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1. 发明授权

US5977357A Phenyl alkyl ketone substituted by cyclic amine and a process for the preparation thereof 失效
标题翻译：由环胺取代的苯基烷基酮及其制备方法
公开(公告)号：US5977357A
公开(公告)日：1999-11-02
申请号：US88218
申请日：1998-06-01
申请人： Rinaldo Husler , Rudolf Schwabe , Reto Luisoli
发明人： Rinaldo Husler , Rudolf Schwabe , Reto Luisoli
IPC分类号： C07D295/10 , C07D211/14 , C07D241/04 , C07D265/28 , C07D265/30 , C07D295/112 , C07D295/12 , C07D295/135 , C08F2/50 , G03F7/028 , G03F7/031 , C07D207/04 , C07D211/32 , C07D233/04
CPC分类号： C07D295/112 , C07D295/135 , C08F2/50 , G03F7/028 , G03F7/031
摘要： A novel process for the preparation of compounds of formula I ##STR1## by aminolysis of a p-halophenyl alkyl ketone of formula II ##STR2## with a cyclic amine of formula III ##STR3## in water at a temperature of at least 130.degree. C., in which formulae X is a halogen atom and R.sub.1, R.sub.2 and R.sub.3 are as claimed in claim 1, as well as the novel compounds of formula I and their use for the preparation of photoinitiators for the photopolymerisation of ethylenically unsaturated compounds.
摘要翻译：通过式II的对卤代苯基烷基酮与式III的环胺在水中在至少130℃的温度下氨基分解来制备式I化合物的新方法，其中式X是卤素原子和R 1，R 2和R 3如权利要求1所述，以及式I的新化合物及其用于制备用于烯属不饱和化合物的光聚合的光引发剂的用途。

2. 发明授权

US5795985A Phenyl alkyl ketone substituted by cyclic amine and a process for the preparation thereof 失效
标题翻译：由环胺取代的苯基烷基酮及其制备方法
公开(公告)号：US5795985A
公开(公告)日：1998-08-18
申请号：US847519
申请日：1997-04-21
申请人： Rinaldo Husler , Rudolf Schwabe , Reto Luisoli
发明人： Rinaldo Husler , Rudolf Schwabe , Reto Luisoli
IPC分类号： C07D295/10 , C07D211/14 , C07D241/04 , C07D265/28 , C07D265/30 , C07D295/112 , C07D295/12 , C07D295/135 , C08F2/50 , G03F7/028 , G03F7/031 , C07D295/116 , C07C221/00 , C07C225/16 , C07C225/22
CPC分类号： C07D295/112 , C07D295/135 , C08F2/50 , G03F7/028 , G03F7/031
摘要： A novel process for the preparation of compounds of formula I ##STR1## by aminolysis of a p-halophenyl alkyl ketone of formula II ##STR2## with a cyclic amine of formula III ##STR3## in water at a temperature of at least 130.degree. C., in which formulae X is a halogen atom and R.sub.1, R.sub.2 and R.sub.3 are as claimed in claim 1, as well as the novel compounds of formula I and their use for the preparation of photoinitiators for the photopolymerisation of ethylenically unsaturated compounds.
摘要翻译：通过将式II的对卤代苯基烷基酮（II）与式III的环胺（III）在水中的分解将式I化合物（I）制备的新方法在至少130℃的温度下，其中式X是卤素原子，R 1，R 2和R 3如权利要求1所述，以及式I的新化合物及其用于制备光引发剂的用途烯属不饱和化合物的光聚合。

3. 发明申请

US20050004249A1 Novel disfunctional photoinitiators 有权
标题翻译：新型失活光引发剂
公开(公告)号：US20050004249A1
公开(公告)日：2005-01-06
申请号：US10494593
申请日：2002-10-31
申请人： Andre Fuchs , Rinaldo Husler , Christian Schregenberger , Martin Kunz
发明人： Andre Fuchs , Rinaldo Husler , Christian Schregenberger , Martin Kunz
IPC分类号： C07B61/00 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/66 , C07C45/81 , C07C49/83 , C08F2/50 , C09D7/12 , C09D11/00 , C09D201/00 , G03F7/031 , C08F2/46 , C07C45/00 , C07C49/213 , C07C49/225 , C07C49/563 , C07C49/76 , C08J3/28
CPC分类号： G03F7/031 , B33Y70/00 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/81 , C07C49/83 , C08F2/50 , C07C49/784 , C07C49/813
摘要： The invention relates to α-hydroxy ketones of formula I or IIa; or mixtures of compounds of formula I and II; or mixtures of compounds of formulae Ia and IIa
摘要翻译：本发明涉及式I或IIa的α-羟基酮; 或式I和II化合物的混合物; 或式Ia和IIa化合物的混合物

