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1. 发明授权

US07829020B2 Simple, field portable colorimetric detection device for organic peroxides and hydrogen peroxide 有权
标题翻译：简单的现场便携式比色检测装置，用于有机过氧化物和过氧化氢
公开(公告)号：US07829020B2
公开(公告)日：2010-11-09
申请号：US12183210
申请日：2008-07-31
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
IPC分类号： G01N33/22
CPC分类号： G01N21/78 , G01N31/228 , Y10T29/49826 , Y10T436/206664
摘要： A simple and effective system for the colorimetric determination of organic peroxides and hydrogen peroxide. A peroxide pen utilizing a swipe material attached to a polyethylene tube contains two crushable vials. The two crushable vials contain a colorimetric reagent separated into dry ingredients and liquid ingredients. After swiping a suspected substance or surface the vials are broken, the reagent is mixed thoroughly and the reagent is allowed to wick into the swipe material. The presence of organic peroxides or hydrogen peroxide is confirmed by a deep blue color.
摘要翻译：用于比色测定有机过氧化物和过氧化氢的简单而有效的系统。使用连接到聚乙烯管上的滑动材料的过氧化物笔包含两个可压碎的小瓶。两个可压碎的小瓶包含分离成干成分和液体成分的比色试剂。打扫怀疑的物质或表面后，小瓶破裂，将试剂充分混合，使试剂吸入滑动材料。有机过氧化物或过氧化氢的存在通过深蓝色证实。

2. 发明申请

US20090068065A1 Simple, Field Portable Colorimetric Detection Device For Organic Peroxides and Hydrogen Peroxide 有权
标题翻译：用于有机过氧化物和过氧化氢的简单现场便携式比色检测装置
公开(公告)号：US20090068065A1
公开(公告)日：2009-03-12
申请号：US12183210
申请日：2008-07-31
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
IPC分类号： G01N21/00 , B23P11/00
CPC分类号： G01N21/78 , G01N31/228 , Y10T29/49826 , Y10T436/206664
摘要： A simple and effective system for the calorimetric determination of organic peroxides and hydrogen peroxide. A peroxide pen utilizing a swipe material attached to a polyethylene tube contains two crushable vials. The two crushable vials contain a calorimetric reagent separated into dry ingredients and liquid ingredients. After swiping a suspected substance or surface the vials are broken, the reagent is mixed thoroughly and the reagent is allowed to wick into the swipe material. The presence of organic peroxides or hydrogen peroxide is confirmed by a deep blue color.
摘要翻译：有机过氧化物和过氧化氢的量热测定的简单而有效的系统。使用连接到聚乙烯管上的滑动材料的过氧化物笔包含两个可压碎的小瓶。两个可压碎的小瓶含有分配成干成分和液体成分的量热试剂。打扫怀疑的物质或表面后，小瓶破裂，将试剂充分混合，使试剂吸入滑动材料。有机过氧化物或过氧化氢的存在通过深蓝色证实。

3. 发明授权

US08815606B2 Thin-layer chromatography and colorimetric analysis of multi-component explosive mixtures 有权
标题翻译：多组分爆炸性混合物的薄层色谱和比色分析
公开(公告)号：US08815606B2
公开(公告)日：2014-08-26
申请号：US12106400
申请日：2008-04-21
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
IPC分类号： G01N30/90 , G01N30/96
CPC分类号： G01N30/94 , G01N30/90 , G01N33/22
摘要： A thin-layer chromatography method for detection and identification of common military and peroxide explosives in samples includes the steps of provide a reverse-phase thin-layer chromatography plate; prepare the plate by marking spots on which to deposit the samples by touching the plate with a marker; spot one micro liter of a first standard onto one of the spots, spot one micro liter of a second standard onto another of the spots, and spot samples onto other of spots producing a spotted plate; add eluent to a developing chamber; add the spotted plate to the developing chamber; remove the spotted plate from the developing chamber producing a developed plate; place the developed plate in an ultraviolet light box; add a visualization agent to a dip tank; dip the developed plate in the dip tank and remove the developed plate quickly; and detect explosives by viewing said developed plate.
摘要翻译：用于检测和鉴定样品中常见的军用和过氧化物炸药的薄层色谱法包括提供反相薄层色谱板的步骤; 通过用标记触摸板来标记沉积样品的斑点来准备板; 将一微升第一标准物放在其中一个斑点上，将一微升第二标准物放在另一个斑点上，并将样品点样到产生斑点板的其他斑点上; 将洗脱液加入显影室; 将点样板加到显影室; 从显影室中取出点样板，产生显影板; 将显影的板放在紫外灯箱中; 将一个可视化代理添加到浸槽中; 将显影的板块浸入浸渍槽中，快速取出显影板; 并通过查看所述显影板来检测爆炸物。

