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1. 发明授权

US09732036B2 Compound having carbazole ring structure, and organic electroluminescent device 有权
公开(公告)号：US09732036B2
公开(公告)日：2017-08-15
申请号：US13391956
申请日：2010-08-25
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano
IPC分类号： H01L51/50 , C07D209/86 , C07D209/88 , C07D401/14 , C07D405/10 , C07D409/14 , C07D413/14 , C07D417/14 , C07D471/04 , C09K11/06 , H01L51/00 , H05B33/14
CPC分类号： C07D209/86 , C07D209/88 , C07D401/14 , C07D405/10 , C07D409/14 , C07D413/14 , C07D417/14 , C07D471/04 , C09K11/06 , C09K2211/1029 , H01L51/0061 , H01L51/5012 , H01L51/5016 , H01L51/5056 , H01L51/5096 , H05B33/14
摘要： [Problem]An organic compound of excellent characteristics is provided that exhibits excellent hole-injecting/transporting performance with electron blocking ability, and that has high stability in the thin-film state and high luminous efficiency, the organic compound being provided as material for an organic electroluminescent device having high efficiency and high durability. The invention also provides a high-efficient, high-durable organic electroluminescent device using the compound.[Means for Resolution] The compound is of the following general formula having a carbazole ring structure. The organic electroluminescent device includes a pair of electrodes, and one or more organic layers sandwiched between the pair of electrodes, and the compound is used as a constituent material of at least one organic layer.

2. 发明授权

US09306174B2 Organic electroluminescent device 有权
标题翻译：有机电致发光器件
公开(公告)号：US09306174B2
公开(公告)日：2016-04-05
申请号：US13503156
申请日：2010-10-22
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano , Eiji Takahashi
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano , Eiji Takahashi
IPC分类号： H01L51/50 , H01L51/00 , H05B33/20
CPC分类号： H01L51/0072 , H01L51/0059 , H01L51/0085 , H01L51/5016 , H01L51/5096 , H05B33/20
摘要： A high-efficiency, high-durability organic electroluminescent device, particularly a phosphorescent organic electroluminescent device is provided by using an organic compound of excellent characteristics that exhibits excellent hole-injecting/transporting performance and has high triplet exciton confining capability with an electron blocking ability, and that has high stability in the thin-film state and high luminous efficiency.The organic electroluminescent device includes a pair of electrodes, and a plurality of organic layers sandwiched between the pair of electrodes and including a light emitting layer and an electron blocking layer, wherein a compound of the following general formula (1) having a carbazole ring structure is used as a constituent material of the electron blocking layer and the light emitting layer.
摘要翻译：通过使用具有优异的空穴注入/输送性能的优异特性的有机化合物，具有高的三重态激子约束能力和电子阻挡能力，提供了高效率，高耐久性的有机电致发光器件，特别是磷光有机电致发光器件，并且在薄膜状态下具有高稳定性和高发光效率。有机电致发光器件包括一对电极和夹在该对电极之间的多个有机层，并且包括发光层和电子阻挡层，其中具有咔唑环结构的以下通式（1）的化合物用作电子阻挡层和发光层的构成材料。

3. 发明申请

US20120175599A1 COMPOUND HAVING CARBAZOLE RING STRUCTURE, AND ORGANIC ELECTROLUMINESCENT DEVICE 有权
标题翻译：具有卡贝环结构的化合物和有机电致发光器件
公开(公告)号：US20120175599A1
公开(公告)日：2012-07-12
申请号：US13391956
申请日：2010-08-25
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano
IPC分类号： H01L51/54 , C07D209/86 , C07D471/04 , C07D401/14 , C07D413/14 , C07D417/14 , C07D403/10 , C07D409/14
CPC分类号： C07D209/86 , C07D209/88 , C07D401/14 , C07D405/10 , C07D409/14 , C07D413/14 , C07D417/14 , C07D471/04 , C09K11/06 , C09K2211/1029 , H01L51/0061 , H01L51/5012 , H01L51/5016 , H01L51/5056 , H01L51/5096 , H05B33/14
摘要： [Problem] An organic compound of excellent characteristics is provided that exhibits excellent hole-injecting/transporting performance with electron blocking ability, and that has high stability in the thin-film state and high luminous efficiency, the organic compound being provided as material for an organic electroluminescent device having high efficiency and high durability. The invention also provides a high-efficient, high-durable organic electroluminescent device using the compound.[Means for Resolution] The compound is of the following general formula having a carbazole ring structure. The organic electroluminescent device includes a pair of electrodes, and one or more organic layers sandwiched between the pair of electrodes, and the compound is used as a constituent material of at least one organic layer.
摘要翻译： [问题]提供了一种优异的有机化合物，其表现出优异的空穴注入/输送性能，具有电子阻挡能力，并且在薄膜状态和高发光效率方面具有高稳定性，有机化合物作为具有高效率和高耐久性的有机电致发光器件。本发明还提供了使用该化合物的高效，高耐久性的有机电致发光器件。 [解决方法]该化合物具有咔唑环结构的以下通式。有机电致发光器件包括一对电极和夹在该对电极之间的一个或多个有机层，并且该化合物用作至少一个有机层的构成材料。