4. 发明授权

US5306600A Oxygen-containing titanocenes, and the use thereof 失效
标题翻译：含氧二茂钛及其用途
公开(公告)号：US5306600A
公开(公告)日：1994-04-26
申请号：US975042
申请日：1992-11-12
申请人： Eginhard Steiner , Harry Beyeler , Martin Riediker , Vincent Desobry , Kurt Dietliker , Rinaldo Husler
发明人： Eginhard Steiner , Harry Beyeler , Martin Riediker , Vincent Desobry , Kurt Dietliker , Rinaldo Husler
IPC分类号： C07F7/28 , C07F17/00 , C08F2/50 , C09D4/00 , G03F7/029
CPC分类号： C07F17/00 , C08F2/50 , G03F7/029 , Y10S430/124 , Y10S430/148 , Y10S526/943
摘要： Titanocenes of the formula I ##STR1## in which R.sup.1 are cyclopentadienyl.sup..crclbar. groups and R.sup.2 and R.sup.3 are aromatic radicals which are substituted in both ortho-positions by fluorine and, in addition, are substituted by an acyloxy group are suitable as photoinitiators for the photopolymerization of ethylenically unsaturated compounds.
摘要翻译：其中R 1是环戊二烯基（ - ）基团并且R 2和R 3是在两个邻位被氟取代并且被酰氧基取代的芳族基团的式I化合物（I）的十六碳烯是合适的作为烯属不饱和化合物的光聚合的光引发剂。

5. 发明授权

US5210110A Silylated acylphosphine oxides 失效
标题翻译：苯乙烯磷酰氧化物
公开(公告)号：US5210110A
公开(公告)日：1993-05-11
申请号：US793759
申请日：1991-11-18
申请人： Werner Rutsch , Rinaldo Husler
发明人： Werner Rutsch , Rinaldo Husler
IPC分类号： C07F9/53 , C07F9/32 , C07F9/40 , C07F9/6596 , C08F2/50 , C08J7/04 , C08K5/53 , C08K5/5397 , C08L23/00 , G03C1/06 , G03F7/029 , G03F7/075
CPC分类号： C07F9/3294 , C07F9/409 , C07F9/6596 , C08F2/50 , G03F7/029 , G03F7/0755
摘要： Silylated acylphosphine oxides of formula I ##STR1## in which R.sub.1, R.sub.2 and R.sub.3 are defined in the specification, are highly suitable as photoinitiators for the photopolymerization of compounds which can be polymerized by means of free radicals, namely ethylenically unsaturated compounds.
摘要翻译：式I中的R 1，R 2和R 3在本说明书中定义的式（I）的甲硅烷基酰基氧化膦非常适合作为可通过自由基即烯属不饱和化合物聚合的化合物的光聚合的光引发剂。

6. 发明授权

US4739052A Phenyl ketone derivatives 失效
标题翻译：苯基酮衍生物
公开(公告)号：US4739052A
公开(公告)日：1988-04-19
申请号：US783377
申请日：1985-10-02
申请人： Rinaldo Husler , Rudolf Kirchmayr , Werner Rutsch
发明人： Rinaldo Husler , Rudolf Kirchmayr , Werner Rutsch
IPC分类号： C07D319/24 , C07C45/46 , C07C45/63 , C07C49/84 , C07C67/00 , C07C225/16 , C07C225/18 , C07C229/38 , C07C235/72 , C07C255/13 , C07C301/00 , C07C309/63 , C07D217/20 , C07D265/30 , C07D295/10 , C07D295/108 , C07D303/48 , C07D307/91 , C07F7/18 , C08F2/00 , C08F2/50 , C09D11/10 , G03F7/031 , C07C97/10
CPC分类号： C07D295/108 , C07C45/46 , C07C45/63 , C07C49/84 , C07D303/48 , C07D307/91 , C08F2/50 , G03F7/031
摘要： Compounds of the formula I, II or III ##STR1## in which Ar and Ar' are an oxygen-containing aromatic radical, R.sup.1 and R.sup.2 are a monovalent hydrocarbon radical which is substituted or unsubstituted, or R.sup.1 and R.sup.2 together form alkylene, oxaalkylene or azaalkylene, R.sup.3 is a direct bond or a divalent hydrocarbon radical, X and X' are a monovalent amino group and Y is a divalent amino or diamino group, are excellent photoinitiators for the photocuring of colored, especially pigmented, compositions containing an olefinically unsaturated, photopolymerizable binder.
摘要翻译：其中Ar和Ar'是含氧芳族基团的式I，II或III化合物其中R 1和R 2是一价烃基，其中是取代或未取代的，或者R 1和R 2一起形成亚烷基，氧杂亚烷基或氮杂亚烷基，R 3是直接键或二价烃基，X和X'是一价氨基，Y是二价氨基或二氨基，是优异的光引发剂用于对含有烯属不饱和的可光聚合粘合剂的着色的，特别是着色的组合物进行光固化。

