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1. 发明授权

US4195151A Phenol-aldehyde-amine resin/glycol curative compositions 失效
标题翻译：苯酚醛胺树脂/乙二醇固化剂组合物
公开(公告)号：US4195151A
公开(公告)日：1980-03-25
申请号：US911523
申请日：1978-06-01
申请人： Raymond A. Dunleavy , Anthony J. Papa
发明人： Raymond A. Dunleavy , Anthony J. Papa
IPC分类号： C08G18/54 , C08G18/65 , C08G8/20 , C08G8/28 , C08G14/06 , C08G14/12
CPC分类号： C08G18/544 , C08G18/6505
摘要： This invention relates to novel curative compositions for use in the production of cellular polyurethane elastomers having outstanding energy-absorbing properties. The curative compositions are composed of mixtures of organic diols and the reaction product of phenols which have at least one unsubstituted reactive position on the aromatic nucleus, aldehydes, and aromatic amines.
摘要翻译：本发明涉及用于生产具有突出的能量吸收特性的多孔聚氨酯弹性体的新型固化剂组合物。固化剂组合物由有机二醇和在芳族核，醛和芳族胺上具有至少一个未取代的反应性位置的酚的反应产物的混合物组成。

2. 发明授权

US4945185A Process for producing mixtures of ketones and aldehydes 失效
标题翻译：制备酮和醛的混合物的方法
公开(公告)号：US4945185A
公开(公告)日：1990-07-31
申请号：US445927
申请日：1989-12-05
申请人： Anthony J. Papa , David R. Bryant
发明人： Anthony J. Papa , David R. Bryant
IPC分类号： B01J31/04 , B01J31/20 , B01J31/22 , B01J31/24 , C07C45/50
CPC分类号： B01J31/2404 , B01J31/20 , C07C45/50 , B01J2231/321 , B01J2531/822 , B01J31/2234 , B01J31/2295
摘要： A hydrocarbonylation process for producing an aldehyde or a mixture of a ketone and an aldehyde which comprises:(I) forming a reaction mixture comprising:(a) a catalytic amount of a complex catalyst consisting essentially of rhodium in complex combination with:(i) a triorganophosphine, and(ii) a carboxylic acid having a phenyl group substituted at the para position with a non-reactive electron-withdrawing group, said phenyl group being free of further substitution and said electron withdrawing group being substantially non-reactive in said process;(b) an alpha-olefin having 2 to 5 carbon atoms,(c) carbon monixide, and(d) hydrogenwith the proviso that the reaction mixture has mole ratio of said carbxoylic acid to rhodium of at least about 2; and(II) maintaining the reaction mixture at a temperature and pressure at which said (b), (c) and (d) react to form an aldehyde or a mixture of an aldehyde and a ketone.
摘要翻译：用于产生醛或酮和醛的混合物的烃基化方法，其包括：（I）形成反应混合物，其包含：（a）催化量的基本上由铑组成的复合催化剂，其复合组合与：（i）三有机膦，和（ii）具有在对位被非反应性吸电子基团取代的苯基的羧酸，所述苯基不再进一步取代，并且所述吸电子基团在所述方法中基本上不反应 ; （b）具有2至5个碳原子的α-烯烃，（c）一碳化碳和（d）氢，条件是反应混合物具有至少约2的所述羧甲基酸与铑的摩尔比; 和（II）将反应混合物保持在所述（b），（c）和（d）反应的温度和压力下，形成醛或醛和酮的混合物。

3. 发明授权

US4528405A Aldol condensation of enolizable aldehydes using a metal carboxylate catalyst 失效
标题翻译：使用金属羧酸盐催化剂的可烯化醛的醛缩醇缩合
公开(公告)号：US4528405A
公开(公告)日：1985-07-09
申请号：US567423
申请日：1983-12-30
申请人： Anthony J. Papa
发明人： Anthony J. Papa
IPC分类号： C07C45/74 , C07C45/45
CPC分类号： C07C45/74
摘要： A process is disclosed for the aldol condensation of enolizable aldehydes to alpha, beta-unsaturated aldehydes, at high selectivities, employing a metal carboxylate catalyst.
摘要翻译：公开了一种使用金属羧酸盐催化剂，以高选择性将可烯化醛醛醛缩合成α，β-不饱和醛的方法。

4. 发明授权

US5231222A Esterification process 失效
标题翻译：确定过程
公开(公告)号：US5231222A
公开(公告)日：1993-07-27
申请号：US724811
申请日：1991-07-02
申请人： Anthony J. Papa , David R. Bryant
发明人： Anthony J. Papa , David R. Bryant
IPC分类号： B01J31/02 , C07B61/00 , C07C67/08 , C07C69/003 , C07C69/02 , C07C69/14 , C07C69/24
CPC分类号： C07C67/08
摘要： An improved esterification process for producing volatile product esters by reacting a lower linear hydrocarbyl carboxylic acid with an alcohol containing from 2 to 10 carbon atoms, in a substantially non-aqueous medium, the improvement comprising minimizing the amount of acidic sulfate contained in the product ester by employing as the esterification catalyst a long chain alkylbenzene sulfonic acid catalyst, the alkyl radical containing from 8 to 20 carbon atoms, or mixtures of such catalysts.

