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1. 发明授权

US07261158B2 Coarse-foamed fracturing fluids and associated methods 有权
$Coarse-foamed fracturing fluids and associated methods$
标题翻译：粗发泡压裂液及相关方法
公开(公告)号：US07261158B2
公开(公告)日：2007-08-28
申请号：US11506703
申请日：2006-08-18
申请人： Richard L. Middaugh , Phillip C. Harris , Stanley J. Heath , Robert S. Taylor , Ottmar F. Hoch , Max L. Phillippi , Billy F. Slabaugh , John M. Terracina
发明人： Richard L. Middaugh , Phillip C. Harris , Stanley J. Heath , Robert S. Taylor , Ottmar F. Hoch , Max L. Phillippi , Billy F. Slabaugh , John M. Terracina
IPC分类号： E21B43/267
CPC分类号： C09K8/703
摘要： A method of fracturing a subterranean formation comprising the steps of: providing a coarse-foamed fracturing fluid comprising a liquid fracturing fluid component, a gas, proppant particulates, and a foaming agent; and placing the coarse-foamed fracturing fluid into a portion of a subterranean formation at a pressure sufficient to create or extend at least one fracture therein.
摘要翻译：一种压裂地下地层的方法，包括以下步骤：提供包含液体压裂液组分，气体，支撑剂颗粒和发泡剂的粗发泡压裂液; 以及将粗发泡压裂液置于足以产生或延伸其中的至少一个裂缝的压力下进入地层的一部分。

2. 发明授权

US5827804A Borate cross-linked well treating fluids and methods 失效
标题翻译：硼酸盐交联井处理液和方法
公开(公告)号：US5827804A
公开(公告)日：1998-10-27
申请号：US832886
申请日：1997-04-04
申请人： Phillip C. Harris , Michael A. McCabe , Lewis R. Norman , Ronald J. Powell , Chris E. Shuchart , Billy F. Slabaugh , John M. Terracina , Joseph G. Yaritz
发明人： Phillip C. Harris , Michael A. McCabe , Lewis R. Norman , Ronald J. Powell , Chris E. Shuchart , Billy F. Slabaugh , John M. Terracina , Joseph G. Yaritz
IPC分类号： C09K8/68 , C09K7/00 , F21B43/17
CPC分类号： C09K8/685 , Y10S507/904 , Y10S507/922
摘要： The present invention provides borate cross-linked well treating fluids and methods of preparing and using the fluids in treating wells such as fracturing subterranean zones therein. The improved cross-linked treating fluids are basically comprised of water, a hydrated galactomannan gelling agent and a borate composition for buffering the treating fluid and cross-linking the hydrated galactomannan gelling agent comprised of water, a soluble boron source and an alkanolamine or alkylamine.
摘要翻译：本发明提供了硼酸盐交联井处理流体以及在处理井中制备和使用流体的方法，例如在其中破裂地下区域。改进的交联处理流体基本上由水，水合半乳甘露聚糖胶凝剂和用于缓冲处理流体和交联由水，可溶性硼源和链烷醇胺或烷基胺组成的水合半乳甘露聚糖胶凝剂的硼酸盐组合物组成。

3. 发明授权

US06214773B1 High temperature, low residue well treating fluids and methods 有权
标题翻译：高温低残液处理液和方法
公开(公告)号：US06214773B1
公开(公告)日：2001-04-10
申请号：US09408059
申请日：1999-09-29
申请人： Phillip C. Harris , Stanley J. Heath , David M. Barrick , Ron J. Powell , Billy F. Slabaugh , Shane L. Milson , Gregory L. Tanaka , Harold G. Walters
发明人： Phillip C. Harris , Stanley J. Heath , David M. Barrick , Ron J. Powell , Billy F. Slabaugh , Shane L. Milson , Gregory L. Tanaka , Harold G. Walters
IPC分类号： C09K300
CPC分类号： C09K8/887 , C09K8/685 , Y10S507/903 , Y10S507/921 , Y10S507/922
摘要： Improved high temperature, low residue viscous well treating fluids and methods of using the fluids are provided by the present invention. The improved viscous well treating fluids are basically comprised of water; a hydrated galactomannan gelling agent; a retarded cross-linking composition for buffering the treating fluid and cross-linking the hydrated galactomannan gelling agent comprised of a liquid solvent, an organotitanate chelate and a borate ion producing compound; and a delayed gel breaker.
摘要翻译：本发明提供改进的高温，低残留粘稠井处理流体和使用流体的方法。改进的粘性井处理流体基本上由水组成; 水合半乳甘露聚糖胶凝剂; 用于缓冲处理流体并交联由液体溶剂，有机钛酸盐螯合物和产生硼酸根离子的化合物组成的水合半乳甘露聚糖胶凝剂的延迟交联组合物; 和延迟凝胶断路器。