7. 发明申请

US20060270748A1 Novel trifunctional photoinitiators 有权
公开(公告)号：US20060270748A1
公开(公告)日：2006-11-30
申请号：US10552952
申请日：2004-05-04
申请人： Reinhard Sommerlade , Rinaldo Husler , Stephen Ilg , Andre Fuchs , Souad Boulmaaz , Jean-Luc Birbaum
发明人： Reinhard Sommerlade , Rinaldo Husler , Stephen Ilg , Andre Fuchs , Souad Boulmaaz , Jean-Luc Birbaum
IPC分类号： C08F2/50
CPC分类号： G03F7/0295 , B33Y70/00 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/71 , C07C49/784 , C07C49/813 , C07C49/83 , C07C49/84 , C07C225/22 , C07C271/20 , C07C2601/14 , C08F2/50 , G03F7/029 , G03F7/031
摘要： The Invention relates to novel ketones of formulae (I) and (II) wherein R1, R2, R3 and R4 are, for example, C1-C8alkyl, R5 is, for example, hydrogen, A is CI, Br, -0-R7, —NR8R9 or —S—R16, A′ is —O—, —NH— or —NR8—, X and Y are each independently of the other —O—R10 or —N(R11)(R12), n is an integer from 1 to 10, R6 is, for example, an n-valent radical of linear or branched C2-C20alkyl the carbon chain of which may be interrupted by cyclohexanediyl, phenylene, —CH(OH)—, —C(C2H5)(CH2—CH2—OH)—, —C(CH3)(CH2—CH2—OH)—, —C(CH2—CH2—OH)2—, —N(CH3)—, —N(C2H5)—, —N(CH2—CH2—OH)—, —CO—O—, —O—CO—, —P(CH2—CH2—OH)—, —P(O)(CH2—CH2—OH)—, -0-P(O—CH2—CH2—OH)—O—, -0-P(O)(0-CH2—CH2—OH)—O—, —O-cyclohexanediyl-C(CH3)2-Cyclohexanediyl-O—, —O-phenylene-C(CH3)2-phenylene-O—, —O-phenylene-CH2-phenylene-O—, —Si(CH3)2—, -0-Si(CH3)2—O—, —O—Si(CH3)(0-CH3)—O—, —Si(CH3)(R17)—O—Si(CH3)(R18)—, 5-(2-hydroxyethyl)-[1,3,5]triazinane-2,4,6-trione-1,3-diyl and/or by from one to nine oxygen atoms.

8. 发明申请

US20060241323A1 Process for the preparation of 1-phenylindan photoinitiators 有权
标题翻译： 1-苯基吲哚类光引发剂的制备方法
公开(公告)号：US20060241323A1
公开(公告)日：2006-10-26
申请号：US10553777
申请日：2004-04-26
申请人： Rinaldo Husler , Thomas Horni
发明人： Rinaldo Husler , Thomas Horni
IPC分类号： C07C45/46
CPC分类号： C08F2/50 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/81 , C07C49/792 , C07C49/813 , C07C49/83
摘要： The invention relates to a process for the preparation of a crystalline isomeric mixture of compounds of formulae (I) and (II) which process comprises the following steps: a) the slow addition of aluminium chloride, in portions, to a solution comprising 1,1,3-trimethyl-3-phenylindan and isobutyric acid halide in a suitable solvent at a reaction temperature of from −20° C. to 20° C., an isomeric mixture consisting of compounds of formulae (Ia) and (IIa) being obtained; b) enol chlorination of compounds (Ia) and (IIa), an isomeric mixture consisting of compounds of formulae (Ib) and (IIb) being obtained; c) hydrolysis of the chlorinated isomeric mixture from step b). The invention relates also to the preparation of the individual compounds (I) and (II).
摘要翻译：本发明涉及一种制备式（I）和（II）化合物的结晶异构体混合物的方法，该方法包括以下步骤：a）将氯化铝缓慢加入到包含1， 1,3-二甲基-3-苯基茚基和异丁酸卤化物在合适的溶剂中，在-20℃至20℃的反应温度下，由式（Ia）和（IIa）化合物组成的异构体混合物为获得; b）化合物（Ia）和（IIa）的烯醇氯化，得到由式（Ib）和（IIb）的化合物组成的异构体混合物; c）步骤b）中氯化异构体混合物的水解。本发明还涉及单个化合物（I）和（II）的制备。

