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1. 发明授权

US06171994B2 Multiple crosslinking type transition metal compound used for olefin polymerization process 有权
标题翻译：用于烯烃聚合过程的多交联型过渡金属化合物
公开(公告)号：US06171994B2
公开(公告)日：2001-01-09
申请号：US09184279
申请日：1998-11-02
申请人： Nobuhiro Yabunouchi , Kiyohiko Yokota , Masami Watanabe , Takuji Okamoto , Noriyuki Tani
发明人： Nobuhiro Yabunouchi , Kiyohiko Yokota , Masami Watanabe , Takuji Okamoto , Noriyuki Tani
IPC分类号： C08F464
CPC分类号： C07F17/00 , C07C35/32 , C07F7/081 , C08F4/61908 , C08F4/61912 , C08F4/61927 , C08F4/65927 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/16 , Y10S526/943 , C08F2500/03 , C08F2500/17 , C08F210/14 , C08F2500/20 , C08F2500/01 , C08F2500/02
摘要： A novel multiply crosslinked transition metal compound represented by the formula (I): wherein M is a metallic element of the Groups 3 to 10 or the lanthanide series of the Periodic Table; E1 and E2 are each a &sgr;-bonding or &pgr;-bonding ligand; X is a &sgr;-bonding ligand; Y is a Lewis base; A1, A2, . . . An and D are each a crosslinking group, and at least one of A1, A2, . . . An comprises a crosslink consisting of carbon alone; n is 2 to 4; p is 1 to 4; q is 1 to 5 and equal to the valence of M minus 2; r is 0 to 3; and s is 0 to 4, and a production process thereof. The transition metal compound is useful as a component of a polymerization catalyst for catalyzing the production of an olefin polymer having a uniform composition and a narrow molecular weight distribution in a high yield.
摘要翻译：一种由式（I）表示的新型多交联过渡金属化合物：其中M是第3至10族的金属元素或元素周期表的镧系元素; E1和E2各自是σ键或π键合配体; X是σ键合配体; Y是路易斯基地; A1，A2，。。。 An和D各自为交联基团，并且A1，A2，...中的至少一个。。。 An包括由单独的碳组成的交联; n为2〜4; p为1〜4; q为1至5，等于M的价数减去2; r为0〜3; s为0〜4，及其制造方法。过渡金属化合物可用作催化以高产率催化生产具有均匀组成和窄分子量分布的烯烃聚合物的组分的组分。

2. 发明授权

US5854165A Transition metal compound, catalyst for olefin polymerization, process for preparing olefin polymer by use of catalyst 失效
标题翻译：过渡金属化合物，用于烯烃聚合的催化剂，使用催化剂制备烯烃聚合物的方法
公开(公告)号：US5854165A
公开(公告)日：1998-12-29
申请号：US619513
申请日：1996-03-29
申请人： Nobuhiro Yabunouchi , Kiyohiko Yokota , Masami Watanabe , Takuji Okamoto , Noriyuki Tani
发明人： Nobuhiro Yabunouchi , Kiyohiko Yokota , Masami Watanabe , Takuji Okamoto , Noriyuki Tani
IPC分类号： C07C35/32 , C07F7/08 , C07F17/00 , C08F4/619 , C08F4/6192 , C08F4/64 , C08F4/6592 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/16
CPC分类号： C07F17/00 , C07C35/32 , C07F7/0818 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/16 , C08F4/61908 , C08F4/61912 , C08F4/61927 , C08F4/65927 , Y10S526/943
摘要： A transition metal compound which is a multiple crosslinking type transition metal complex represented by the general formula (I) ##STR1## wherein M is a metallic element in the groups 3 to 10 or a lanthanoide series of the periodic table; E.sup.1 and E.sup.2 are each a .sigma.-bonding or a .pi.-bonding ligand; X is a .sigma.-bonding ligand; L is a Lewis base; A.sup.1, A.sup.2 . . . A.sup.n and D arc each a crosslinking group; n is 2 to 4; p is 1 to 4; q is 1 to 5; r is 0 to 3; and s is 0 to 4; and catalysts for olefin polymerization containing the transition metal compound or complexes thereof and a process for preparing an olefin polymer employing the catalyst.
摘要翻译： PCT No.PCT / JP94 / 01626 Sec。 371日期：1996年3月29日 102（e）1996年3月29日PCT 1994年9月30日PCT PCT。公开号WO95 / 09172 日期：1995年04月6日，是由通式（I）表示的多交联型过渡金属络合物的过渡金属化合物，其中M为第3〜10族中的金属元素或镧系元素周期表; E1和E2各自为σ-键合或π-键合配体; X是σ-键合配体; L是路易斯碱; A1，A2。。。 An和D各自为交联基团; n为2〜4; p为1〜4; q为1〜5; r为0〜3; s为0〜4; 以及含有过渡金属化合物或其络合物的烯烃聚合催化剂和使用该催化剂制备烯烃聚合物的方法。

