(R12) or —S—R18 or hydrogen, X is —O—R10 or —N(R13)(R14), n is an integer from 1 to 10, preferably an integer from 1 to 4, especially 1, 2 or 3; R7 is a linker; R8 is a bivalent C2-C3alkylele radical.

2. 发明申请

US20060241323A1 Process for the preparation of 1-phenylindan photoinitiators 有权
标题翻译： 1-苯基吲哚类光引发剂的制备方法
公开(公告)号：US20060241323A1
公开(公告)日：2006-10-26
申请号：US10553777
申请日：2004-04-26
申请人： Rinaldo Husler , Thomas Horni
发明人： Rinaldo Husler , Thomas Horni
IPC分类号： C07C45/46
CPC分类号： C08F2/50 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/81 , C07C49/792 , C07C49/813 , C07C49/83
摘要： The invention relates to a process for the preparation of a crystalline isomeric mixture of compounds of formulae (I) and (II) which process comprises the following steps: a) the slow addition of aluminium chloride, in portions, to a solution comprising 1,1,3-trimethyl-3-phenylindan and isobutyric acid halide in a suitable solvent at a reaction temperature of from −20° C. to 20° C., an isomeric mixture consisting of compounds of formulae (Ia) and (IIa) being obtained; b) enol chlorination of compounds (Ia) and (IIa), an isomeric mixture consisting of compounds of formulae (Ib) and (IIb) being obtained; c) hydrolysis of the chlorinated isomeric mixture from step b). The invention relates also to the preparation of the individual compounds (I) and (II).
摘要翻译：本发明涉及一种制备式（I）和（II）化合物的结晶异构体混合物的方法，该方法包括以下步骤：a）将氯化铝缓慢加入到包含1， 1,3-二甲基-3-苯基茚基和异丁酸卤化物在合适的溶剂中，在-20℃至20℃的反应温度下，由式（Ia）和（IIa）化合物组成的异构体混合物为获得; b）化合物（Ia）和（IIa）的烯醇氯化，得到由式（Ib）和（IIb）的化合物组成的异构体混合物; c）步骤b）中氯化异构体混合物的水解。本发明还涉及单个化合物（I）和（II）的制备。

3. 发明授权

US07307192B2 Process for the preparation of 1-phenylindan photoinitiators 有权
标题翻译： 1-苯基吲哚类光引发剂的制备方法
公开(公告)号：US07307192B2
公开(公告)日：2007-12-11
申请号：US10553777
申请日：2004-04-26
申请人： Rinaldo Hüsler , Thomas Horni
发明人： Rinaldo Hüsler , Thomas Horni
IPC分类号： C07C45/00
CPC分类号： C08F2/50 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/81 , C07C49/792 , C07C49/813 , C07C49/83
摘要： The invention relates to a process for the preparation of a crystalline isomeric mixture of compounds of formulae (I) and (II) which process comprises the following steps: a) the slow addition of aluminium chloride, in portions, to a solution comprising 1,1,3-trimethyl-3-phenylindan and isobutyric acid halide in a suitable solvent at a reaction temperature of from −20° C. to 20° C., an isomeric mixture consisting of compounds of formulae (Ia) and (IIa) being obtained; b) enol chlorination of compounds (Ia) and (IIa), an isomeric mixture consisting of compounds of formulae (Ib) and (IIb) being obtained; c) hydrolysis of the chlorinated isomeric mixture from step b). The invention relates also to the preparation of the individual compounds (I) and (II).
摘要翻译：本发明涉及一种制备式（I）和（II）化合物的结晶异构体混合物的方法，该方法包括以下步骤：a）将氯化铝缓慢加入到包含1， 1,3-二甲基-3-苯基茚基和异丁酸卤化物在合适的溶剂中，在-20℃至20℃的反应温度下，由式（Ia）和（IIa）化合物组成的异构体混合物为获得; b）化合物（Ia）和（IIa）的烯醇氯化，得到由式（Ib）和（IIb）的化合物组成的异构体混合物; c）步骤b）中氯化异构体混合物的水解。本发明还涉及单个化合物（I）和（II）的制备。

