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1. 发明申请

US20110239745A1 Rapid Identification of Explosives Using Thin-Layer Chromatography and Colorimetric Techniques 审中-公开
标题翻译：使用薄层色谱和比色技术快速鉴定炸药
公开(公告)号：US20110239745A1
公开(公告)日：2011-10-06
申请号：US13028072
申请日：2011-02-15
申请人： Joe H. Satcher, JR. , Philip F. Pagoria , Richard E. Whipple , M. Leslie Carman
发明人： Joe H. Satcher, JR. , Philip F. Pagoria , Richard E. Whipple , M. Leslie Carman
IPC分类号： G01N30/02
CPC分类号： G01N30/90 , G01N30/95 , G01N33/22
摘要： A thin-layer chromatography method for identifying material present in a sample on a location including the steps of provide a thin-layer chromatography plate, wetting a swab is with a solvent providing a wetted swab, contacted the location of interest is with the wetted swab to obtain the sample providing a wetted swab with sample, placing the wetted swab with sample in the solvent to dissolve the sample and provide a solvent with sample, dipping a micropipette into the solvent with sample to obtain an amount of the solvent with sample, spotting the amount of the solvent with sample on the thin-layer chromatography plate, allowed the amount of the solvent with sample on the thin-layer chromatography plate to dry providing a thin-layer chromatography plate with sample, placing the a thin-layer chromatography plate with sample into a developing chamber with solvent mixture, allowing the thin-layer chromatography plate with sample to develop producing a developed thin-layer chromatography plate with sample, removing the developed thin-layer chromatography plate with sample from the developing chamber, and illuminating the developed thin-layer chromatography plate with sample with ultra violet light to produce an image for identifying the material present in the sample.
摘要翻译：用于识别样品中存在的位置的薄层色谱法包括提供薄层色谱板，润湿拭子的步骤是用提供湿拭子的溶剂，与感染的位置接触的湿拭子为了获得样品提供湿润的棉签，将带有样品的浸湿棉签放在溶剂中以溶解样品并向样品中提供溶剂，将样品浸入溶剂中以获得一定量的溶剂与样品，点样在薄层色谱板上的样品溶剂量允许在薄层色谱板上的样品溶剂的量干燥，提供具有样品的薄层色谱板，将薄层色谱板将样品放入具有溶剂混合物的显影室中，允许具有样品的薄层色谱板开发生产显影的薄层色谱仪 y板，样品从显影室中取出开发的薄层色谱板，并用紫外光照射显影的薄层色谱板，以产生用于鉴定样品中存在的材料的图像。

2. 发明申请

US20090068065A1 Simple, Field Portable Colorimetric Detection Device For Organic Peroxides and Hydrogen Peroxide 有权
标题翻译：用于有机过氧化物和过氧化氢的简单现场便携式比色检测装置
公开(公告)号：US20090068065A1
公开(公告)日：2009-03-12
申请号：US12183210
申请日：2008-07-31
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
IPC分类号： G01N21/00 , B23P11/00
CPC分类号： G01N21/78 , G01N31/228 , Y10T29/49826 , Y10T436/206664
摘要： A simple and effective system for the calorimetric determination of organic peroxides and hydrogen peroxide. A peroxide pen utilizing a swipe material attached to a polyethylene tube contains two crushable vials. The two crushable vials contain a calorimetric reagent separated into dry ingredients and liquid ingredients. After swiping a suspected substance or surface the vials are broken, the reagent is mixed thoroughly and the reagent is allowed to wick into the swipe material. The presence of organic peroxides or hydrogen peroxide is confirmed by a deep blue color.
摘要翻译：有机过氧化物和过氧化氢的量热测定的简单而有效的系统。使用连接到聚乙烯管上的滑动材料的过氧化物笔包含两个可压碎的小瓶。两个可压碎的小瓶含有分配成干成分和液体成分的量热试剂。打扫怀疑的物质或表面后，小瓶破裂，将试剂充分混合，使试剂吸入滑动材料。有机过氧化物或过氧化氢的存在通过深蓝色证实。