4. 发明授权

US09306175B2 Organic electroluminescent device 有权
标题翻译：有机电致发光器件
公开(公告)号：US09306175B2
公开(公告)日：2016-04-05
申请号：US13503186
申请日：2010-10-22
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano , Eiji Takahashi
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano , Eiji Takahashi
IPC分类号： H01L51/50 , H01L51/00 , C07D209/86 , C07D209/88 , C07D403/04 , C07D409/04 , C07D471/04
CPC分类号： H01L51/0072 , C07D209/86 , C07D209/88 , C07D403/04 , C07D409/04 , C07D471/04 , H01L51/5016 , H01L51/5056 , H01L51/5088
摘要： A high-efficiency, high-durability organic electroluminescent device, particularly a phosphorescent organic electroluminescent device is provided by using an organic compound of excellent characteristics that exhibits excellent hole-injecting/transporting performance and has high triplet exciton confining capability with an electron blocking ability, and that has high stability in the thin-film state and high luminous efficiency.The organic electroluminescent device includes a pair of electrodes, and a plurality of organic layers sandwiched between the pair of electrodes and including a phosphorescent light-emitting material-containing light emitting layer and a hole transport layer, wherein a compound of the following general formula (1) having a carbazole ring structure is used as a constituent material of the hole transport layer.
摘要翻译：通过使用具有优异的空穴注入/输送性能的优异特性的有机化合物，具有高的三重态激子约束能力和电子阻挡能力，提供了高效率，高耐久性的有机电致发光器件，特别是磷光有机电致发光器件，并且在薄膜状态下具有高稳定性和高发光效率。有机电致发光器件包括一对电极和夹在该对电极之间的多个有机层，并且包括含磷光发光材料的发光层和空穴传输层，其中以下通式的化合物（ 1）使用咔唑环结构作为空穴传输层的构成材料。

5. 发明申请

US20120273767A1 ORGANIC ELECTROLUMINESCENT DEVICE 有权
标题翻译：有机电致发光器件
公开(公告)号：US20120273767A1
公开(公告)日：2012-11-01
申请号：US13503156
申请日：2010-10-22
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano , Eiji Takahashi
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano , Eiji Takahashi
IPC分类号： H01L51/54
CPC分类号： H01L51/0072 , H01L51/0059 , H01L51/0085 , H01L51/5016 , H01L51/5096 , H05B33/20
摘要： A high-efficiency, high-durability organic electroluminescent device, particularly a phosphorescent organic electroluminescent device is provided by using an organic compound of excellent characteristics that exhibits excellent hole-injecting/transporting performance and has high triplet exciton confining capability with an electron blocking ability, and that has high stability in the thin-film state and high luminous efficiency.The organic electroluminescent device includes a pair of electrodes, and a plurality of organic layers sandwiched between the pair of electrodes and including a light emitting layer and an electron blocking layer, wherein a compound of the following general formula (1) having a carbazole ring structure is used as a constituent material of the electron blocking layer and the light emitting layer.
摘要翻译：通过使用具有优异的空穴注入/输送性能的优异特性的有机化合物，具有高的三重态激子约束能力和电子阻挡能力，提供了高效率，高耐久性的有机电致发光器件，特别是磷光有机电致发光器件，并且在薄膜状态下具有高稳定性和高发光效率。有机电致发光器件包括一对电极和夹在该对电极之间的多个有机层，并且包括发光层和电子阻挡层，其中具有咔唑环结构的以下通式（1）的化合物用作电子阻挡层和发光层的构成材料。