3. 发明授权

US06339135B1 Transition metal compound, catalyst for olefin polymerization, process for preparing olefin polymer 失效
标题翻译：过渡金属化合物，用于烯烃聚合的催化剂，制备烯烃聚合物的方法
公开(公告)号：US06339135B1
公开(公告)日：2002-01-15
申请号：US08913364
申请日：1997-09-29
申请人： Takashi Kashiwamura , Nobuhiro Yabunouchi , Masami Watanabe , Noriyuki Tani , Takuji Okamoto , Kiyohiko Yokota , Mitsugu Kanzawa , Tetsuya Inoue
发明人： Takashi Kashiwamura , Nobuhiro Yabunouchi , Masami Watanabe , Noriyuki Tani , Takuji Okamoto , Kiyohiko Yokota , Mitsugu Kanzawa , Tetsuya Inoue
IPC分类号： C08F464
CPC分类号： B01J31/143 , B01J31/2295 , B01J2531/46 , B01J2531/48 , C07F17/00 , C08F4/61908 , C08F4/61912 , C08F4/61927 , C08F4/65908 , C08F4/65912 , C08F10/00 , C08F110/06 , C08F210/16 , Y10S526/943 , C08F4/65927 , C08F2500/17 , C08F2500/20 , C08F210/14
摘要： A novel double crosslinking type transition metal compound is herein disclosed which is represented by the general formula (I) wherein M is a metallic element in the groups 3 to 10 or a lanthanoide series of the periodic table; E1 and E2 are each a cyclopentadienyl group, an indenyl group or the like, and they form a crosslinking structure via A1 and A2; A1 and A2 are each a crosslinking group comprising a hydrocarbon group of one or more carbon atoms; X is a &sgr;-bonding ligand; and Y is a Lewis base. Also disclosed are a double crosslinking type biscyclopentadienyl derivative and bisindenyl derivative for use in the above-mentioned transition metal compound, its preparation process, a catalyst for olefin polymerization using the transition metal compound, and a preparation process of an olefin polymer by the use of this catalyst.
摘要翻译：本文公开了由通式（I）表示的新型双交联型过渡金属化合物，其中M为3至10族中的金属元素或周期表的镧系元素; E1和E2各自为环戊二烯基，茚基等，它们通过A1和A2形成交联结构; A1和A2各自为包含一个或多个碳原子的烃基的交联基团; X是σ-键合配体; Y是路易斯碱。还公开了用于上述过渡金属化合物的双交联型双环戊二烯基衍生物和双茚基衍生物，其制备方法，使用过渡金属化合物的烯烃聚合催化剂，以及使用烯烃聚合物的制备方法这种催化剂。

