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1. 发明授权

US5760099A Production of rigid or semirigid polyurethane foams and composite elements comprising such polyurethane foams 失效
标题翻译：制备刚性或半刚性聚氨酯泡沫和包含这种聚氨酯泡沫的复合元件
公开(公告)号：US5760099A
公开(公告)日：1998-06-02
申请号：US711452
申请日：1996-09-06
申请人： Peter Horn , Gerhard Lehr , Sarbananda Chakrabarti , Dieter Hertel , Ludwig Jung
发明人： Peter Horn , Gerhard Lehr , Sarbananda Chakrabarti , Dieter Hertel , Ludwig Jung
IPC分类号： C08J9/02 , B32B27/30 , B32B27/40 , C08G18/00 , C08G18/08 , C08G18/40 , C08J9/00 , C08J9/14 , C08L75/00 , C08J9/06
CPC分类号： C08J9/0061 , C08J9/0033 , C08J9/0038 , C08J2375/04 , C08J2471/00
摘要： Rigid polyurethane foams, preferably semirigid polyurethane foams, are produced by reacting an organic and/or modified organic polyisocyanates with relatively high molecular weight polyhydroxyl compounds and, optionally, low molecular weight chain extenders and/or crosslinkers in the presence of water or mixtures of water and physically acting blowing agents, optionally, catalysts, at least one additive selected from the group consisting of sulfonate salts of an acid group-containing alkylene oxide polymer, a phosphonate salt of an acid group-containing alkylene oxide polymer, and mixtures thereof, additional other additives and optionally, auxiliaries. The polyurethane foams produced by this process can be used to produce composite comprising at least one covering layer and at least one layer comprising a rigid or semirigid polyurethane foam produced by the process of the present invention.
摘要翻译：刚性聚氨酯泡沫，优选半刚性聚氨酯泡沫，通过有机和/或改性的有机多异氰酸酯与相对高分子量的多羟基化合物和任选的低分子量增链剂和/或交联剂在水或水的混合物和物理作用的发泡剂，任选的催化剂，至少一种选自含酸基的烯化氧聚合物的磺酸盐，含酸基的烯化氧聚合物的膦酸盐及其混合物的添加剂，另外其他添加剂和任选的助剂。通过该方法生产的聚氨酯泡沫可用于生产包含至少一个覆盖层和至少一层包含通过本发明方法制备的刚性或半刚性聚氨酯泡沫的层的复合材料。

2. 发明授权

US5539134A Process for the preparation of N-alkanoyl-polyhydroxyalkylamines 失效
标题翻译：制备N-烷酰基 - 多羟基烷基胺的方法
公开(公告)号：US5539134A
公开(公告)日：1996-07-23
申请号：US325182
申请日：1995-04-24
申请人： Beate Strecker , Helmut Wolf , Gerhard Wolf , Alfred Oftring , Hans-Heinrich Bechtolsheimer , Dieter Hertel
发明人： Beate Strecker , Helmut Wolf , Gerhard Wolf , Alfred Oftring , Hans-Heinrich Bechtolsheimer , Dieter Hertel
IPC分类号： C07C231/02 , C07C233/18 , C07C231/00
CPC分类号： C07C231/02
摘要： The preparation von N-alkanoyl-polyhydroxyalkylamines I in which ##STR1## in which Z stands for the polyhydroxyalkyl radical of a monosaccharide or oligosaccharide,R.sup.1 denotes hydrogen or C.sub.1 -C.sub.8 alkyl andR.sup.2 denotes C.sub.1 -C.sub.21 alkyl, by the reaction of polyhydroxyalkylamines of the general formula IIZ--NH--R.sup.1 (II),with alkyl carboxylates of the general formula III ##STR2## in which R.sup.3 denotes a C.sub.1 -C.sub.4 alkyl radical,in the presence of a basic catalyst, in which(a) all of the ester III is placed in the reactor and is heated to the reaction temperature, and the amine II is metered in in the form of a melt while the reaction proceeds, while alcohol R.sup.3 --OH formed is continuously removed by distillation,(b) the reaction is carried out at a temperature of from 55.degree. to 110.degree. C., and(c) the reaction is carried out in the absence of organic solvents.
摘要翻译： PCT No.PCT / EP93 / 02852 Sec。 371日期1995年04月24日 102（e）1995年4月24日PCT PCT 1993年10月15日PCT公布。公开号WO94 / 10130 日期1994年5月11日其中Z代表单糖或寡糖的多羟基羟基烷基的R1代表氢或C1-C8烷基，R2表示C1-C21烷基，通过通式IIZ-NH-R1（II）的多羟基烷基胺与通式III的烷基羧酸盐（III）反应，其中R 3表示C 1 -C 4烷基，在碱存在下催化剂，其中（a）将所有酯III置于反应器中并加热至反应温度，并且当反应进行时，以熔体形式计量胺II，而形成的醇R3-OH为通过蒸馏连续除去，（b）反应在55℃至110℃的温度下进行，和（c）反应在不存在有机溶剂的情况下进行。