3. 发明授权

US07829020B2 Simple, field portable colorimetric detection device for organic peroxides and hydrogen peroxide 有权
标题翻译：简单的现场便携式比色检测装置，用于有机过氧化物和过氧化氢
公开(公告)号：US07829020B2
公开(公告)日：2010-11-09
申请号：US12183210
申请日：2008-07-31
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman , John G. Reynolds , Peter Nunes , Sharon J. Shields
IPC分类号： G01N33/22
CPC分类号： G01N21/78 , G01N31/228 , Y10T29/49826 , Y10T436/206664
摘要： A simple and effective system for the colorimetric determination of organic peroxides and hydrogen peroxide. A peroxide pen utilizing a swipe material attached to a polyethylene tube contains two crushable vials. The two crushable vials contain a colorimetric reagent separated into dry ingredients and liquid ingredients. After swiping a suspected substance or surface the vials are broken, the reagent is mixed thoroughly and the reagent is allowed to wick into the swipe material. The presence of organic peroxides or hydrogen peroxide is confirmed by a deep blue color.
摘要翻译：用于比色测定有机过氧化物和过氧化氢的简单而有效的系统。使用连接到聚乙烯管上的滑动材料的过氧化物笔包含两个可压碎的小瓶。两个可压碎的小瓶包含分离成干成分和液体成分的比色试剂。打扫怀疑的物质或表面后，小瓶破裂，将试剂充分混合，使试剂吸入滑动材料。有机过氧化物或过氧化氢的存在通过深蓝色证实。

4. 发明申请

US20090221085A1 Thin-Layer Chromatography and Colorimetric Analysis of Multi-Component Explosive Mixtures 有权
标题翻译：多组分爆炸混合物的薄层色谱和比色分析
公开(公告)号：US20090221085A1
公开(公告)日：2009-09-03
申请号：US12106400
申请日：2008-04-21
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
IPC分类号： G01N30/90
CPC分类号： G01N30/94 , G01N30/90 , G01N33/22
摘要： A thin-layer chromatography method for detection and identification of common military and peroxide explosives in samples includes the steps of provide a reverse-phase thin-layer chromatography plate; prepare the plate by marking spots on which to deposit the samples by touching the plate with a marker; spot one micro liter of a first standard onto one of the spots, spot one micro liter of a second standard onto another of the spots, and spot samples onto other of spots producing a spotted plate; add eluent to a developing chamber; add the spotted plate to the developing chamber; remove the spotted plate from the developing chamber producing a developed plate; place the developed plate in an ultraviolet light box; add a visualization agent to a dip tank; dip the developed plate in the dip tank and remove the developed plate quickly; and detect explosives by viewing said developed plate.
摘要翻译：用于检测和鉴定样品中常见的军用和过氧化物炸药的薄层色谱法包括提供反相薄层色谱板的步骤; 通过用标记触摸板来标记沉积样品的斑点来准备板; 将一微升第一标准物放在其中一个斑点上，将一微升第二标准物放在另一个斑点上，并将样品点样到产生斑点板的其他斑点上; 将洗脱液加入显影室; 将点样板加到显影室; 从显影室中取出点样板，产生显影板; 将显影的板放在紫外灯箱中; 将一个可视化代理添加到浸槽中; 将显影的板块浸入浸渍槽中，快速取出显影板; 并通过查看所述显影板来检测爆炸物。

5. 发明授权

US08815606B2 Thin-layer chromatography and colorimetric analysis of multi-component explosive mixtures 有权
标题翻译：多组分爆炸性混合物的薄层色谱和比色分析
公开(公告)号：US08815606B2
公开(公告)日：2014-08-26
申请号：US12106400
申请日：2008-04-21
申请人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
发明人： Philip F. Pagoria , Alexander R. Mitchell , Richard E. Whipple , M. Leslie Carman
IPC分类号： G01N30/90 , G01N30/96
CPC分类号： G01N30/94 , G01N30/90 , G01N33/22
摘要： A thin-layer chromatography method for detection and identification of common military and peroxide explosives in samples includes the steps of provide a reverse-phase thin-layer chromatography plate; prepare the plate by marking spots on which to deposit the samples by touching the plate with a marker; spot one micro liter of a first standard onto one of the spots, spot one micro liter of a second standard onto another of the spots, and spot samples onto other of spots producing a spotted plate; add eluent to a developing chamber; add the spotted plate to the developing chamber; remove the spotted plate from the developing chamber producing a developed plate; place the developed plate in an ultraviolet light box; add a visualization agent to a dip tank; dip the developed plate in the dip tank and remove the developed plate quickly; and detect explosives by viewing said developed plate.
摘要翻译：用于检测和鉴定样品中常见的军用和过氧化物炸药的薄层色谱法包括提供反相薄层色谱板的步骤; 通过用标记触摸板来标记沉积样品的斑点来准备板; 将一微升第一标准物放在其中一个斑点上，将一微升第二标准物放在另一个斑点上，并将样品点样到产生斑点板的其他斑点上; 将洗脱液加入显影室; 将点样板加到显影室; 从显影室中取出点样板，产生显影板; 将显影的板放在紫外灯箱中; 将一个可视化代理添加到浸槽中; 将显影的板块浸入浸渍槽中，快速取出显影板; 并通过查看所述显影板来检测爆炸物。