4. 发明授权

US06838409B1 Catalyst for olefin/styrene copolymerization, and process for producing olefin/styrene copolymer 失效
标题翻译：用于烯烃/苯乙烯共聚的催化剂，以及生产烯烃/苯乙烯共聚物的方法
公开(公告)号：US06838409B1
公开(公告)日：2005-01-04
申请号：US09914254
申请日：2000-02-25
申请人： Nobuhiro Yabunouchi , Nobuhide Ishihara , Kiyohiko Yokota
发明人： Nobuhiro Yabunouchi , Nobuhide Ishihara , Kiyohiko Yokota
IPC分类号： C08F4/64 , C08F4/642 , C08F4/646 , C08F4/6592 , C08F10/00 , C08F210/00 , C08F210/02 , C08F210/08 , C08F212/08 , B01J31/00 , B01J37/00 , C08F4/02 , C08F4/60
CPC分类号： C08F212/08 , C08F4/6592 , C08F10/00 , C08F210/02 , C08F4/65912 , C08F4/602 , C08F2500/03
摘要： Catalysts for copolymerization of olefins and styrenes, comprising (A) a transition metal compound, (B) an oxygen-containing compound and/or a compound capable of reacting with a transition metal compound to form an ionic complex, (C) a specific compound such as a reaction product of triphenylmethyl alcohol and triisobutylaluminium, and optionally (D) an alkylating agent, and methods for producing olefin-styrene copolymers in the presence of such catalysts, which catalysts have the advantages of enhancing the copolymerization activity and reducing the amount of the promoter such as oxygen-containing compounds, etc, and using them, olefin-styrene copolymers can be produced efficiently and inexpensively.

5. 发明授权

US5739225A Process for preparing olefin polymer, and ethylenic polymer 失效
标题翻译：制备烯烃聚合物和烯属聚合物的方法
公开(公告)号：US5739225A
公开(公告)日：1998-04-14
申请号：US666471
申请日：1996-06-28
申请人： Toshinori Tazaki , Shuji Machida , Nobuo Kawasaki , Nobuhiro Yabunouchi , Yasunori Kadoi , Mizutomo Takeuchi , Kenji Nakacho , Haruo Shikuma , Noriyuki Tani
发明人： Toshinori Tazaki , Shuji Machida , Nobuo Kawasaki , Nobuhiro Yabunouchi , Yasunori Kadoi , Mizutomo Takeuchi , Kenji Nakacho , Haruo Shikuma , Noriyuki Tani
IPC分类号： C08F4/6392 , C08F4/64 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/02 , C08F210/16 , C08F210/18
CPC分类号： C08F10/02 , C08F10/00 , C08F110/02 , C08F210/02 , C08F210/16 , C08F210/18 , C08F4/6392 , C08F4/65912 , C08F4/6592 , Y10S526/943
摘要： An olefin polymer is prepared by homopolymerizing an olefin or copolymerizing two different olefins or an olefin and another polymerizable unsaturated compound in the presence of a polymerization catalyst containing (A) a transition metal compound represented by the formula (I): CpML.sub.x-1 (I) wherein M is a metallic element of Groups 3 to 10 of the Periodic Table or a metallic element of the lanthanide series; Cp is a cyclic compound group having a cyclopentadienyl skeleton of 5 to 30 carbon atoms; L is R', OR', SR', SO.sub.3 R'N'R'R", PR'R", wherein R' and R" are each a C.sub.1-20 hydrocarbon group or a silyl group, NO.sub.2, a halogen atom, a 1-pyrrolyl group or a 1-pyrrolidinyl group, with the proviso that at least one of the L groups is OR', SR', N'R'R" or PR'R", wherein R' and R" are each a C.sub.1-20 hydrocarbon group or a silyl group; and x is a valence number of M, and when a plurality of L's are present, the respective L's may be the same or different, and (B) an aluminoxane, wherein the molar ratio of the component (B)/component (A) (in terms of the metallic atoms) is in the range of 2 to 500.
摘要翻译： PCT No.PCT / JP94 / 02251 Sec。 371日期：1996年6月28日 102（e）日期1996年6月28日PCT 1994年12月27日PCT PCT。 WO95 / 18158 PCT出版物日期：1995年7月6日烯烃聚合物通过在含有（A）由式（I）表示的过渡金属化合物的聚合催化剂存在下，使烯烃均聚或共聚两种不同的烯烃或烯烃和另一种可聚合不饱和化合物来制备： CpMLx-1（I）其中M是周期表第3至10族的金属元素或镧系金属元素; Cp是具有5至30个碳原子的环戊二烯基骨架的环状化合物基团; L是R'，OR'，SR'，SO3R'N'R'R“，PR'R”，其中R'和R“各自为C1-20烃基或甲硅烷基，NO2，卤素原子，1-吡咯基或1-吡咯烷基，条件是至少一个L基团是OR'，SR'，N'R'R“或PR'R”，其中R' 和R“各自为C 1-20烃基或甲硅烷基; （B）/成分（A）的摩尔比，X是价数M，当存在多个L s时，各自的L可以相同或不同，（B）铝氧烷，（以金属原子计）在2〜500的范围内。

