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1. 发明授权

US5273663A Oxidative removal of aqueous cyanide under acidic conditions 失效
标题翻译：在酸性条件下氧化氰化水
公开(公告)号：US5273663A
公开(公告)日：1993-12-28
申请号：US16355
申请日：1993-02-11
申请人： Paul R. Kurek , Robert R. Frame , Tom N. Kalnes , Mark D. Moser
发明人： Paul R. Kurek , Robert R. Frame , Tom N. Kalnes , Mark D. Moser
IPC分类号： C02F1/72 , C02F1/78 , C02F9/00 , C02F11/08
CPC分类号： C02F9/00 , C02F11/08 , C02F1/72 , C02F1/722 , C02F1/725 , C02F1/78 , C02F2101/18 , Y10S210/904
摘要： The oxidation of cyanide under acid conditions using oxygen as the oxidizing agent can be effected under mild reaction conditions when certain metal chelates are used as catalysts. Especially effective chelates are metal phthalocyanines, particularly where the metal is vanadium or a member of the iron group metals. The oxidation can be effected homogeneously using water soluble metal chelates, or can be performed heterogeneously, especially in a continuous fashion using a packed bed reactor, by using suitable water-insoluble metal chelates, especially when supported on appropriate carriers.
摘要翻译：使用氧作为氧化剂的酸性条件下氰化物的氧化可以在温和的反应条件下进行，当某些金属螯合物用作催化剂时。特别有效的螯合物是金属酞菁，特别是金属是钒或铁族金属的成分时。可以使用水溶性金属螯合物均匀地进行氧化，或者通过使用合适的水不溶性金属螯合物，特别是当在适当的载体上负载时，可以使用填充床反应器，特别是以连续的方式进行非均匀地进行氧化。

2. 发明授权

US5376285A Oxidative removal of aqueous metal-complexed cyanide under acidic conditions 失效
标题翻译：在酸性条件下氧化除去金属络合的氰化物水溶液
公开(公告)号：US5376285A
公开(公告)日：1994-12-27
申请号：US150294
申请日：1993-11-12
申请人： Paul R. Kurek , Robert R. Frame , Tom N. Kalnes , Mark D. Moser
发明人： Paul R. Kurek , Robert R. Frame , Tom N. Kalnes , Mark D. Moser
IPC分类号： C02F1/72 , C02F1/78 , C02F9/00 , C02F11/08
CPC分类号： C02F9/00 , C02F11/08 , C02F1/72 , C02F1/722 , C02F1/725 , C02F1/78 , C02F2101/18 , Y10S210/904
摘要： The oxidation of metal-complexed cyanide under acid conditions using oxygen as the oxidizing agent can be performed effectively with certain metal chelates as catalysts. Especially effective chelates are metal phthalocyanines, particularly where the metal is vanadium or a member of the iron group metals. The oxidation can be effected homogeneously using water soluble metal chelates, or can be performed heterogeneously, especially in a continuous fashion using a packed bed reactor, by using suitable water-insoluble metal chelates, especially when supported on appropriate carriers.
摘要翻译：使用氧作为氧化剂的酸性条件下金属络合的氰化物的氧化可以用某些金属螯合物作为催化剂有效地进行。特别有效的螯合物是金属酞菁，特别是金属是钒或铁族金属成分时。可以使用水溶性金属螯合物均匀地进行氧化，或者通过使用合适的水不溶性金属螯合物，特别是当在适当的载体上负载时，可以使用填充床反应器，特别是以连续的方式进行非均匀地进行氧化。