3. 发明授权

US5856538A Preparation of N-acylamino carboxylic acids and N-acylamino sulfonic acids and their alkali metal salts 失效
标题翻译：制备N-酰基氨基羧酸和N-酰基氨基磺酸及其碱金属盐
公开(公告)号：US5856538A
公开(公告)日：1999-01-05
申请号：US809139
申请日：1997-03-24
申请人： Beate Strecker , Alfred Oftring , Dieter Hertel , Georg Schuh
发明人： Beate Strecker , Alfred Oftring , Dieter Hertel , Georg Schuh
IPC分类号： C07B61/00 , C07C231/02 , C07C233/47 , C07C303/22 , C07C303/32 , C07C309/15 , C07C231/00 , C07C205/00 , C07C229/00
CPC分类号： C07C303/22 , C07C231/02 , C07C233/47 , C07C303/32
摘要： N-acylamino carboxylic acids and N-acylamino sulfonic acids and their alkali metal salts from the technical alkali metal salts of amino carboxylic acids and amino sulfonic acids, respectively, with an active content of 50-95% by weight, based on the solids content of the technical alkali metal salts, and from alkyl carboxylates, are prepared by(a) preparing a suspension of the solid anhydrous technical alkali metal salts of the amino carboxylic acids or amino sulfonic acids in the alkyl carboxylates,(b) reacting this suspension by adding more than 30 to 150 mol % of strong bases to give the alkali metal salts of the N-acylamino carboxylic acids or N-acylamino sulfonic acids, and(c) if required preparing therefrom the free N-acylamino carboxylic acids or N-acylamino sulfonic acids in a conventional way by adding acids.
摘要翻译： PCT No.PCT / EP95 / 03584 371日期1997年3月24日 102（e）1997年3月24日PCT PCT 1995年9月12日PCT公布。出版物WO96 / 09278 日期1996年3月28日N-酰氨基羧酸和N-酰氨基磺酸及其碱金属盐分别来自氨基羧酸和氨基磺酸的工业碱金属盐，活性含量为50-95重量％（a）制备氨基羧酸或氨基磺酸的固体无水工业碱金属盐在羧酸烷基酯中的悬浮液（b），其基于工业碱金属盐和羧酸烷基酯的固体含量，（b））通过加入大于30至150mol％的强碱使该悬浮液反应得到N-酰基氨基羧酸或N-酰基氨基磺酸的碱金属盐，和（c）如果需要，由游离的N-酰基氨基羧酸酸或N-酰氨基磺酸以常规方式加入酸。