4. 发明申请

US20090221085A1 Thin-Layer Chromatography and Colorimetric Analysis of Multi-Component Explosive Mixtures 有权
标题翻译：多组分爆炸混合物的薄层色谱和比色分析
公开(公告)号：US20090221085A1
公开(公告)日：2009-09-03
申请号：US12106400
申请日：2008-04-21
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
IPC分类号： G01N30/90
CPC分类号： G01N30/94 , G01N30/90 , G01N33/22
摘要： A thin-layer chromatography method for detection and identification of common military and peroxide explosives in samples includes the steps of provide a reverse-phase thin-layer chromatography plate; prepare the plate by marking spots on which to deposit the samples by touching the plate with a marker; spot one micro liter of a first standard onto one of the spots, spot one micro liter of a second standard onto another of the spots, and spot samples onto other of spots producing a spotted plate; add eluent to a developing chamber; add the spotted plate to the developing chamber; remove the spotted plate from the developing chamber producing a developed plate; place the developed plate in an ultraviolet light box; add a visualization agent to a dip tank; dip the developed plate in the dip tank and remove the developed plate quickly; and detect explosives by viewing said developed plate.
摘要翻译：用于检测和鉴定样品中常见的军用和过氧化物炸药的薄层色谱法包括提供反相薄层色谱板的步骤; 通过用标记触摸板来标记沉积样品的斑点来准备板; 将一微升第一标准物放在其中一个斑点上，将一微升第二标准物放在另一个斑点上，并将样品点样到产生斑点板的其他斑点上; 将洗脱液加入显影室; 将点样板加到显影室; 从显影室中取出点样板，产生显影板; 将显影的板放在紫外灯箱中; 将一个可视化代理添加到浸槽中; 将显影的板块浸入浸渍槽中，快速取出显影板; 并通过查看所述显影板来检测爆炸物。

5. 发明申请

US20110239745A1 Rapid Identification of Explosives Using Thin-Layer Chromatography and Colorimetric Techniques 审中-公开
标题翻译：使用薄层色谱和比色技术快速鉴定炸药
公开(公告)号：US20110239745A1
公开(公告)日：2011-10-06
申请号：US13028072
申请日：2011-02-15
申请人： Joe H. Satcher, JR. , Philip F. Pagoria , Richard E. Whipple , M. Leslie Carman
发明人： Joe H. Satcher, JR. , Philip F. Pagoria , Richard E. Whipple , M. Leslie Carman
IPC分类号： G01N30/02
CPC分类号： G01N30/90 , G01N30/95 , G01N33/22
摘要： A thin-layer chromatography method for identifying material present in a sample on a location including the steps of provide a thin-layer chromatography plate, wetting a swab is with a solvent providing a wetted swab, contacted the location of interest is with the wetted swab to obtain the sample providing a wetted swab with sample, placing the wetted swab with sample in the solvent to dissolve the sample and provide a solvent with sample, dipping a micropipette into the solvent with sample to obtain an amount of the solvent with sample, spotting the amount of the solvent with sample on the thin-layer chromatography plate, allowed the amount of the solvent with sample on the thin-layer chromatography plate to dry providing a thin-layer chromatography plate with sample, placing the a thin-layer chromatography plate with sample into a developing chamber with solvent mixture, allowing the thin-layer chromatography plate with sample to develop producing a developed thin-layer chromatography plate with sample, removing the developed thin-layer chromatography plate with sample from the developing chamber, and illuminating the developed thin-layer chromatography plate with sample with ultra violet light to produce an image for identifying the material present in the sample.
摘要翻译：用于识别样品中存在的位置的薄层色谱法包括提供薄层色谱板，润湿拭子的步骤是用提供湿拭子的溶剂，与感染的位置接触的湿拭子为了获得样品提供湿润的棉签，将带有样品的浸湿棉签放在溶剂中以溶解样品并向样品中提供溶剂，将样品浸入溶剂中以获得一定量的溶剂与样品，点样在薄层色谱板上的样品溶剂量允许在薄层色谱板上的样品溶剂的量干燥，提供具有样品的薄层色谱板，将薄层色谱板将样品放入具有溶剂混合物的显影室中，允许具有样品的薄层色谱板开发生产显影的薄层色谱仪 y板，样品从显影室中取出开发的薄层色谱板，并用紫外光照射显影的薄层色谱板，以产生用于鉴定样品中存在的材料的图像。

