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1. 发明申请

US20100230339A1 Particulate chiral separation material 审中-公开
标题翻译：颗粒状手性分离材料
公开(公告)号：US20100230339A1
公开(公告)日：2010-09-16
申请号：US11641257
申请日：2006-12-19
申请人： Regina Valluzzi , Liya Liu , Christopher Sprout , Benjamin Chaloner-Gill
发明人： Regina Valluzzi , Liya Liu , Christopher Sprout , Benjamin Chaloner-Gill
IPC分类号： B01D15/08 , B32B1/00 , C07K1/00
CPC分类号： C07B57/00 , B01D15/3833 , B01J20/24 , B01J20/26 , B01J20/265 , B01J20/267 , B01J20/28004 , B01J20/28019 , B01J20/28023 , B01J20/28047 , B01J20/28083 , B01J20/28095 , B01J20/285 , B01J20/287 , B01J20/29 , B01J20/3092 , B01J20/3208 , B01J20/3246 , B01J31/061 , B01J31/068 , B01J31/165 , B01J2220/4856 , B01J2220/54 , B01J2220/58 , Y10T428/2982
摘要： A chiral particulate material and method of making the same are provided. The material includes a fibrous protein or chiral synthetic polymer, optionally crosslinked, organized into a multilayered chiral structure including nanoscale chiral pores or channels. The particles are useful for performing chiral separations, including in chromatographic applications.
摘要翻译：提供了手性颗粒材料及其制备方法。该材料包括任选交联的纤维蛋白质或手性合成聚合物，被组织成包括纳米级手性孔或通道的多层手性结构。颗粒可用于进行手性分离，包括色谱应用。

2. 发明申请

US20070255042A1 Production of chiral materials using crystallization inhibitors 审中-公开
标题翻译：使用结晶抑制剂生产手性材料
公开(公告)号：US20070255042A1
公开(公告)日：2007-11-01
申请号：US11641344
申请日：2006-12-19
申请人： Regina Valluzzi , Liya Liu
发明人： Regina Valluzzi , Liya Liu
IPC分类号： C07K2/00
CPC分类号： C07B57/00 , B01D15/3833 , B01J20/24 , B01J20/26 , B01J20/265 , B01J20/267 , B01J20/28004 , B01J20/28019 , B01J20/28023 , B01J20/28047 , B01J20/28083 , B01J20/28095 , B01J20/285 , B01J20/287 , B01J20/29 , B01J20/3092 , B01J20/3208 , B01J20/3246 , B01J31/061 , B01J31/068 , B01J31/165 , B01J2220/4856 , B01J2220/54 , B01J2220/58 , Y10T428/2982
摘要： A method is disclosed for producing a chiral gel. A polymer including chiral monomers, such as a protein, is dissolved to generate a sol, which is optionally dialyzed. The sol is contacted with a crystallization inhibitor that allows it to form a gel. The gel in wet or dried form is useful for performing chiral separations.
摘要翻译：公开了一种用于制备手性凝胶的方法。将包含手性单体（例如蛋白质）的聚合物溶解以产生任选地透析的溶胶。将该溶胶与允许其形成凝胶的结晶抑制剂接触。湿或干燥形式的凝胶可用于进行手性分离。

3. 发明申请

US20060205927A1 Templated native silk smectic gels 有权
公开(公告)号：US20060205927A1
公开(公告)日：2006-09-14
申请号：US10533611
申请日：2003-10-31
申请人： Hyoung-Joon Jin , Jae-Hyung Park , Regina Valluzzi
发明人： Hyoung-Joon Jin , Jae-Hyung Park , Regina Valluzzi
IPC分类号： C07K14/78 , C07K14/435
CPC分类号： A61K47/42 , C07K14/43586 , Y10T436/25375
摘要： One aspect of the present invention relates to a method of preparing a fibrous protein smectic hydrogel by way of a solvent templating process, comprising the steps of pouring an aqueous fibrous protein solution into a container comprising a solvent that is not miscible with water; sealing the container and allowing it to age at about room temperature; and collecting the resulting fibrous protein smectic hydrogel and allowing it to dry. Another aspect of the present invention relates to a method of obtaining predominantly one enantiomer from a racemic mixture, comprising the steps of pouring an aqueous fibrous protein solution into a container comprising a solvent that is not miscible with water; sealing the container and allowing it to age at about room temperature; allowing the enantiomers of racemic mixture to diffuse selectively into the smectic hydrogel in solution; removing the smectic hydrogel from the solution; rinsing predominantly one enantiomer from the surface of the smectic hydrogel; and extracting predominantly one enantiomer from the interior of the smectic hydrogel. The present invention also relates to a smectic hydrogel prepared according to an aforementioned method.