3. 发明授权

US5120453A Oxidative removal of cyanide from aqueous streams 失效
标题翻译：从水流中氧化氰化物
公开(公告)号：US5120453A
公开(公告)日：1992-06-09
申请号：US632798
申请日：1990-12-24
申请人： Robert R. Frame , Tom N. Kalnes , Mark D. Moser
发明人： Robert R. Frame , Tom N. Kalnes , Mark D. Moser
IPC分类号： C02F1/58 , B01J31/12 , B01J31/16 , B01J31/18 , C02F20060101 , C02F1/32 , C02F1/72 , C02F1/74 , C02F1/78 , C02F9/00
CPC分类号： B01J31/183 , B01J31/1616 , B01J31/1815 , C02F1/72 , C02F1/725 , B01J2531/025 , B01J2531/56 , B01J2531/842 , B01J2531/845 , B01J2531/96 , C02F1/32 , C02F1/722 , C02F1/74 , C02F1/78 , C02F2101/18 , C02F2101/20 , Y10S210/904
摘要： The oxidation of cyanide using oxygen as the oxidizing agent can be effected under mild reaction conditions when certain metal chelates are used as catalysts. Especially effective chelates are metal phthalocyanines, particularly where the metal is vanadium or a member of the iron group metals. The oxidation can be effected homogeneously using water soluble metal chelates, or can be performed heterogeneously, especially in a continuous fashion using a packed bed reactor, by using suitable water-insoluble metal chelates, especially when supported on appropriate carriers.
摘要翻译：使用氧作为氧化剂的氰化物的氧化可以在温和的反应条件下，当某些金属螯合物用作催化剂时。特别有效的螯合物是金属酞菁，特别是金属是钒或铁族金属的成分时。可以使用水溶性金属螯合物均匀地进行氧化，或者通过使用合适的水不溶性金属螯合物，特别是当在适当的载体上负载时，可以使用填充床反应器，特别是以连续的方式进行非均匀地进行氧化。

4. 发明授权

US5238581A Oxidative removal of cyanide from aqueous streams abetted by ultraviolet irradiation 失效
标题翻译：通过紫外线照射从水流中氧化除去氰化物
公开(公告)号：US5238581A
公开(公告)日：1993-08-24
申请号：US862149
申请日：1992-04-02
申请人： Robert R. Frame , Tom N. Kalnes , Mark D. Moser
发明人： Robert R. Frame , Tom N. Kalnes , Mark D. Moser
IPC分类号： C02F1/58 , B01J31/12 , B01J31/16 , B01J31/18 , C02F20060101 , C02F1/32 , C02F1/72 , C02F1/74 , C02F1/78 , C02F9/00
CPC分类号： B01J31/183 , B01J31/1616 , B01J31/1815 , C02F1/72 , C02F1/725 , B01J2531/025 , B01J2531/56 , B01J2531/842 , B01J2531/845 , B01J2531/96 , C02F1/32 , C02F1/722 , C02F1/74 , C02F1/78 , C02F2101/18 , C02F2101/20 , Y10S210/904
摘要： The oxidation of complexed cyanide using oxygen as the oxidizing agent when certain metal chelates are used as catalysts may be enhanced by irradiating the complexed cyanide with ultraviolet light prior to or concurrent with the oxidation. Especially effective chelates are metal phthalocyanines, particularly where the metal is vanadium or a member of the iron group metals. The oxidation can be effected homogeneously using water soluble metal chelates, or can be performed heterogeneously, especially in a continuous fashion using a packed bed reactor, by using suitable water-insoluble metal chelates, especially when supported on appropriate carriers.
摘要翻译：当使用某些金属螯合物作为催化剂时，使用氧作为氧化剂的络合氰化物的氧化可以通过在氧化之前或同时用紫外线照射络合的氰化物来增强。特别有效的螯合物是金属酞菁，特别是金属是钒或铁族金属的成分时。可以使用水溶性金属螯合物均匀地进行氧化，或者通过使用合适的水不溶性金属螯合物，特别是当在适当的载体上负载时，可以使用填充床反应器，特别是以连续的方式进行非均匀地进行氧化。