6. 发明申请

US20120018710A1 NOVEL POLYMERIZABLE MONOMER AND POLYMER OF THE POLYMERIZABLE MONOMER, AND MATERIAL FOR ORGANIC DEVICE, HOLE INJECTION/TRANSPORT MATERIAL AND ORGANIC ELECTROLUMINESCENT ELEMENT EACH COMPRISING THE POLYMER 审中-公开
标题翻译：可聚合单体的新型可聚合单体和聚合物，有机装置的材料，注入/运输材料和有机电致发光元件，每个包含聚合物
公开(公告)号：US20120018710A1
公开(公告)日：2012-01-26
申请号：US13144796
申请日：2010-02-09
申请人： Mitsuru Eida , Masami Watanabe , Masahiko Fukuda , Nobuhiro Yabunouchi
发明人： Mitsuru Eida , Masami Watanabe , Masahiko Fukuda , Nobuhiro Yabunouchi
IPC分类号： H01L51/54 , C07C69/587 , C07C233/88 , C07D307/91 , C07D209/82 , C07D333/76 , C08F26/02 , C08F20/60 , C08F32/08 , C08F24/00 , C08F26/06 , C08F28/06 , C08F38/00 , C08F20/34 , C07C211/54
CPC分类号： C08F120/34 , C07C211/54 , C07C211/58 , C07C211/61 , C07C217/84 , C07C219/32 , C07C219/34 , C07C233/44 , C07C2602/42 , C07C2603/18 , C07D207/273 , C07D209/86 , C07D307/91 , C07D333/76 , C08F120/60 , C08G61/08 , C08G2261/143 , C08G2261/3324 , C08G2261/418 , H01L51/004 , H01L51/0043 , H01L51/0059 , H01L51/0061 , H01L51/0072 , H01L51/0073 , H01L51/0074
摘要： A polymerizable monomer represented by the following formula (1) which is substituted by one or more groups comprising a polymerizable functional group wherein Ar1 and Ar4 to Ar6 are independently a substituted or unsubstituted aryl group having 6 to 40 ring carbon atoms; and Ar2, Ar3 and L1 are a substituted or unsubstituted arylene group having 6 to 40 ring carbon atoms:
摘要翻译：由下式（1）表示的可聚合单体，其被一个或多个包含可聚合官能团的基团取代，其中Ar1和Ar4至Ar6独立地为取代或未取代的环碳原子数为6〜40的芳基; Ar2，Ar3和L1是取代或未取代的环碳原子数为6〜40的亚芳基，