4. 发明授权

US5554742A Preparation of alkyl glycosides 失效
标题翻译：烷基糖苷的制备
公开(公告)号：US5554742A
公开(公告)日：1996-09-10
申请号：US295795
申请日：1994-09-15
申请人： Gerhard Wolf , Alfred Oftring , Georg Schuh , Helmut Wolf , Rudolf Alt , Hans-Heinrich Bechtolsheimer , Dieter Hertel
发明人： Gerhard Wolf , Alfred Oftring , Georg Schuh , Helmut Wolf , Rudolf Alt , Hans-Heinrich Bechtolsheimer , Dieter Hertel
IPC分类号： C07H15/04 , C07H1/00
CPC分类号： C07H15/04
摘要： The preparation of alkyl glycosides by reaction of aqueous glycoses having a water content of 10-80% by weight with aliphatic primary alcohols having from 5 to 30 C atoms is described, in which(a) the alcohols and the glycoses are employed in a molar ratio of 2:1 to 10:1,(b) 0.1-5% by weight, based on the amount of the glycoses employed, of the acidic form of an anionic surfactant is used as the acidic catalyst having emulsifying properties,(c) 1-30% by weight, based on the amount of the glycoses employed, of alkyl glycosides is used as a further emulsifier,(d) the aqueous glycose is preheated to 50.degree.-90.degree. C. and the preheated aqueous solution of the glycose is metered with effective mixing into the reaction mixture of alcohol, acidic catalyst and emulsifier in such a manner that an emulsion is formed,(e) the reaction is carried out at from 100.degree. to 150.degree. C. and from 10 to 100 mbar, the water introduced into the reaction mixture and the water formed by the reaction being continuously removed by distillation,(f) after the reaction has ended, the acidic catalyst is neutralized by addition of a base such that the resulting mixture has a pH of 8-10, then(g) the excess alcohol is removed by distillation at from 0.01 to 10 mbar down to a residual content of less than 5% by weight, based on the amount of alkyl glycoside present, and(h) the reaction mixture is bleached at pH 8-10 after conversion into an aqueous paste having a content of from 30 to 70% by weight of alkyl glycoside using a compound eliminating active oxygen.
摘要翻译： PCT No.PCT / EP93 / 00791 Sec。 371日期1994年9月15日 102（e）1994年9月15日PCT 1993年4月1日PCT PCT。出版物WO93 / 21196 日期：1993年10月28日描述了通过水含量为10-80％（重量）的水性糖苷与具有5至30个碳原子的脂族伯醇反应制备烷基糖苷，其中（a）醇和糖以摩尔比为2：1至10：1使用，（b）0.1-95重量％，基于所用糖苷的量，酸性形式的阴离子表面活性剂用作具有乳化性的酸性催化剂性质，（c）基于所用糖糖的量，将1-30重量％的烷基糖苷用作另外的乳化剂，（d）将糖水溶液预热至50-90℃，将预热的以醇，酸性催化剂和乳化剂的反应混合物中有效混合糖的水溶液，使得形成乳液，（e）反应在100-150℃和从 10至100毫巴，引入反应混合物中的水和由t形成的水通过蒸馏连续除去反应，（f）反应结束后，通过加入碱中和酸性催化剂，使得所得混合物的pH值为8-10，然后（g）过量的醇通过以0.01至10毫巴蒸馏至基于存在的烷基糖苷的量小于5重量％的残留含量，和（h）将反应混合物在转化成具有使用除去活性氧的化合物，含有30〜70重量％的烷基糖苷。

5. 发明授权

US5942635A Continuous preparation of N-acylamino carboxylic acids and N-acylamino sulphonic acids, and their alkali metal salts 失效
标题翻译：连续制备N-酰基氨基羧酸和N-酰基氨基磺酸及其碱金属盐
公开(公告)号：US5942635A
公开(公告)日：1999-08-24
申请号：US68012
申请日：1998-04-30
申请人： Beate Ehle , Georg Schuh , Martin aus dem Kahmen , Dieter Hertel
发明人： Beate Ehle , Georg Schuh , Martin aus dem Kahmen , Dieter Hertel
IPC分类号： C07C231/02 , C07C233/47 , C07C233/49 , C07C309/15 , C07C231/00
CPC分类号： C07C231/02
摘要： In a process and an apparatus for the continuous preparation of N-acylamino carboxylic acids and N-acylamino sulfonic acids, and their alkali metal salts, from the alkali metal salts of amino carboxylic acids and amino sulfonic acids, respectively, and carbonyl halides in a reactor designed as circulating circuit, the reactants are fed for immediate reaction into the circulating circuit, and a part of the product solution corresponding to the amount fed in is continuously discharged from the circulating circuit. The reactants are circulated by a circulating pump. The temperature in the reactors is controlled. The heat produced in the reaction is removed.
摘要翻译： PCT No.PCT / EP96 / 04723 Sec。 371日期：1998年4月30日 102（e）1998年4月30日PCT PCT 1996年10月30日PCT公布。公开号WO97 / 16409 日期1997年5月9日在氨基羧酸和氨基磺酸的碱金属盐分别连续制备N-酰基氨基羧酸和N-酰基氨基磺酸及其碱金属盐的方法和装置中，设计为循环回路的反应器中的羰基卤化物，将反应物供给立即反应进入循环回路，并且与进料量对应的一部分产物溶液从循环回路连续排出。反应物通过循环泵循环。控制反应器中的温度。除去反应产生的热量。

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