6. 发明授权

US08669115B2 Spot test kit for explosives detection 有权
标题翻译：用于爆炸物检测的现货测试套件
公开(公告)号：US08669115B2
公开(公告)日：2014-03-11
申请号：US12785299
申请日：2010-05-21
申请人： Philip F. Pagoria , Richard E. Whipple , Peter J. Nunes , Joel Del Eckels , John G. Reynolds , Robin R. Miles , Marina L. Chiarappa-Zucca
发明人： Philip F. Pagoria , Richard E. Whipple , Peter J. Nunes , Joel Del Eckels , John G. Reynolds , Robin R. Miles , Marina L. Chiarappa-Zucca
IPC分类号： G01N21/00
CPC分类号： G01N31/22 , B01L3/5023 , B01L3/5029 , B01L2200/16 , B01L2300/0867 , B01L2300/1827 , B01L2300/1877 , B01L2400/0406 , B01L2400/0683 , G01N1/02 , G01N33/227 , G01N2001/022 , G01N2001/028
摘要： An explosion tester system comprising a body, a lateral flow membrane swab unit adapted to be removeably connected to the body, a first explosives detecting reagent, a first reagent holder and dispenser operatively connected to the body, the first reagent holder and dispenser containing the first explosives detecting reagent and positioned to deliver the first explosives detecting reagent to the lateral flow membrane swab unit when the lateral flow membrane swab unit is connected to the body, a second explosives detecting reagent, and a second reagent holder and dispenser operatively connected to the body, the second reagent holder and dispenser containing the second explosives detecting reagent and positioned to deliver the second explosives detecting reagent to the lateral flow membrane swab unit when the lateral flow membrane swab unit is connected to the body.
摘要翻译：一种爆炸测试器系统，包括主体，适于可移除地连接到主体的侧面流动的薄膜拭子单元，第一爆炸物检测试剂，可操作地连接到主体的第一试剂保持器和分配器，第一试剂保持器和分配器包含第一爆炸物检测试剂，并且定位成当侧流膜拭子单元连接到身体时将第一炸药检测试剂输送到侧流膜拭子单元，第二爆炸物检测试剂和可操作地连接到身体的第二试剂保持器和分配器，所述第二试剂保持器和分配器包含所述第二炸药检测试剂，并且定位成当所述侧流膜拭子单元连接到所述主体时将所述第二炸药检测试剂输送到所述侧流膜拭子单元。

7. 发明申请

US20100229633A1 Spot Test Kit For Explosives Detection 有权
标题翻译：爆炸物检测用现货检测套件
公开(公告)号：US20100229633A1
公开(公告)日：2010-09-16
申请号：US12785299
申请日：2010-05-21
申请人： Philip F. Pagoria , Richard E. Whipple , Peter J. Nunes , Joel Del Eckels , John G. Reynolds , Robin R. Miles , Marina L. Chiarappa-Zucca
发明人： Philip F. Pagoria , Richard E. Whipple , Peter J. Nunes , Joel Del Eckels , John G. Reynolds , Robin R. Miles , Marina L. Chiarappa-Zucca
IPC分类号： G01N33/22
CPC分类号： G01N31/22 , B01L3/5023 , B01L3/5029 , B01L2200/16 , B01L2300/0867 , B01L2300/1827 , B01L2300/1877 , B01L2400/0406 , B01L2400/0683 , G01N1/02 , G01N33/227 , G01N2001/022 , G01N2001/028
摘要： An explosion tester system comprising a body, a lateral flow membrane swab unit adapted to be removeably connected to the body, a first explosives detecting reagent, a first reagent holder and dispenser operatively connected to the body, the first reagent holder and dispenser containing the first explosives detecting reagent and positioned to deliver the first explosives detecting reagent to the lateral flow membrane swab unit when the lateral flow membrane swab unit is connected to the body, a second explosives detecting reagent, and a second reagent holder and dispenser operatively connected to the body, the second reagent holder and dispenser containing the second explosives detecting reagent and positioned to deliver the second explosives detecting reagent to the lateral flow membrane swab unit when the lateral flow membrane swab unit is connected to the body.
摘要翻译：一种爆炸测试器系统，包括主体，适于可移除地连接到主体的侧面流动的薄膜拭子单元，第一爆炸物检测试剂，可操作地连接到主体的第一试剂保持器和分配器，第一试剂保持器和分配器包含第一爆炸物检测试剂，并且定位成当侧流膜拭子单元连接到身体时将第一炸药检测试剂输送到侧流膜拭子单元，第二爆炸物检测试剂和可操作地连接到身体的第二试剂保持器和分配器，所述第二试剂保持器和分配器包含所述第二炸药检测试剂，并且定位成当所述侧流膜拭子单元连接到所述主体时将所述第二炸药检测试剂输送到所述侧流膜拭子单元。