6. 发明申请

US20120205642A1 ORGANIC ELECTROLUMINESCENT DEVICE 有权
标题翻译：有机电致发光器件
公开(公告)号：US20120205642A1
公开(公告)日：2012-08-16
申请号：US13503186
申请日：2010-10-22
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano , Eiji Takahashi
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Shigeru Kusano , Eiji Takahashi
IPC分类号： H01L51/50
CPC分类号： H01L51/0072 , C07D209/86 , C07D209/88 , C07D403/04 , C07D409/04 , C07D471/04 , H01L51/5016 , H01L51/5056 , H01L51/5088
摘要： A high-efficiency, high-durability organic electroluminescent device, particularly a phosphorescent organic electroluminescent device is provided by using an organic compound of excellent characteristics that exhibits excellent hole-injecting/transporting performance and has high triplet exciton confining capability with an electron blocking ability, and that has high stability in the thin-film state and high luminous efficiency.The organic electroluminescent device includes a pair of electrodes, and a plurality of organic layers sandwiched between the pair of electrodes and including a phosphorescent light-emitting material-containing light emitting layer and a hole transport layer, wherein a compound of the following general formula (1) having a carbazole ring structure is used as a constituent material of the hole transport layer.
摘要翻译：通过使用具有优异的空穴注入/输送性能的优异特性的有机化合物，具有高的三重态激子约束能力和电子阻挡能力，提供了高效率，高耐久性的有机电致发光器件，特别是磷光有机电致发光器件，并且在薄膜状态下具有高稳定性和高发光效率。有机电致发光器件包括一对电极和夹在该对电极之间的多个有机层，并且包括含磷光发光材料的发光层和空穴传输层，其中以下通式的化合物（ 1）使用咔唑环结构作为空穴传输层的构成材料。

7. 发明申请

US20110257404A1 METHOD OF PRODUCING AROMATIC AMINO COMPOUNDS 有权
标题翻译：生产芳族氨基化合物的方法
公开(公告)号：US20110257404A1
公开(公告)日：2011-10-20
申请号：US13123098
申请日：2010-01-25
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi
IPC分类号： C07D401/14 , C07D209/82 , C07C65/03 , C07C213/08
CPC分类号： C07D209/86 , C07C209/10 , C07C2603/18 , C07D249/08 , C07D401/14 , C07C211/55
摘要： [Problem] To provide a method of producing an aromatic amino compound by using a primary or secondary amine compound and a halogenated aromatic compound as starting materials, and relying upon the Ullmann reaction, the method being capable of obtaining the highly pure aromatic amino compound in high yields and inexpensively.[Means for Solution] A method of producing an aromatic amino compound by using a primary or secondary amine compound having an aromatic ring group and a halogenated aromatic compound as starting materials, reacting the amine compound with the halogenated aromatic compound in the presence of a copper catalyst and a base so as to produce the aromatic amino compound having a structure in which an aromatic ring group derived from the halogenated aromatic compound is coupled to the amino group of the amine compound, wherein the amine compound and the halogenated aromatic compound are reacted together under a condition where an aromatic oxycarboxylic acid having a hydroxyl group and a hydroxycarbonyl group that are bonded to neighboring carbon atoms, is made present together with the copper catalyst and the base.
摘要翻译： [问题]为了提供通过使用伯胺或仲胺化合物和卤代芳族化合物作为原料制备芳香族氨基化合物的方法，依赖于乌尔曼反应，该方法能够获得高纯度芳香族氨基化合物产量高，成本低廉。 [解决方案]通过使用具有芳环基和卤代芳族化合物的伯胺或仲胺化合物作为起始原料制备芳族氨基化合物的方法，使胺化合物与卤代芳族化合物在铜的存在下反应催化剂和碱，以产生具有这样一种结构的芳族氨基化合物，其中衍生自卤代芳族化合物的芳族环基团与胺化合物的氨基偶合，其中胺化合物和卤代芳族化合物一起反应在具有与相邻碳原子键合的羟基和羟基羰基的芳族羟基羧酸的情况下，与铜催化剂和碱一起存在。

8. 发明授权

US09196837B2 Compound having indenocarbazole ring structure, and organic electroluminescent device 有权
标题翻译：具有茚基咔唑环结构的化合物和有机电致发光器件
公开(公告)号：US09196837B2
公开(公告)日：2015-11-24
申请号：US13812995
申请日：2011-07-29
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Kouki Kase , Eiji Takahashi
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Kouki Kase , Eiji Takahashi
IPC分类号： H01L51/00 , C07D209/70 , C07D209/86 , C07D401/10 , C07D403/10 , C07D403/14 , C07D409/10 , C07D413/10 , C07D417/14 , C09B57/00 , H01L51/50
CPC分类号： H01L51/0053 , C07D209/70 , C07D209/86 , C07D401/10 , C07D403/10 , C07D403/14 , C07D409/10 , C07D413/10 , C07D417/14 , C09B57/00 , C09B57/008 , H01L51/0058 , H01L51/0059 , H01L51/0061 , H01L51/0072 , H01L51/5012 , H01L51/5048 , H01L51/5088 , H01L51/5096
摘要： An organic compound with excellent characteristics excelling in hole-injecting/transporting performance and having electron blocking ability, high stability in a thin-film state and high luminous efficiency is provided as material for an organic electroluminescent device.The compound of a general formula (1) having an indenocarbazole ring structure is used as a constituent material of at least one organic layer in the organic electroluminescent device that includes a pair of electrodes and one or more organic layers sandwiched between the pair of electrodes.
摘要翻译：作为有机电致发光器件的材料，提供了具有优异的空穴注入/输送性能优良，具有电子阻挡能力，薄膜状态的高稳定性和高发光效率的有机化合物。具有茚碳咔唑环结构的通式（1）的化合物用作有机电致发光器件中至少一个有机层的构成材料，其包括一对电极和夹在该对电极之间的一个或多个有机层。