4. 发明授权

US6024170A Methods of treating subterranean formation using borate cross-linking compositions 失效
标题翻译：使用硼酸盐交联组合物处理地层的方法
公开(公告)号：US6024170A
公开(公告)日：2000-02-15
申请号：US89531
申请日：1998-06-03
申请人： Michael A. McCabe , Phillip C. Harris , Billy Slabaugh , Ronald J. Powell , John M. Terracina , Joseph G. Yaritz , Chris E. Shuchart
发明人： Michael A. McCabe , Phillip C. Harris , Billy Slabaugh , Ronald J. Powell , John M. Terracina , Joseph G. Yaritz , Chris E. Shuchart
IPC分类号： C09K8/20 , C09K8/68 , E21B43/22 , E21B43/26
CPC分类号： C09K8/206 , C09K8/685 , Y10S507/901 , Y10S507/902 , Y10S507/903
摘要： The present invention provides improved methods of treating subterranean formations using borate cross-linking compositions and borate cross-linked well treating fluids. The borate cross-linking compositions are basically comprised of a low viscosity hydrocarbon liquid, an organophillic clay, a slightly water soluble borate, a buffer and a dispersing agent.
摘要翻译：本发明提供了使用硼酸盐交联组合物和硼酸盐交联井处理流体处理地下地层的改进方法。硼酸盐交联组合物基本上由低粘度烃液体，有机微生物粘土，微溶于水的硼酸盐，缓冲剂和分散剂组成。

5. 发明申请

US20100181070A1 Methods of designing treatment fluids based on solid-fluid interactions 有权
标题翻译：基于固体 - 液体相互作用设计处理液的方法
公开(公告)号：US20100181070A1
公开(公告)日：2010-07-22
申请号：US12321315
申请日：2009-01-16
申请人： Phillip C. Harris , Stanley J. Heath , Harold G. Walters
发明人： Phillip C. Harris , Stanley J. Heath , Harold G. Walters
IPC分类号： E21B43/267 , G01N31/00 , G01N11/00
CPC分类号： C09K8/80 , C09K8/04 , C09K8/42 , C09K8/665 , C09K8/685 , C09K8/703 , C09K8/805
摘要： Methods that comprise selecting proppant for use in a fracturing fluid based on one or more factors, wherein the one or more factors comprise an interaction between the proppant and the fracturing fluid. Methods that comprise designing a treatment fluid that comprises a gelled base fluid and a particulate based on one or more factors, wherein the one or more factors comprise an interaction between the particulate and the gelled base fluid.
摘要翻译：包括基于一种或多种因素选择用于压裂流体的支撑剂的方法，其中所述一种或多种因素包括支撑剂和压裂液之间的相互作用。包括基于一个或多个因素设计包含凝胶基础流体和颗粒的处理流体的方法，其中所述一个或多个因素包括所述颗粒和所述凝胶化基础流体之间的相互作用。