6. 发明申请

US20100256923A1 COMPOUNDS FOR NEUTRON RADIATION DETECTORS AND SYSTEMS THEREOF 有权
标题翻译：用于中子辐射检测器及其系统的化合物
公开(公告)号：US20100256923A1
公开(公告)日：2010-10-07
申请号：US12418450
申请日：2009-04-03
申请人： Stephen A. Payne , Wolfgang Stoeffl , Natalia P. Zaitseva , Nerine J. Cherepy , M. Leslie Carman
发明人： Stephen A. Payne , Wolfgang Stoeffl , Natalia P. Zaitseva , Nerine J. Cherepy , M. Leslie Carman
IPC分类号： G06F19/00 , G01T3/00 , G01T1/00 , C07C15/16 , C07C63/331 , C07C13/573 , C07C15/14 , C07C15/52 , C07C15/54 , C07D263/32 , C07C43/205 , C07C229/54
CPC分类号： G01T1/2023 , C07C15/12 , C07C15/14 , C07C15/16 , C07C15/28 , C07C15/52 , C07C15/54 , C07C43/205 , C07C63/331 , C07C229/58 , C07D263/32 , G01T1/2006 , G01T3/06 , Y10T428/2982
摘要： One embodiment includes a material exhibiting an optical response signature for neutrons that is different than an optical response signature for gamma rays, said material exhibiting performance comparable to or superior to stilbene in terms of distinguishing neutrons from gamma rays, wherein the material is not stilbene. Another embodiment includes a substantially pure crystal exhibiting an optical response signature for neutrons that is different than an optical response signature for gamma rays, the substantially pure crystal comprising a material selected from a group consisting of: 1-1-4-4-tetraphenyl-1-3-butadiene; 2-fluorobiphenyl-4-carboxylic acid; 4-biphenylcarboxylic acid; 9-10-diphenylanthracene; 9-phenylanthracene; 1-3-5-triphenylbenzene; m-terphenyl; bis-MSB; p-terphenyl; diphenylacetylene; 2-5-diphenyoxazole; 4-benzylbiphenyl; biphenyl; 4-methoxybiphenyl; n-phenylanthranilic acid; and 1-4-diphenyl-1-3-butadiene.
摘要翻译：一个实施例包括表现出与γ射线的光学响应特征不同的中子的光学响应特征的材料，所述材料在区分中子与γ射线方面表现出与二苯乙烯相当或优于其他物质的性能，其中该材料不是二苯乙烯。另一个实施方案包括显示与γ射线的光学响应特征不同的中子的光学响应特征的基本上纯的晶体，所述基本上纯的晶体包括选自以下的材料：1-1-4-4-四苯基 - 1-3丁二烯; 2-氟联苯-4-羧酸; 4-联苯基羧酸; 9-10-二苯基蒽; 9-苯基蒽; 1-3,5-三苯基苯; 三联苯; 双MSB; 对三联苯二苯基乙炔 2-5-diphenyoxazole; 4-苄基联苯; 联苯 4-甲氧基联苯; 邻苯二甲酸和1-4-二苯基-1,3-丁二烯。

7. 发明授权

US08872125B2 Solution-grown crystals for neutron radiation detectors, and methods of solution growth 有权
标题翻译：用于中子辐射探测器的溶液生长晶体和溶液生长方法
公开(公告)号：US08872125B2
公开(公告)日：2014-10-28
申请号：US13477910
申请日：2012-05-22
申请人： Natalia Zaitseva , M. Leslie Carman , Steve Payne
发明人： Natalia Zaitseva , M. Leslie Carman , Steve Payne
IPC分类号： G01T3/06
CPC分类号： G01T3/06 , C07C15/14 , C07C15/20 , C07C15/28 , C07C15/50 , C07C15/52 , C07C15/54 , C07C51/43 , C07C63/72 , C07C229/58 , C07C2603/24 , C30B7/06 , C30B29/54 , Y10T428/2982 , C07C63/331
摘要： An organic crystal according to one embodiment includes an organic crystal comprising diphenylacetylene and stilbene or a stilbene derivative, the crystal having physical characteristics of formation from solution, the organic crystal exhibiting a signal response signature for neutrons from a radioactive source. A system according to one embodiment includes an organic crystal comprising diphenylacetylene and stilbene or a stilbene derivative, the crystal having physical characteristics of formation from solution, the organic crystal exhibiting a signal response signature for neutrons from a radioactive source; and a photodetector for detecting the signal response of the organic crystal. Methods of making such crystals are also provided.
摘要翻译：根据一个实施方案的有机晶体包括含有二苯基乙炔和二苯乙烯或二苯乙烯衍生物的有机晶体，具有从溶液形成的物理特性的晶体，所述有机晶体对放射源表现出中子的信号响应特征。根据一个实施方案的系统包括含有二苯基乙炔和二苯乙烯或二苯乙烯衍生物的有机晶体，所述晶体具有从溶液形成的物理特性，所述有机晶体对放射源表现出中子的信号响应特征; 以及用于检测有机晶体的信号响应的光电检测器。还提供了制备这种晶体的方法。

