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1. 发明授权

US4335117A 1-Hydroxy-2,2,2-trichloroethane-thionophosphonic acid dimethyl esters as insecticide 失效
标题翻译： 1-羟基-2,2,2-三氯乙烷 - 硫代磷酸二甲酯作为杀虫剂
公开(公告)号：US4335117A
公开(公告)日：1982-06-15
申请号：US865084
申请日：1977-12-27
申请人： Reimer Colln , Wilhelm Sirrenberg , Wolfgang Behrenz , Wilhelm Stendel
发明人： Reimer Colln , Wilhelm Sirrenberg , Wolfgang Behrenz , Wilhelm Stendel
IPC分类号： A01N57/20 , A01N57/12 , A01P7/04 , C07F9/38 , C07F9/40
CPC分类号： A01N57/12 , C07F9/4006
摘要： 1-Hydroxy-2,2,2-trichloroethane-thionophosphonic acid dialkyl esters of the formula ##STR1## in which R and R.sub.1 each independently is an alkyl radical with 1 to 4 carbon atoms,which possess arthropodicidal properties.
摘要翻译：具有式（I）的1-羟基-2,2,2-三氯乙烷 - 硫代磷酸二烷基酯，其中R和R 1各自独立地是具有1〜4个碳原子的烷基，其具有节肢杀虫特性。

2. 发明授权

US4123478A Preparation of O, O-dimethyl-O-(2,2-dichlorovinyl)-thionophosphoric acid ester 失效
标题翻译：制备O，O-二甲基-O-（2,2-二氯乙烯基） - 硫代磷酸酯
公开(公告)号：US4123478A
公开(公告)日：1978-10-31
申请号：US820500
申请日：1977-07-29
申请人： Reimer Colln , Wilhelm Sirrenberg
发明人： Reimer Colln , Wilhelm Sirrenberg
IPC分类号： C07F9/173 , C07F9/165
CPC分类号： C07F9/173
摘要： A process for the preparation of O,O-dimethyl-O-(2,2-dichlorovinyl)-thionophosphoric acid ester of the formula ##STR1## comprising reacting O,O-dimethyl-1-hydroxy-2,2,2-trichloroethane-thionophosphonic acid ester of the formula ##STR2## in isopropanol with a 30-50% aqueous solution of an alkali metal hydroxide, possibly present in a small molar excess.
摘要翻译：制备式（I）的O，O-二甲基-O-（2,2-二氯乙烯基） - 硫代磷酸酯的方法，包括使O，O-二甲基-1-羟基-2,2，具有式（IMAGE）（II）的2-三氯乙烷 - 硫代磷酸酯在异丙醇中与30-50％的碱金属氢氧化物水溶液，可能以小摩尔过量存在。

3. 发明授权

US4127401A Aminomethanephosphonic acid compounds containing plant-growth regulant compositions 失效
标题翻译：含有植物生长调节剂组合物的氨基甲基膦酸化合物
公开(公告)号：US4127401A
公开(公告)日：1978-11-28
申请号：US770349
申请日：1977-02-22
申请人： Reimer Colln , Klaus Lurssen
发明人： Reimer Colln , Klaus Lurssen
IPC分类号： C07F9/38 , A01N9/36
CPC分类号： C07F9/3808
摘要： Plant-growth regulating compositions and methods having strong effects on plant growth, containing an aminomethanephosphonic acid composed of the formula ##STR1## in which R is an NH.sub.2 group or an --NH.sup..sym..sub.3 X.sup..crclbar. radical whereinX.sup..crclbar. is one equivalent of an anion of an organic or inorganic acid, andR' and R", which may be identical or different, are each alkyl of from 1 to 6 carbon atoms, one equivalent of an alkali metal or alkaline earth metal cation, one equivalent of a protonized nitrogen base or of a compound which contains an N.sup..sym. H.sub.3 group, or hydrogen, provided that R' and R" can simultaneously be hydrogen only if R is an --N.sup..sym. H.sub.3 X.sup..crclbar. radical.
摘要翻译：植物生长调节组合物和对植物生长具有强烈影响的方法，其含有由下式（I）组成的氨基甲烷膦酸，其中R是NH 2基或-NH（+）3 X（ - ）基，其中X（ - ）是有机或无机酸的阴离子的1当量，R'和R“可以相同或不同，分别为1至6个碳原子的烷基，1当量的碱金属或碱土金属金属阳离子，1当量的质子化氮碱或含有N（+）H3基团或氢的化合物，条件是R'和R“可以同时为氢，只要R是-N（+）H3X （ - ）激进。