5. 发明授权

US5705078A Oxidative removal of aqueous cyanide by manganese(IV)-containing oxides 失效
标题翻译：通过含锰（IV）的氧化物氧化除去氰化水溶液
公开(公告)号：US5705078A
公开(公告)日：1998-01-06
申请号：US707985
申请日：1996-08-23
申请人： Paul R. Kurek , Tom N. Kalnes , Gregory John Lewis
发明人： Paul R. Kurek , Tom N. Kalnes , Gregory John Lewis
IPC分类号： C02F1/72 , C02F1/74 , C02F1/78
CPC分类号： C02F1/74 , C02F1/725 , C02F1/722 , C02F1/78 , C02F2101/18 , Y10S210/904
摘要： Manganese(IV)-containing oxides are effective catalysts for oxidation of water-soluble cyanide over a wide pH range (0.5-12) and temperature (15.degree.-250.degree. C.). Oxygen is the preferred oxidizing agent at partial pressures between about 0.2 and 5 atmospheres (2.9-75 psi, 20-517 kPa). Electrolytically deposited MnO.sub.2 is one preferred form of the catalyst. Another preferred manganese(IV)-containing oxide is the group of cation-stabilized manganese(IV)-containing oxides illustrated by cryptomelane. Yet another preferred form of manganese(IV)-containing oxide is a group of crystalline manganese phosphate compositions having an extended network and an empirical composition on an anhydrous basis expressed by an empirical formula of: (A.sup.a+).sub.v (Mn.sup.b+)(M.sup.c+).sub.x P.sub.y O.sub.z where A is a templating agent selected from the group consisting of alkali metals, alkaline earth metals, hydronium ion, ammonium ion, organoammonium ions, and mixtures thereof, "a" represents a weighted average valence of A and varies from 1.0 to 2.0, "v" is the mole ratio of A to Mn and varies from about 0.1 to about 5, "b" is the average valence of Mn and has a value of greater than 3 to about 4, M is a metal selected from the group consisting of Al, Fe.sup.3+, Ca, Sn.sup.4+, Ti, Sb.sup.5+, and mixtures thereof, "x" is the mole ratio of M to Mn and varies from 0 to about 3.0, "c" is the weighted average valence of M and varies from about 1.0 to about 5.0, "y" is the mole ratio of P to Mn and varies from about 0.10 to about 5.0 and "z" is the mole ratio of O to Mn and has a value determined by the equation z=1/2(a.times.v+b+x.times.c+5.times.y).
摘要翻译：含有锰（IV）的氧化物是在宽pH范围（0.5-12）和温度（15-250℃）下氧化水溶性氰化物的有效催化剂。在约0.2和5个大气压（2.9-75psi，20-517kPa）之间的分压下，氧气是优选的氧化剂。电解沉积的MnO 2是催化剂的一种优选形式。另一种优选的含有锰（Ⅳ）的氧化物是由赤藓烷所示的阳离子稳定化的含锰（Ⅳ）的氧化物。另一种优选形式的含锰（IV）的氧化物是一组结晶磷酸锰组合物，其具有延伸的网络和无水基础上的经验组成，其经验式为：（Aa +）v（Mnb +）（Mc +）xPyOz A是选自碱金属，碱土金属，水合氢离子，铵离子，有机铵离子及其混合物的模板剂，“a”表示A的加权平均化合价，为1.0至2.0，“v “是A与Mn的摩尔比，在约0.1至约5之间变化，”b“是Mn的平均化合价并且具有大于3至约4的值，M是选自Al ，Fe 3+，Ca，Sn 4+，Ti，Sb 5+及其混合物，“x”是M与Mn的摩尔比，从0变化到约3.0，“c”是M的加权平均价，约5.0，“y”是P与Mn的摩尔比，约0.10至约5.0，“z”是mo O与Mn的比值，并且具有由方程z = + E，fra 1/2 + EE（axv + b + xxc + 5xy）确定的值。