4. 发明申请

US20100294716A1 Templated Native Silk Smectic Gels 有权
标题翻译：模板本地丝绸水晶凝胶
公开(公告)号：US20100294716A1
公开(公告)日：2010-11-25
申请号：US12536793
申请日：2009-08-06
申请人： Hyoung-Joon Jin , Jae-Hyung Park , Regina Valluzzi
发明人： Hyoung-Joon Jin , Jae-Hyung Park , Regina Valluzzi
IPC分类号： B01D15/08 , B01D59/26 , C07K14/435 , B32B9/02 , C12N9/00 , C09K3/00 , B01J31/02
CPC分类号： A61K47/42 , C07K14/43586 , Y10T436/25375
摘要： One aspect of the present invention relates to a method of preparing a fibrous protein smectic hydrogel by way of a solvent templating process, comprising the steps of pouring an aqueous fibrous protein solution into a container comprising a solvent that is not miscible with water; sealing the container and allowing it to age at about room temperature; and collecting the resulting fibrous protein smectic hydrogel and allowing it to dry. Another aspect of the present invention relates to a method of obtaining predominantly one enantiomer from a racemic mixture, comprising the steps of pouring an aqueous fibrous protein solution into a container comprising a solvent that is not miscible with water; sealing the container and allowing it to age at about room temperature; allowing the enantiomers of racemic mixture to diffuse selectively into the smectic hydrogel in solution; removing the smectic hydrogel from the solution; rinsing predominantly one enantiomer from the surface of the smectic hydrogel; and extracting predominantly one enantiomer from the interior of the smectic hydrogel. The present invention also relates to a smectic hydrogel prepared according to an aforementioned method.
摘要翻译：本发明的一个方面涉及一种通过溶剂模板法制备纤维蛋白质近晶水凝胶的方法，包括以下步骤：将水性纤维蛋白溶液倒入包含不与水混溶的溶剂的容器中; 密封容器并使其在约室温下老化; 并收集所得到的纤维蛋白质近晶凝胶并使其干燥。本发明的另一方面涉及从外消旋混合物主要获得一种对映异构体的方法，包括以下步骤：将水性纤维蛋白溶液倒入包含不与水混溶的溶剂的容器中; 密封容器并使其在约室温下老化; 允许外消旋混合物的对映体选择性地扩散到溶液中的近晶水凝胶中; 从溶液中除去近晶凝胶; 从近晶水凝胶的表面主要漂洗一种对映异构体; 并从近晶水凝胶的内部主要提取一种对映异构体。本发明还涉及根据上述方法制备的近晶型水凝胶。

5. 发明申请

US20080314835A1 Chiral separating agents with active support 审中-公开
标题翻译：具有活性支持的手性分离剂
公开(公告)号：US20080314835A1
公开(公告)日：2008-12-25
申请号：US12009232
申请日：2008-01-16
申请人： Regina Valluzzi
发明人： Regina Valluzzi
IPC分类号： B01J20/29 , B01D15/08
CPC分类号： B01D15/3833 , B01J20/286 , B01J20/29 , G01N2030/027
摘要： A chiral stationary phase for use in chromatographic separation comprising a chiral selector compound and a chiral support material, wherein the chiral support material comprises a polymer comprising at least 30% chiral monomer of the same orientation.
摘要翻译：用于色谱分离的手性固定相，其包含手性选择剂化合物和手性载体材料，其中所述手性载体材料包含包含至少30％相同取向的手性单体的聚合物。

6. 发明授权

US08580924B2 Templated native silk smectic gels 有权
公开(公告)号：US08580924B2
公开(公告)日：2013-11-12
申请号：US12536793
申请日：2009-08-06
申请人： Hyoung-Joon Jin , Jae-Hyung Park , Regina Valluzzi
发明人： Hyoung-Joon Jin , Jae-Hyung Park , Regina Valluzzi
IPC分类号： A61K38/17
CPC分类号： A61K47/42 , C07K14/43586 , Y10T436/25375
摘要： One aspect of the present invention relates to a method of preparing a fibrous protein smectic hydrogel by way of a solvent templating process, comprising the steps of pouring an aqueous fibrous protein solution into a container comprising a solvent that is not miscible with water; sealing the container and allowing it to age at about room temperature; and collecting the resulting fibrous protein smectic hydrogel and allowing it to dry. Another aspect of the present invention relates to a method of obtaining predominantly one enantiomer from a racemic mixture, comprising the steps of pouring an aqueous fibrous protein solution into a container comprising a solvent that is not miscible with water; sealing the container and allowing it to age at about room temperature; allowing the enantiomers of racemic mixture to diffuse selectively into the smectic hydrogel in solution; removing the smectic hydrogel from the solution; rinsing predominantly one enantiomer from the surface of the smectic hydrogel; and extracting predominantly one enantiomer from the interior of the smectic hydrogel. The present invention also relates to a smectic hydrogel prepared according to an aforementioned method.