9. 发明申请

US20130126856A1 COMPOUND HAVING INDENOCARBAZOLE RING STRUCTURE, AND ORGANIC ELECTROLUMINESCENT DEVICE 有权
标题翻译：具有吲哚环唑结构的化合物和有机电致发光器件
公开(公告)号：US20130126856A1
公开(公告)日：2013-05-23
申请号：US13812995
申请日：2011-07-29
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Kouki Kase , Eiji Takahashi
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi , Kouki Kase , Eiji Takahashi
IPC分类号： H01L51/00 , C07D403/14 , C07D409/10 , C07D417/14 , C07D413/10 , C07D403/10 , C07D401/10
CPC分类号： H01L51/0053 , C07D209/70 , C07D209/86 , C07D401/10 , C07D403/10 , C07D403/14 , C07D409/10 , C07D413/10 , C07D417/14 , C09B57/00 , C09B57/008 , H01L51/0058 , H01L51/0059 , H01L51/0061 , H01L51/0072 , H01L51/5012 , H01L51/5048 , H01L51/5088 , H01L51/5096
摘要： An organic compound with excellent characteristics excelling in hole-injecting/transporting performance and having electron blocking ability, high stability in a thin-film state and high luminous efficiency is provided as material for an organic electroluminescent device. The compound of a general formula (1) having an indenocarbazole ring structure is used as a constituent material of at least one organic layer in the organic electroluminescent device that includes a pair of electrodes and one or more organic layers sandwiched between the pair of electrodes.
摘要翻译：作为有机电致发光器件的材料，提供了具有优异的空穴注入/输送性能优良，具有电子阻挡能力，薄膜状态的高稳定性和高发光效率的有机化合物。具有茚碳咔唑环结构的通式（1）的化合物用作有机电致发光器件中至少一个有机层的构成材料，其包括一对电极和夹在该对电极之间的一个或多个有机层。

10. 发明授权

US08735626B2 Method of producing aromatic amino compounds 有权
标题翻译：制备芳香族氨基化合物的方法
公开(公告)号：US08735626B2
公开(公告)日：2014-05-27
申请号：US13123098
申请日：2010-01-25
申请人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi
发明人： Norimasa Yokoyama , Makoto Nagaoka , Kazunori Togashi
IPC分类号： C07C211/00 , C07C59/00 , C07C65/21
CPC分类号： C07D209/86 , C07C209/10 , C07C2603/18 , C07D249/08 , C07D401/14 , C07C211/55
摘要： A method of producing an aromatic amino compound using a primary or secondary amine compound and a halogenated aromatic compound as starting materials, and relying upon the Ullmann reaction, the method being capable of obtaining the highly pure aromatic amino compound in high yields and inexpensively. A primary or secondary amine compound having an aromatic ring group and a halogenated aromatic compound as starting materials, are reacted with the halogenated aromatic compound in the presence of copper catalyst and base to produce the aromatic amino compound having a structure in which an aromatic ring group derived from the halogenated aromatic compound is coupled to the amino group of the amine compound, wherein the amine compound and the halogenated aromatic compound are reacted together such that an aromatic oxycarboxylic acid having a hydroxyl group and a hydroxycarbonyl group bonded to neighboring carbon atoms, is present together with the copper catalyst and the base.
摘要翻译：使用伯胺或仲胺化合物和卤代芳族化合物作为原料制备芳香族氨基化合物的方法，依赖乌尔曼反应，该方法能够以高收率和低成本获得高纯度芳香族氨基化合物。具有芳环基团和卤代芳族化合物作为起始原料的伯胺或仲胺化合物与卤化芳族化合物在铜催化剂和碱存在下反应，生成具有芳环基团的芳族氨基化合物来自卤代芳香族化合物的胺化合物的氨基与胺化合物的氨基偶联，其中胺化合物和卤代芳香族化合物反应，使得具有与相邻碳原子键合的羟基和羟基羰基的芳族羟基羧酸为与铜催化剂和碱一起存在。

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