8. 发明授权

US07939029B2 Chemical analysis kit for the presence of explosives 有权
标题翻译：爆炸物存在的化学分析试剂盒
公开(公告)号：US07939029B2
公开(公告)日：2011-05-10
申请号：US11158480
申请日：2005-06-21
申请人： Joel Del Eckels , Peter J. Nunes , Armando Alcaraz , Richard E. Whipple
发明人： Joel Del Eckels , Peter J. Nunes , Armando Alcaraz , Richard E. Whipple
IPC分类号： G01N33/00
CPC分类号： B01L3/5029 , B01L2300/1827 , G01N1/02 , G01N33/22 , G01N2001/027 , G01N2001/028
摘要： A tester for testing for explosives associated with a test location comprising a first explosives detecting reagent; a first reagent holder, the first reagent holder containing the first explosives detecting reagent; a second explosives detecting reagent; a second reagent holder, the second reagent holder containing the second explosives detecting reagent; a sample collection unit for exposure to the test location, exposure to the first explosives detecting reagent, and exposure to the second explosives detecting reagent; and a body unit containing a heater for heating the sample collection unit for testing the test location for the explosives.
摘要翻译：用于测试与测试位置相关联的爆炸物的测试器，包括第一爆炸物检测试剂; 第一试剂架，所述第一试剂架包含所述第一爆炸物检测试剂; 第二种爆炸物检测试剂; 第二试剂架，所述第二试剂架包含所述第二炸药检测试剂; 用于暴露于测试位置的样品收集单元，暴露于第一炸药检测试剂，以及暴露于第二炸药检测试剂; 以及包含加热器的身体单元，用于加热用于测试爆炸物的测试位置的样本收集单元。

9. 发明授权

US07771653B2 Explosives tester with heater 有权
标题翻译：具有加热器的爆炸物测试仪
公开(公告)号：US07771653B2
公开(公告)日：2010-08-10
申请号：US11593257
申请日：2006-11-01
申请人： Joel Del Eckels , Peter J. Nunes , Randall L. Simpson , Richard E. Whipple , J. Chance Carter , John G. Reynolds
发明人： Joel Del Eckels , Peter J. Nunes , Randall L. Simpson , Richard E. Whipple , J. Chance Carter , John G. Reynolds
IPC分类号： G01N33/00
CPC分类号： G01N21/78 , G01N2001/024 , G01N2001/028 , G01N2021/786
摘要： An inspection tester system for testing for explosives. The tester includes a body and a swab unit adapted to be removeably connected to the body. At least one reagent holder and dispenser is operatively connected to the body. The reagent holder and dispenser contains an explosives detecting reagent and is positioned to deliver the explosives detecting reagent to the swab unit. A heater is operatively connected to the body and the swab unit is adapted to be operatively connected to the heater.
摘要翻译：用于爆炸物检测的检验测试仪系统。测试器包括适于可移除地连接到身体的主体和棉签单元。至少一个试剂保持器和分配器可操作地连接到主体。试剂保持器和分配器包含爆炸物检测试剂，并定位成将炸药检测试剂输送到拭子单元。加热器可操作地连接到主体，并且拭子单元适于可操作地连接到加热器。

10. 发明授权

US4248730A Evaporation-based Ge/.sup.68 Ga Separation 失效
标题翻译：基于蒸发的Ge / 68Ga分离
公开(公告)号：US4248730A
公开(公告)日：1981-02-03
申请号：US74855
申请日：1979-09-13
申请人： Saed Mirzadeh , Richard E. Whipple , Patrick M. Grant , Harold A. O'Brien, Jr.
发明人： Saed Mirzadeh , Richard E. Whipple , Patrick M. Grant , Harold A. O'Brien, Jr.
IPC分类号： G21G4/08 , C09K3/00 , C09K11/04
CPC分类号： G21G4/08
摘要： Micro concentrations of .sup.68 Ga in secular equilibrium with .sup.68 Ge in strong aqueous HCl solution may readily be separated in ionic form from the .sup.68 Ge for biomedical use by evaporating the solution to dryness and then leaching the .sup.68 Ga from the container walls with dilute aqueous solutions of HCl or NaCl. The chloro-germanide produced during the evaporation may be quantitatively recovered to be used again as a source of .sup.68 Ga. If the solution is distilled to remove any oxidizing agents which may be present as impurities, the separation factor may easily exceed 10.sup.5. The separation is easily completed and the .sup.68 Ga made available in ionic form in 30 minutes or less.
摘要翻译：通过将溶液蒸发至干，然后用稀释的HCl或NaCl水溶液从容器壁中浸出68Ga，可将离子形式的68Ge与68Ge在强HCl水溶液中的微量浓度容易地与68Ge分离，用于生物医学用途。。在蒸发期间产生的氯代锗烷可以定量回收再次用作68Ga的来源。如果蒸馏溶液以除去可能作为杂质存在的任何氧化剂，则分离因子可能容易超过105.分离容易完成，并且在30分钟或更短时间内可以以离子形式提供68Ga。

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