7. 发明授权

US07572894B2 Templated native silk smectic gels 有权
标题翻译：模板的天然丝状近晶凝胶
公开(公告)号：US07572894B2
公开(公告)日：2009-08-11
申请号：US10533611
申请日：2003-10-31
申请人： Hyoung-Joon Jin , Jae-Hyung Park , Regina Valluzzi
发明人： Hyoung-Joon Jin , Jae-Hyung Park , Regina Valluzzi
IPC分类号： C07K14/00 , G01N33/50
CPC分类号： A61K47/42 , C07K14/43586 , Y10T436/25375
摘要： One aspect of the present invention relates to a method of preparing a fibrous protein smectic hydrogel by way of a solvent templating process, comprising the steps of pouring an aqueous fibrous protein solution into a container comprising a solvent that is not miscible with water; sealing the container and allowing it to age at about room temperature; and collecting the resulting fibrous protein smectic hydrogel and allowing it to dry. Another aspect of the present invention relates to a method of obtaining predominantly one enantiomer from a racemic mixture, comprising the steps of pouring an aqueous fibrous protein solution into a container comprising a solvent that is not miscible with water; sealing the container and allowing it to age at about room temperature; allowing the enantiomers of racemic mixture to diffuse selectively into the smectic hydrogel in solution; removing the smectic hydrogel from the solution; rinsing predominantly one enantiomer from the surface of the smectic hydrogel; and extracting predominantly one enantiomer from the interior of the smectic hydrogel. The present invention also relates to a smectic hydrogel prepared according to an aforementioned method.
摘要翻译：本发明的一个方面涉及一种通过溶剂模板法制备纤维蛋白质近晶水凝胶的方法，包括以下步骤：将水性纤维蛋白溶液倒入包含不与水混溶的溶剂的容器中; 密封容器并使其在约室温下老化; 并收集所得到的纤维蛋白质近晶凝胶并使其干燥。本发明的另一方面涉及从外消旋混合物主要获得一种对映异构体的方法，包括以下步骤：将水性纤维蛋白溶液倒入包含不与水混溶的溶剂的容器中; 密封容器并使其在约室温下老化; 允许外消旋混合物的对映体选择性扩散到溶液中的近晶水凝胶中; 从溶液中除去近晶凝胶; 从近晶水凝胶的表面主要漂洗一种对映异构体; 并从近晶水凝胶的内部主要提取一种对映异构体。本发明还涉及根据上述方法制备的近晶型水凝胶。

8. 发明申请

US20050090641A1 Self-assembling polymers, and materials fabricated therefrom 审中-公开
标题翻译：自组装聚合物和由其制成的材料
公开(公告)号：US20050090641A1
公开(公告)日：2005-04-28
申请号：US10490799
申请日：2002-10-02
申请人： Regina Valluzzi , David Kaplan
发明人： Regina Valluzzi , David Kaplan
IPC分类号： C12N15/09 , A61K47/42 , A61K47/48 , B01J31/06 , C07K7/06 , C07K7/08 , C07K14/00 , C07K14/435 , C07K14/46 , C07K14/47 , C08G63/48 , C08G63/91 , C08G69/10
CPC分类号： C08G69/10 , B01J31/062 , B82Y30/00 , C07K7/06 , C07K7/08 , C07K14/001
摘要： The invention features miniblock polymers containing solubilizing blocks and folding blocks, wherein the miniblock polymers in solution can self-fabricate to form materials having a long-range order. Also disclosed are rigid well-fabricated materials and methods of using these materials.
摘要翻译：本发明的特征是含有增溶嵌段和折叠嵌段的小嵌段聚合物，其中溶液中的微型嵌段聚合物可以自行制造以形成具有长程顺序的材料。还公开了使用这些材料的刚性良好的材料和方法。

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