4. 发明授权

US4528379A Preparation of substituted thiadiazolyloxyacetamides 失效
标题翻译：取代的噻二唑氧基乙酰胺的制备
公开(公告)号：US4528379A
公开(公告)日：1985-07-09
申请号：US515084
申请日：1983-07-18
申请人： Reimer Colln , Karl H. Mohrmann
发明人： Reimer Colln , Karl H. Mohrmann
IPC分类号： A01N43/824 , A01N43/836 , C07D285/08 , C07D285/12 , C07D285/13 , C07D417/12
CPC分类号： C07D285/08 , C07D285/13
摘要： In a process for the preparation of a substituted thiadiazolyloxyacetamide of the formula ##STR1## in which R.sup.1 and R.sup.2 each independently is hydrogen, alkyl, alkenyl, alkenyl, alkinyl, optionally substituted cycloalkyl or cycloalkenyl, halogenoalkyl, alkoxyalkyl, alkoxy, aralkyl or optionally substituted aryl, orR.sup.1 and R.sup.2, together with the nitrogen atom to which they are bonded, form an optionally substituted heterocyclic structure which can contain further hetero atoms,One of X and Y is a nitrogen atom and the other a C-R.sup.3 a grouping, andR.sup.3 is alkyl, alkoxy, alkylthio, alkylsulphonyl, halogenoalkyl, aralkyl, aralkoxy, aralkythio or optionally substituted aryl,wherein a substituted 5-halogenothiadiazole of the formula ##STR2## in which Hal is halogen, is reacted with a hydroxyacetamide of the formula ##STR3## in the presence of a base as an acid acceptor and, optionally in the presence of a diluent, the improvement which comprises employing lithium hydroxide or its hydrate as the base, and carrying out the reaction at a temperature between about -10.degree. C. and +60.degree. C. The end products are known herbicides.
摘要翻译：在制备式“IMAGE”的取代的噻二唑氧基乙酰胺的方法中，其中R 1和R 2各自独立地为氢，烷基，烯基，烯基，炔基，任选取代的环烷基或环烯基，卤代烷基，烷氧基烷基，烷氧基，芳烷基或任选取代芳基或R 1和R 2与它们所键合的氮原子一起形成可含有其它杂原子的任选取代的杂环结构，X和Y之一是氮原子，另一个是C-R 3a组，和 R 3是烷基，烷氧基，烷硫基，烷基磺酰基，卤代烷基，芳烷基，芳烷氧基，芳烷基或任选取代的芳基，其中Hal为卤素的式“IMAGE”的取代的5-卤代噻二唑与下式的羟基乙酰胺在作为酸受体的碱存在下，并且任选地在稀释剂的存在下，包括使用氢氧化锂或其水合物作为碱的改进，并在约-10℃至+ 60℃的温度下进行反应。最终产物是已知的除草剂。