9. 发明授权

US4837350A Process for the preparation of benzoin sulfonates 失效
标题翻译：苯偶姻磺酸盐的制备方法
公开(公告)号：US4837350A
公开(公告)日：1989-06-06
申请号：US129574
申请日：1987-12-07
申请人： Werner Rutsch , Rinaldo Husler
发明人： Werner Rutsch , Rinaldo Husler
IPC分类号： C07D307/46 , C07B45/02 , C07C67/00 , C07C301/00 , C07C303/08 , C07C309/63 , C07C309/65 , C07C309/72 , C07C309/73 , C07C313/00 , C07C319/20 , C07C323/22 , C07C323/52 , C07C323/66
CPC分类号： C07C309/00 , C07B45/02
摘要： Benzoin esters of aromatic sulfonic acids can be obtained in high yield from benzoin and the respective sulfonyl halide in molar amounts of a base by carrying out the reaction at low temperature in an organic solvent with the addition of water. Aqueous NaOh or KOH can be used as base in this process.
摘要翻译：芳族磺酸的苯偶姻酯可以通过加入水在有机溶剂中通过在低温下进行反应而以高收率从苯偶姻和相应的磺酰卤以碱的摩尔量获得。 NaOh或KOH水溶液可用作本方法中的碱。

10. 发明授权

US4559371A Photocurable colored compositions employing alpha-amino phenone initiator 失效
标题翻译：使用α-氨基苯酮引发剂的光固化着色组合物
公开(公告)号：US4559371A
公开(公告)日：1985-12-17
申请号：US579622
申请日：1984-02-13
申请人： Rinaldo Husler , Rudolf Kirchmayr , Werner Rutsch
发明人： Rinaldo Husler , Rudolf Kirchmayr , Werner Rutsch
IPC分类号： C07D319/24 , C07C45/46 , C07C45/63 , C07C49/84 , C07C67/00 , C07C225/16 , C07C225/18 , C07C229/38 , C07C235/72 , C07C255/13 , C07C301/00 , C07C309/63 , C07D217/20 , C07D265/30 , C07D295/10 , C07D295/108 , C07D303/48 , C07D307/91 , C07F7/18 , C08F2/00 , C08F2/50 , C09D11/10 , G03F7/031
CPC分类号： C07D295/108 , C07C45/46 , C07C45/63 , C07C49/84 , C07D303/48 , C07D307/91 , C08F2/50 , G03F7/031
摘要： Compounds of the formula I, II or III ##STR1## in which Ar and Ar' are an oxygen-containing aromatic radical, R.sup.1 and R.sup.2 are a monovalent hydrocarbon radical which is substituted or unsubstituted, or R.sup.1 and R.sup.2 together form alkylene, oxaalkylene or azaalkylene, R.sup.3 is a direct bond or a divalent hydrocarbon radical, X and X' are a monovalent amino group and Y is a divalent amino or diamino group, are excellent photoinitiators for the photocuring of colored, especially pigmented, compositions containing an olefinically unsaturated, photopolymerizable binder.
摘要翻译：其中Ar和Ar'是含氧芳族基团的式I，II或III化合物其中R 1和R 2是一价烃基，其中是取代或未取代的，或者R 1和R 2一起形成亚烷基，氧杂亚烷基或氮杂亚烷基，R 3是直接键或二价烃基，X和X'是一价氨基，Y是二价氨基或二氨基，是优异的光引发剂用于对含有烯属不饱和的可光聚合粘合剂的着色的，特别是着色的组合物的光固化。

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