6. 发明授权

US5393810A Method and composition for breaking crosslinked gels 失效
标题翻译：断开交联凝胶的方法和组成
公开(公告)号：US5393810A
公开(公告)日：1995-02-28
申请号：US176165
申请日：1993-12-30
申请人： Phillip C. Harris , Stanley J. Heath
发明人： Phillip C. Harris , Stanley J. Heath
IPC分类号： C08K9/08 , C09K8/68 , C09K8/80 , E21B43/267 , C08K5/15 , C08K3/38 , C08L5/00 , E21B43/26
CPC分类号： C09K8/805 , C08K9/08 , C09K8/685 , E21B43/267 , C09K2208/26
摘要： Compositions and methods are provided which provide improved viscosity reduction of crosslinked hydratable polymer treating fluids in the presence of uncured resin-coated proppants. The uncured resins are generally uncured phenolic or furan resins. The breaker comprises an oxidizing agent to which is added a sequestering agent comprising a copolymer of vinylpyrrolidone and acrylic acid to sequester at least a portion of any phenolic extracts from said resin that may be present in said treating fluid from contact with the uncured resin.
摘要翻译：提供了组合物和方法，其在未固化的树脂涂覆的支撑剂存在下提供交联的可氢化聚合物处理流体的改进的粘度降低。未固化的树脂通常是未固化的酚或呋喃树脂。断路器包括氧化剂，向其中加入包含乙烯基吡咯烷酮和丙烯酸的共聚物的多价螯合剂以螯合所述处理流体中可能存在的与未固化的树脂接触的来自所述树脂的任何酚类提取物的至少一部分。

7. 发明申请

US20080139411A1 Methods of treating subterranean formations using hydrophobically modified polymers and compositions of the same 审中-公开
标题翻译：使用疏水改性聚合物及其组合物处理地下地层的方法
公开(公告)号：US20080139411A1
公开(公告)日：2008-06-12
申请号：US11635980
申请日：2006-12-07
申请人： Phillip C. Harris , Stanley J. Heath , Gary P. Funkhouser
发明人： Phillip C. Harris , Stanley J. Heath , Gary P. Funkhouser
IPC分类号： C09K8/00
CPC分类号： C09K8/685
摘要： Among the many embodiments provided by the invention, in one embodiment, a method is presented that comprises: providing a treating fluid comprising water, a charged polymer in an amount in the range of from about 2000 to about 20000 ppm, and a surfactant having a charge that is opposite to that of the charged polymer, the surfactant being capable of forming a micellar bond between a hydrophobic group on the polymer and a hydrophobic group on the same or an adjacent polymer molecule to form a crosslink; and placing the treating fluid into a well bore. Another embodiment provides a method that comprises: providing a viscosified treating fluid comprising: water; a charged polymer in an amount in the range of from about 2000 to about 20000 ppm; a surfactant having a charge that is opposite to that of the charged polymer; and at least one micellar association of between the surfactant with the charged polymer; and placing the viscosified treating fluid into a well bore.
摘要翻译：在本发明提供的许多实施方案中，在一个实施方案中，提出了一种方法，其包括：提供包含水，约2000至约20000ppm范围内的带电聚合物的处理流体，以及具有电荷与带电聚合物的电荷相反，表面活性剂能够在聚合物上的疏水基团和相同或相邻的聚合物分子上的疏水基团之间形成胶束键以形成交联; 并将处理流体放置在井眼中。另一个实施方案提供了一种方法，其包括：提供稠化处理流体，其包含：水; 一种带电聚合物，其量为约2000至约20000ppm; 具有与带电聚合物相反的电荷的表面活性剂; 和表面活性剂与带电聚合物之间的至少一个胶束缔合; 并将稠化的处理流体放入井眼中。

8. 发明授权

US07225874B2 Methods and compositions for reducing the viscosity of treatment fluids used in subterranean operations 有权
标题翻译：用于降低地下作业中使用的处理液粘度的方法和组合物
公开(公告)号：US07225874B2
公开(公告)日：2007-06-05
申请号：US11203045
申请日：2005-08-12
申请人： Phillip C. Harris , Stanley J. Heath
发明人： Phillip C. Harris , Stanley J. Heath
IPC分类号： E21B43/27 , E21B43/26
CPC分类号： C09K8/68 , C09K8/685 , C09K8/70 , C09K8/706
摘要： Methods and compositions for reducing the viscosity of subterranean treatment fluids that comprise a gelling agent utilizing breakers that comprise hydroquinone and/or a derivative thereof. In one embodiment, the present invention provides a method comprising: providing a treatment fluid that comprises an aqueous base fluid and a gelling agent; providing a breaker that comprises a hydroquinone component; allowing the breaker to interact with the treatment fluid; and allowing the breaker to at least partially reduce the viscosity of the treatment fluid.
摘要翻译：使用包含氢醌和/或其衍生物的断路器降低包含胶凝剂的地下处理流体粘度的方法和组合物。在一个实施方案中，本发明提供了一种方法，包括：提供包含基础水基和胶凝剂的处理流体; 提供包含氢醌组分的断路器; 允许断路器与处理流体相互作用; 并且允许断路器至少部分地降低处理流体的粘度。