8. 发明授权

US06165356A In situ microbial filter used for bioremediation 失效
标题翻译：用于生物修复的原位微生物过滤器
公开(公告)号：US06165356A
公开(公告)日：2000-12-26
申请号：US200301
申请日：1998-11-25
申请人： M. Leslie Carman , Robert T. Taylor
发明人： M. Leslie Carman , Robert T. Taylor
IPC分类号： B09C1/00 , B09C1/10 , C02F3/34
CPC分类号： B09C1/10 , B09C1/002 , B09C2101/00 , C02F3/34 , C02F3/342 , Y02E50/343
摘要： An improved method for in situ microbial filter bioremediation having increasingly operational longevity of an in situ microbial filter emplaced into an aquifer. A method for generating a microbial filter of sufficient catalytic density and thickness, which has increased replenishment interval, improved bacteria attachment and detachment characteristics and the endogenous stability under in situ conditions. A system for in situ field water remediation.
摘要翻译：用于原位微生物过滤器生物修复的改进方法具有放置在含水层中的原位微生物过滤器具有越来越多的操作寿命。一种产生足够催化密度和厚度的微生物过滤器的方法，其具有增加的补充间隔，改善细菌附着和分离特性以及在原位条件下的内源稳定性。一种现场水处理系统。

9. 发明授权

US5888395A Method for enhanced longevity of in situ microbial filter used for bioremediation 失效
标题翻译：用于生物修复的原位微生物过滤器寿命延长的方法
公开(公告)号：US5888395A
公开(公告)日：1999-03-30
申请号：US706152
申请日：1996-08-30
申请人： M. Leslie Carman , Robert T. Taylor
发明人： M. Leslie Carman , Robert T. Taylor
IPC分类号： B09C1/00 , B09C1/10 , C02F3/34
CPC分类号： B09C1/10 , B09C1/002 , C02F3/34 , C02F3/342 , B09C2101/00 , Y02E50/343
摘要： An improved method for in situ microbial filter bioremediation having increasingly operational longevity of an in situ microbial filter emplaced into an aquifer. A method for generating a microbial filter of sufficient catalytic density and thickness, which has increased replenishment interval, improved bacteria attachment and detachment characteristics and the endogenous stability under in situ conditions. A system for in situ field water remediation.
摘要翻译：用于原位微生物过滤器生物修复的改进方法具有放置在含水层中的原位微生物过滤器具有越来越多的操作寿命。一种产生足够催化密度和厚度的微生物过滤器的方法，其具有增加的补充间隔，改善细菌附着和分离特性以及在原位条件下的内源稳定性。一种现场水处理系统。

10. 发明授权

US09650564B2 System and plastic scintillator for discrimination of thermal neutron, fast neutron, and gamma radiation 有权
公开(公告)号：US09650564B2
公开(公告)日：2017-05-16
申请号：US13471259
申请日：2012-05-14
申请人： Natalia P. Zaitseva , M. Leslie Carman , Michelle A. Faust , Andrew M. Glenn , H. Paul Martinez , Iwona A. Pawelczak , Stephen A. Payne , Keith E. Lewis
发明人： Natalia P. Zaitseva , M. Leslie Carman , Michelle A. Faust , Andrew M. Glenn , H. Paul Martinez , Iwona A. Pawelczak , Stephen A. Payne , Keith E. Lewis
IPC分类号： G01T1/20 , C09K11/06 , G01T1/203 , G01T3/06 , G21K4/00
CPC分类号： C09K11/06 , G01T1/203 , G01T3/06 , G21K4/00
摘要： A scintillator material according to one embodiment includes a polymer matrix; a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount of 3 wt % or more; and at least one component in the polymer matrix, the component being selected from a group consisting of B, Li, Gd, a B-containing compound, a Li-containing compound and a Gd-containing compound, wherein the scintillator material exhibits an optical response signature for thermal neutrons that is different than an optical response signature for fast neutrons and gamma rays. A system according to one embodiment includes a scintillator material as disclosed herein and a photodetector for detecting the response of the material to fast neutron, thermal neutron and gamma ray irradiation.

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