6. 发明授权

US5773549A Process for hydrotreating an organic feedstock containing a halogenated component and contaminated with distillable oxygen and nitrogen compounds having boiling points lower than the halogenated compounds 失效
标题翻译：加氢处理含有卤化成分并受沸点低于卤代化合物的可蒸馏氧和氮化合物污染的有机原料的方法
公开(公告)号：US5773549A
公开(公告)日：1998-06-30
申请号：US822532
申请日：1997-03-24
申请人： Mark D. Moser , Tom N. Kalnes , Chwu-Ching Jan
发明人： Mark D. Moser , Tom N. Kalnes , Chwu-Ching Jan
IPC分类号： C10G45/02
CPC分类号： C10G45/02
摘要： The invention provides a process for hydrotreating an organic feedstock containing a halogenated component and contaminated with distillable oxygen compounds, and/or distillable nitrogen compounds having boiling points lower than the halogenated compounds by means of removing the distillable oxygen compounds and distillable nitrogen compounds with a fractionation zone and then contacting the resulting organic feedstock having a reduced concentration of distillable oxygen and nitrogen compounds and a gaseous recycle stream containing hydrogen with a hydrogenation catalyst in a hydrogenation reaction zone to produce an anhydrous liquid stream comprising hydrogenated hydrocarbonaceous compounds having a reduced concentration of organic halide and a hydrogen halide compound. The resulting effluent from the hydrogenation zone is optionally separated to produce a hydrogenated hydrocarbonaceous stream having a reduced level of halogen and an anhydrous stream comprising a hydrogen halide compound.
摘要翻译：本发明提供了一种加氢处理含有卤化组分并被可蒸馏的氧化合物和/或可蒸馏的氮化合物加热处理的方法，其中沸点低于卤代化合物，通过用分馏法除去可蒸馏的氧化合物和可蒸馏的氮化合物然后在氢化反应区中将具有降低浓度的可蒸馏氧和氮化合物的所得有机原料与含氢的气态再循环料流与氢化催化剂接触，以产生包含具有降低的有机物浓度的氢化烃类化合物的无水液体料流卤化物和卤化氢化合物。任选分离来自加氢区的所得流出物，以产生具有降低的卤素含量的氢化烃流和包含卤化氢化合物的无水流。

7. 发明授权

US5354931A Process for hydrotreating an organic feedstock containing oxygen compounds and a halogen component 失效
标题翻译：用于加氢处理含有氧化合物和卤素组分的有机原料的方法
公开(公告)号：US5354931A
公开(公告)日：1994-10-11
申请号：US28862
申请日：1993-03-10
申请人： Chwu-Ching Jan , Mark D. Moser , Tom N. Kalnes , George R. Hibel
发明人： Chwu-Ching Jan , Mark D. Moser , Tom N. Kalnes , George R. Hibel
IPC分类号： C01B7/00 , C01B7/01 , C07C1/26 , C07C5/00 , C01B7/07 , C10G25/00
CPC分类号： C01B7/00 , C01B7/01 , C07C1/26 , C07C2529/08 , C07C2529/70
摘要： The invention provides a process for hydrotreating an organic feedstock containing oxygen compounds and a halogen component by means of removing the oxygen compounds with an adsorbent and then contacting the resulting organic feedstock having a reduced concentration of oxygen compounds and a gaseous recycle stream containing hydrogen with a hydrogenation catalyst in a hydrogenation reaction zone to produce an anhydrous liquid stream comprising hydrogenated hydrocarbonaceous compounds having a reduced concentration of halogen and a hydrogen halide compound. The resulting effluent from the hydrogenation zone is optionally separated to produce a hydrogenated hydrocarbonaceous stream having a reduced level of halogen and an anhydrous stream comprising a hydrogen halide compound.
摘要翻译：本发明提供了一种通过用吸附剂除去氧化合物来加氢处理含有氧化合物和卤素组分的有机原料的方法，然后使得到的具有降低浓度的氧化合物的所得有机原料和含有氢的气态再循环料流与氢化催化剂，以产生包含具有降低的卤素浓度和卤化氢化合物的氢化烃类化合物的无水液体流。任选分离来自加氢区的所得流出物，以产生具有降低的卤素含量的氢化烃流和包含卤化氢化合物的无水流。

8. 发明授权

US5314614A Process for hydrotreating an organic feedstock containing olefinic compounds and a halogen component 失效
标题翻译：加氢处理含有烯烃化合物和卤素组分的有机原料的方法
公开(公告)号：US5314614A
公开(公告)日：1994-05-24
申请号：US899804
申请日：1992-06-17
申请人： Mark D. Moser , Tom N. Kalnes , Chwu-Ching Jan , George R. Hibel
发明人： Mark D. Moser , Tom N. Kalnes , Chwu-Ching Jan , George R. Hibel
IPC分类号： A62D3/00 , A62D3/34 , A62D3/37 , A62D101/20 , A62D101/22 , C01B7/01 , C10G49/00 , C10G15/02
CPC分类号： A62D3/37 , C01B7/01 , C10G49/007 , A62D2101/20 , A62D2101/22 , Y10S210/909
摘要： The invention provides a process for hydrotreating an organic feedstock containing thermally unstable compounds and a halogen component by means of contacting the organic feedstock and a gaseous recycle stream containing hydrogen and a hydrogen halide compound with a hydrogenation catalyst in a hydrogenation reaction zone to produce a hydrogenated hydrocarbonaceous stream having a reduced concentration of halogen and a halide compound stream. The resulting effluent from the hydrogenation zone is separated to produce a recycle stream containing a hydrogen halide compound.
摘要翻译：本发明提供了一种通过使含有热不稳定化合物和卤素组分的有机原料加氢处理的方法，该方法是通过在氢化反应区中将有机原料和含有氢和卤化氢化合物的气态循环物流与氢化催化剂接触以产生氢化具有降低的卤素浓度和卤化物化合物流的烃流。将来自加氢区的所得流出物分离以产生含有卤化氢化合物的再循环流。