9. 发明授权

US06782735B2 Testing device and method for viscosified fluid containing particulate material 有权
标题翻译：含有颗粒材料的粘稠液体的测试装置和方法
公开(公告)号：US06782735B2
公开(公告)日：2004-08-31
申请号：US10342173
申请日：2003-01-14
申请人： Harold G. Walters , Billy J. Slabaugh , Ronnie G. Morgan , Phillip C. Harris , Stanley J. Heath , Ronald J. Powell , David M. Barrick , Johnny W. Johnson
发明人： Harold G. Walters , Billy J. Slabaugh , Ronnie G. Morgan , Phillip C. Harris , Stanley J. Heath , Ronald J. Powell , David M. Barrick , Johnny W. Johnson
IPC分类号： G01N1114
CPC分类号： G01N11/14
摘要： A device and a method for testing a viscosified fluid containing particulate indicate when the particulate is in suspension within the fluid and when it is not. The device and method stir the fluid and particulate mixture for a time during which the viscosity of the fluid changes such that during a first period of the stirring time substantially all the particulate remains suspended in the fluid and during a second period of the stirring time substantially all the particulate settles out of suspension in the fluid. A signal is generated during the first and second periods such that the signal has a characteristic that changes from the first period to the second period to indicate the change in particle carrying ability of the fluid. Other characteristics, including crosslinking time, can also be determined. A test chamber includes interacting projections extending from the inner surface of a cup receiving the fluid and from an axial support extending into the fluid in the cup.
摘要翻译：用于测试含有颗粒的粘稠液体的装置和方法指示当颗粒在流体内悬浮时以及何时不是。该装置和方法搅拌流体和颗粒状混合物一段时间，在此期间流体的粘度发生变化，使得在搅拌时间的第一阶段，基本上所有的颗粒保持悬浮在流体中，并且在搅拌时间的第二时间段内基本上所有的颗粒都从液体中悬浮液中沉淀出来。在第一和第二周期期间产生信号，使得信号具有从第一周期到第二周期变化的特征，以指示流体的粒子承载能力的变化。还可以确定其他特征，包括交联时间。测试室包括从容纳流体的杯的内表面和延伸到杯中的流体的轴向支撑件延伸的相互作用的突起。

10. 发明授权

US5591700A Fracturing fluid with encapsulated breaker 失效
标题翻译：压裂液与封装破碎机
公开(公告)号：US5591700A
公开(公告)日：1997-01-07
申请号：US362393
申请日：1994-12-22
申请人： Phillip C. Harris , Ronald J. Powell , Stanley J. Heath
发明人： Phillip C. Harris , Ronald J. Powell , Stanley J. Heath
IPC分类号： C09K8/62 , C09K8/68 , C09K8/70 , C09K8/92 , E21B43/26
CPC分类号： C09K8/706 , C09K8/68 , C09K8/685
摘要： An aqueous fracturing fluid composition and method for fracturing subterranean formations penetrated by a well bore wherein the fracturing fluid comprises a viscosity breaker that comprises a surfactant and a breaker which is solid at ambient surface conditions and dissolves at temperatures in the formation.
摘要翻译：一种水力压裂流体组合物和用于压裂井眼的地下地层的压裂方法，其中压裂流体包括粘度破坏剂，其包含表面活性剂和在环境表面条件下为固体并在地层温度下溶解的破碎剂。

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