5. 发明授权

US4535187A Preparation of isophorone and mesityl oxide from acetone 失效
标题翻译：从丙酮制备异佛尔酮和三甲氧基硅烷
公开(公告)号：US4535187A
公开(公告)日：1985-08-13
申请号：US564023
申请日：1983-12-21
申请人： Anthony J. Papa , Steven W. Kaiser
发明人： Anthony J. Papa , Steven W. Kaiser
IPC分类号： C07C49/203 , B01J21/04 , B01J23/02 , C07B61/00 , C07C45/00 , C07C45/74 , C07C49/603 , C07C67/00 , C07C45/45
CPC分类号： C07C45/74 , B01J23/02
摘要： The aldol condensation of acetone to isophorone and mesityl oxides in high conversions and efficiencies is achieved by a catalyst comprising a calcined calcium salt deposited on an alumina support.
摘要翻译：通过包含沉积在氧化铝载体上的煅烧钙盐的催化剂来实现丙酮与异佛尔酮和均三甲苯氧化物的高转化率和效率的醛醇缩合。

6. 发明授权

US4162353A Method of producing flexible flame retarded polyurethane foam 失效
标题翻译：制造柔性阻燃聚氨酯泡沫的方法
公开(公告)号：US4162353A
公开(公告)日：1979-07-24
申请号：US892752
申请日：1978-04-03
申请人： Anthony J. Papa , Walter W. Runyan
发明人： Anthony J. Papa , Walter W. Runyan
IPC分类号： C07F9/09 , C08J9/00 , C08K5/52
CPC分类号： C08J9/0038 , C07F9/098 , C08K5/52 , C08J2375/04
摘要： Novel haloalkyl polyphosphates are prepared by reacting at elevated temperatures a halosubstituted alkyl phosphate such as, for example, tris (2-chloroethyl) phosphate, and an unsubstituted trialkyl phosphate such as, for example, triethyl phosphate. The character of the mixture of the thermal condensates formed can be influenced by the ratio of reactants employed and the extent to which the reaction is allowed to proceed. The resulting reaction products possess superior flame retardant efficiency and impart durable flame resistance when incorporated into flexible urethane foams.
摘要翻译：新型卤代烷基多磷酸盐通过在升高的温度下使卤代烷基磷酸酯例如磷酸三（2-氯乙基）和未取代的三烷基磷酸酯例如磷酸三乙酯反应制备。所形成的热缩合物的混合物的特性可以受所用反应物的比例和允许反应进行的程度的影响。所得反应产物具有优异的阻燃效率，并且在掺入柔性聚氨酯泡沫中时赋予耐久的阻燃性。

7. 发明授权

US5618973A Esterification process 失效
标题翻译：酯化过程
公开(公告)号：US5618973A
公开(公告)日：1997-04-08
申请号：US337101
申请日：1994-11-10
申请人： Anthony J. Papa , Brian T. Keen
发明人： Anthony J. Papa , Brian T. Keen
IPC分类号： C07C67/08
CPC分类号： C07C67/08 , Y02P20/582
摘要： An esterification process for producing glycol ether esters which comprises reacting a lower hydrocarbyl carboxylic acid with a glycol ether alcohol in the presence of a long chain alkyl substituted aryl sulfonic acid esterification catalyst, the alkyl radical having from 8 to 20 carbon atoms.
摘要翻译：用于生产二醇醚酯的酯化方法，其包括在长链烷基取代的芳基磺酸酯化催化剂存在下使低级烃基羧酸与二醇醚醇反应，所述烷基具有8至20个碳原子。

8. 发明授权

US4434301A Production of low color refined isophorone 失效
标题翻译：生产低色精制异佛尔酮
公开(公告)号：US4434301A
公开(公告)日：1984-02-28
申请号：US411280
申请日：1982-08-25
申请人： Anthony J. Papa
发明人： Anthony J. Papa
IPC分类号： C07C49/603 , C07C45/00 , C07C45/78 , C07C45/79 , C07C45/82 , C07C67/00 , C07C45/85 , B01D3/38
CPC分类号： C07C45/79 , C07C45/78 , C07C45/82
摘要： Crude isophorone is refined by contacting it with aqueous caustic followed by washing and fractional distillation.
摘要翻译：通过使其与苛性碱水溶液接触，然后进行洗涤和分馏，精制异佛尔酮。

9. 发明授权

US4110415A Methylol phosphonates and process for making same 失效
标题翻译：羟甲基膦酸酯及其制备方法
公开(公告)号：US4110415A
公开(公告)日：1978-08-29
申请号：US645133
申请日：1975-12-29
申请人： Eugene J. Boros , Anthony J. Papa
发明人： Eugene J. Boros , Anthony J. Papa
IPC分类号： C07F9/40 , C08G18/38 , C08K5/5333 , C08J9/00
CPC分类号： C08K5/5333 , C07F9/4006 , C08G18/388
摘要： Novel polymethylol polyphosphonates are prepared by reacting a trisubstituted polyphosphite having at least one alkyl group and formaldehyde. The phosphite reactant may contain the requisite hydroxyl functionality [e.g. - heptakis (dipropylene glycol) triphosphite] or the hydroxyl functionality may be introduced by carrying out the reaction in the presence of a polyol, e.g. - glycerol, as a protic solvent. The resulting reaction product is a water-soluble liquid of relatively low viscosity and may be employed without any refining. The thus-formed polyphosphonates can be readily incorporated into either rigid urethane foam formulations to impart flame retardancy or phenolic resins to improve flexibility.
摘要翻译：通过使具有至少一个烷基的三取代多亚磷酸酯和甲醛反应来制备新的多羟甲基多聚膦酸酯。亚磷酸酯反应物可含有必需的羟基官能团[例如 - 七（二丙二醇）三亚磷酸酯]或羟基官能团可以通过在多元醇的存在下进行反应来引入。 - 甘油，作为质子溶剂。所得反应产物是相对低粘度的水溶性液体，可以不经任何精制而使用。如此形成的聚膦酸盐可以容易地并入刚性聚氨酯泡沫制剂中以赋予阻燃性或酚醛树脂以改善柔韧性。

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