4. 发明授权

US07642296B2 Photoinitiators 有权
标题翻译：光引发剂
公开(公告)号：US07642296B2
公开(公告)日：2010-01-05
申请号：US11578595
申请日：2005-04-11
申请人： Rinaldo Hüsler , Thomas Horni , André Fuchs , Tunja Jung , Reinhard H. Sommerlade
发明人： Rinaldo Hüsler , Thomas Horni , André Fuchs , Tunja Jung , Reinhard H. Sommerlade
IPC分类号： C08F2/50 , C03C25/10 , C07C49/84
CPC分类号： C07C45/46 , B33Y70/00 , C07C45/58 , C07C45/63 , C07C45/64 , C07C45/71 , C07C45/74 , C07C49/792 , C07C49/82 , C07C49/83 , C07C49/84 , C07C69/96 , C07C271/12 , C07C317/24 , C07D295/108 , C07D295/112 , C07D493/08 , C08F2/50 , C07C49/76 , C07C49/80 , C07C49/813
摘要： The invention relates to novel photoinitators of formulae (I), (II), (III), (IV), (V) and (VI) wherein R1 and R2 are each independently of the other C1-C8alkyl; C1-C4alkyl substituted by OH, C1-C4alkoxy, —COO(C1-C8alkyl), (C1-C4alkyl)-COO—, —CN, benzyl, phenyl or by —N(R15)(R16); C3-C6alkerlyl, benzyl, —CH2—C6H4—(C1-C4alkyl) or phenyl; or R1 and R2 together are unbranched or branched C2-C9alkylene or C3-C6-oxa- or -azaalkylene; R3, R4, R5 and R6 are each independently of the others hydrogen, C1-C8alkyl, C3-C6alkenyl, benzyl, —CH2—C6H4—(C1-C4alkyl) or phenyl; R3 and R4 together and/or R5 and R6 together are unbranched or branched C2-C9alkylene; A is CI, Br, —O—R9, —N(R11)(R12) or —S—R18, A′ is —O—, —NH— or —NR11—; A″ is CI, Br, —O—R9, —N(R11)(R12) or —S—R18 or hydrogen, X is —O—R10 or —N(R13)(R14), n is an integer from 1 to 10, preferably an integer from 1 to 4, especially 1, 2 or 3; R7 is a linker; R8 is a bivalent C2-C3alkylele radical.
摘要翻译：本发明涉及式（I），（II），（III），（IV），（V）和（VI）的新型光引发剂，其中R 1和R 2各自独立地为C 1 -C 8烷基; 被OH，C1-C4烷氧基，-COO（C1-C8烷基），（C1-C4烷基）-COO-，-CN，苄基，苯基或-N（R15）（R16）取代的C1-C4烷基; C3-C6链烯基，苄基，-CH2-C6H4-（C1-C4烷基）或苯基; 或R 1和R 2一起是非支链或支链C 2 -C 9亚烷基或C 3 -C 6 - 氧杂 - 或 - 亚烷基; R 3，R 4，R 5和R 6各自独立地为氢，C 1 -C 8烷基，C 3 -C 6烯基，苄基，-CH 2 -C 6 H 4 - （C 1 -C 4烷基）或苯基; R 3和R 4一起和/或R 5和R 6一起是非支链或支链C 2 -C 9亚烷基; A是Cl，Br，-O-R9，-N（R11）（R12）或-S-R18，A'是-O - ， - NH-或-NR11-; A“是Cl，Br，-O-R9，-N（R11）（R12）或-S-R18或氢，X是-O-R10或-N（R13）（R14），n是 1至10，优选1至4的整数，特别是1,2或3; R7是连接体; R8是二价C2-C3烷基基团。

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