5. 发明授权

US4154780A Preparation of dithiophosphoric acid diester-halides 失效
标题翻译：二硫代磷酸二酯 - 卤化物的制备
公开(公告)号：US4154780A
公开(公告)日：1979-05-15
申请号：US783371
申请日：1977-03-31
申请人： Reimer Colln , Hermann Arold , Vidyanatha A. Prasad
发明人： Reimer Colln , Hermann Arold , Vidyanatha A. Prasad
IPC分类号： B01J31/00 , B32B27/00 , C07B61/00 , C07F9/20
CPC分类号： C07F9/20 , B32B27/00
摘要： A process for the preparation of a dithiophosphoric acid diester-halide of the formula ##STR1## IN WHICH R.sup.1 is alkyl with 1 to 10 carbon atoms, aralkyl with 1 to 6 carbon atoms in the alkyl radical, or alkoxyalkyl or alkylthioalkyl with 1 to 5 carbon atoms in each alkyl radical,R.sup.2 is alkyl with 1 to 8 carbon atoms, andHal is halogen,Which comprises reacting an S-alkyl or S-aralkyl ester of a dithiophosphoric acid dihalide of the formula ##STR2## WITH ABOUT A 5 TO 300% MOLAR EXCESS OF AN ALCOHOL OF THE FORMULAR.sup.2 OHin the presence of about a 5 to 300% molar excess of a tertiary pyridine base or tertiary aralkyl-alkylamine at a temperature between about -10.degree. and +60.degree. C. Advantageously the tertiary base is pyridine, 2-, 3- or 4-methyl-pyridine, 4-ethyl-pyridine, 5-ethyl-2-methyl-pyridine, 2,4- or 2,6-dimethyl-pyridine, 2,4,6-trimethyl-pyridine, quinoline, isoquinoline, 2-, 4- or 6-methyl-quinoline, 6-chloro-2-methyl-quinoline, 2-chloro-4-methyl-quinoline, 8-chloro-2-methyl-quinoline or dimethylbenzylamine, the reaction is carried out at about 0.degree. to 30.degree. C., the alcohol is ethanol employed in about a 15 to 30% molar excess, about a 20 to 210% molar excess of the tertiary base is employed, R.sup.1 is alkyl with 1 to 8 carbon atoms, aralkyl with 1 to 3 carbon atoms in the alkyl radical, or alkoxyalkyl or alkylthioalkyl with 1 to 3 carbon atoms in each alkyl radical and Hal is chlorine.
摘要翻译：一种制备下式的二硫代磷酸二酯 - 卤化物的方法，其中R1是具有1-10个碳原子的烷基，在烷基中具有1-6个碳原子的芳烷基，或具有1-5个碳原子的烷氧基烷基或烷硫基烷基每个烷基中的碳原子，R 2是具有1至8个碳原子的烷基，Hal是卤素，其包含反应式为“A”的二硫代磷酸二卤化物的S-烷基或S-芳烷基酯在约5-10％摩尔过量的叔吡啶碱或叔芳烷基 - 烷基胺的存在下，在约-10℃和+ 60℃之间的温度下，在摩尔过量的情况下，300摩尔过量的式碱是吡啶，2-，3-或4-甲基 - 吡啶，4-乙基 - 吡啶，5-乙基-2-甲基 - 吡啶，2,4-或2,6-二甲基 - 吡啶，2,4,6 - 三甲基 - 吡啶，喹啉，异喹啉，2-，4-或6-甲基 - 喹啉，6-氯-2-甲基 - 喹啉，2-氯-4-甲基 - 喹啉，8-氯-2-甲基 - 喹啉 e或二甲基苄胺，反应在约0℃至30℃进行，醇为约15至30摩尔过量的乙醇，约20至210摩尔过量的叔碱，R1 具有1至8个碳原子的烷基，在烷基中具有1至3个碳原子的芳烷基，或每个烷基中具有1至3个碳原子的烷氧基烷基或烷硫基烷基，Hal为氯。

6. 发明授权

US4067970A Pesticidal O-ethyl-S-n-propyl-O[pyrazolo(1,5-a)-pyrimidin-(2) yl]-thionothiolphosphoric acid esters 失效
标题翻译：杀虫剂O-乙基-S-正丙基-O {8吡唑并（1,5-a） - 嘧啶 - （2）基{9-硫代硫代磷酸酯
公开(公告)号：US4067970A
公开(公告)日：1978-01-10
申请号：US727203
申请日：1976-09-27
申请人： Reimer Colln , Hans-Jochem Riebel , Ingeborg Hammann , Bernhard Homeyer
发明人： Reimer Colln , Hans-Jochem Riebel , Ingeborg Hammann , Bernhard Homeyer
IPC分类号： A01N57/16 , C07F9/6561 , A01N9/36 , C07D239/00
CPC分类号： C07F9/6561 , A01N57/16
摘要： O-Ethyl-S-n-propyl-O-[pyrazolo(1,5a)-pyrimidin(2)-yl]-thionothiolphosphoric acid esters of the formula ##STR1## in which R is hydrogen or halogen,R.sub.1 is alkyl with 1 to 5 carbon atoms or hydrogen,R.sub.2 is hydrogen, halogen or acetyl, andR.sub.3 is hydrogen, alkyl with 1 to 4 carbon atoms or carbalkoxy with 1 to 4 carbon atoms in the alkyl radical,Which possess arthropodicidal and nematicidal properties.
摘要翻译：具有式（I）的O-乙基-S-丙基-O- [吡唑并（1,5a） - 嘧啶（2） - 基] - 硫代硫代磷酸酯，其中R是氢或卤素，R 1是烷基具有1至5个碳原子或氢，R 2是氢，卤素或乙酰基，并且R 3是氢，具有1至4个碳原子的烷基或在烷基中具有1至4个碳原子的烷氧基，具有无定形的抗坏血酸和非特异性。

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