9. 发明授权

US09284494B2 Solids management in slurry hydroprocessing 有权
标题翻译：浆料加氢处理中的固体管理
公开(公告)号：US09284494B2
公开(公告)日：2016-03-15
申请号：US12271857
申请日：2008-11-15
申请人： Lorenz J. Bauer , Tom N. Kalnes , James F. McGehee
发明人： Lorenz J. Bauer , Tom N. Kalnes , James F. McGehee
IPC分类号： C10G67/04 , C10G47/26 , C10G67/02
CPC分类号： C10G47/26 , C10G67/02
摘要： The recovery of solids, and particularly solid particulates used as catalysts in slurry hydroprocessing, from asphaltene containing hydrocarbons is improved by controlling asphaltene precipitation. The formation of agglomerates of the solid particulates, having an increased diameter, results in the presence of precipitated asphaltenes, possibly due to flocculation. Asphaltene precipitation is controlled by varying process parameters or introducing additional diluent or flush streams that change the polarity of an asphaltene containing liquid product recovered from an effluent of a slurry hydroprocessing reaction zone.
摘要翻译：通过控制沥青质沉淀，改善了含沥青质烃的固体，特别是用作浆料加氢处理催化剂的固体颗粒。具有直径增加的固体颗粒的附聚物的形成导致沉淀的沥青质的存在，这可能是由于絮凝。沥青质沉淀通过变化的工艺参数控制或引入另外的稀释剂或冲洗流，其改变从浆料加氢处理反应区的流出物回收的含沥青质的液体产物的极性。

10. 发明授权

US08853476B2 Production of diesel fuel from biorenewable feedstocks with heat integration 有权
标题翻译：从具有热集成的生物可再生原料生产柴油
公开(公告)号：US08853476B2
公开(公告)日：2014-10-07
申请号：US13029297
申请日：2011-02-17
申请人： Tom N. Kalnes , John P. Brady , Marco Di Stanislao
发明人： Tom N. Kalnes , John P. Brady , Marco Di Stanislao
IPC分类号： C07C1/00 , C10G3/00
CPC分类号： C10G3/45 , C10G3/46 , C10G3/47 , C10G3/50 , C10G2300/1014 , C10G2300/1018 , C10G2300/1022 , C10G2300/1037 , C10G2300/4081 , C10G2400/02 , C10G2400/04 , C10G2400/28 , C12N2310/30 , Y02E50/13 , Y02P30/20
摘要： A process has been developed for producing diesel boiling range fuel or fuel blending component from renewable feedstocks such as plant oils and greases. The process involves treating a renewable feedstock by hydrogenating and deoxygenating i.e. decarboxylating and/or hydrodeoxygenating to provide a hydrocarbon fraction useful as a diesel fuel. The hydrocarbon fraction is isomerized to improve cold flow properties. At least one interstage stream of the hydrogenating and deoxygenating reaction zone is heat exchanged with the feed to the isomerization reaction zone, and/or the effluent of the hydrogenating and deoxygenating reaction zone is heat exchanged with the feed to the isomerization reaction zone.
摘要翻译：已经开发了用于从可再生原料如植物油和油脂生产柴油沸程燃料或燃料混合组分的方法。该方法包括通过氢化和脱氧处理可再生原料，即脱羧和/或加氢脱氧以提供可用作柴油燃料的烃馏分。烃馏分异构化以改善冷流动性能。氢化和脱氧反应区的至少一个级间流与异构化反应区的进料热交换，和/或氢化和脱氧反应区的流出物与异构化反应区的进料热交换。

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