7. 发明申请

US20110315964A1 NOVEL POLYMERIZABLE MONOMER, AND MATERIAL FOR ORGANIC DEVICE, HOLE INJECTION/TRANSPORT MATERIAL, MATERIAL FOR ORGANIC ELECTROLUMINESCENT ELEMENT AND ORGANIC ELECTROLUMINESCENT ELEMENT EACH COMPRISING POLYMER (POLYMERIC COMPOUND) OF THE POLYMERIZABLE MONOMER 审中-公开
标题翻译：新型可聚合单体和有机装置材料，注入/运输材料，有机电致发光元件和有机电致发光元件，每个包含可聚合单体的聚合物（聚合物）
公开(公告)号：US20110315964A1
公开(公告)日：2011-12-29
申请号：US13138603
申请日：2010-03-05
申请人： Mitsuru Eida , Nobuhiro Yabunouchi , Yumiko Mizuki , Masami Watanabe , Akinori Yomogita
发明人： Mitsuru Eida , Nobuhiro Yabunouchi , Yumiko Mizuki , Masami Watanabe , Akinori Yomogita
IPC分类号： H01L51/54 , C07D209/82 , C07C211/60 , C07C69/52 , C07C233/34 , C08F128/06 , C07D333/52 , C08F124/00 , C08F126/02 , C08F122/40 , C08F126/06 , C07D307/91 , C07D207/444
CPC分类号： H01L51/0035 , C07C211/61 , C07C219/34 , C07C233/44 , C07C2602/42 , C07C2603/18 , C07D207/452 , C07D209/86 , C07D209/88 , C07D307/91 , C07D333/76 , C07D403/14 , C07D405/12 , C07D405/14 , C07D409/12 , C08F12/22 , C08F12/26 , C08F12/30 , C08F12/32 , C08F20/34 , C08F22/38 , C08F22/40 , C09B57/00 , C09B57/008 , H01L51/004 , H01L51/0059 , H01L51/0072 , H01L51/0073 , H01L51/5012 , H01L51/5048 , H01L51/5056 , H01L51/5088
摘要： A polymerizable monomer represented by the following formula (1) wherein at least one of Ar1 to Ar3 is substituted by a group represented by the following formula (2) and which is substituted by one or more groups comprising a polymerizable functional group.Ar1 to Ar3 are a substituted or unsubstituted aryl group having 6 to 40 ring carbon atoms, Ar6 is a substituted or unsubstituted aryl group having 6 to 40 ring carbon atoms and Ar4 and Ar5 are a substituted or unsubstituted arylene group having 6 to 40 ring carbon atoms.
摘要翻译：由下式（1）表示的可聚合单体，其中Ar 1至Ar 3中的至少一个被下式（2）表示的基团取代，并被一个或多个包含可聚合官能团的基团取代。 Ar 1〜Ar 3为取代或未取代的环碳原子数为6〜40的芳基，Ar 6为取代或未取代的环碳原子数为6〜40的芳基，Ar 4和Ar 5为取代或未取代的碳原子数为6〜40的亚芳基原子

8. 发明授权

US5955557A Branched ethylenic macromonomer and its polymer 失效
标题翻译：分支乙烯大分子单体及其聚合物
公开(公告)号：US5955557A
公开(公告)日：1999-09-21
申请号：US632475
申请日：1996-04-26
申请人： Shuji Machida , Masahiro Mitani , Masami Watanabe , Nobuhiro Yabunouchi
发明人： Shuji Machida , Masahiro Mitani , Masami Watanabe , Nobuhiro Yabunouchi
IPC分类号： C08F4/659 , C08F4/6592 , C08F8/04 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/02 , C08F210/16 , C08F10/14
CPC分类号： C08F10/02 , C08F10/00 , C08F8/04 , C08F110/02 , C08F210/02 , C08F210/16 , C08F4/65912 , C08F4/6592 , Y10S526/943
摘要： A copolymer having the excellent molding and working properties obtainable by using a branched ethylenic macromonomer and a comonomer selected from the group consisting of ethylene, an .alpha.-olefin having 3 to 20 carbon atoms, cyclic olefins and styrenes. The branched ethylenic macromonomer of the present invention is derivable from ethylene singly or derivable from ethylene and another olefin, (a) a molar ratio of a terminal methyl group/a vinyl group in the macromonomer being in the range of 1 to 100, the macromonomer having a branch other than the branch directly derived from the other olefin, (b) a ratio of vinyl groups to the total unsaturated groups in the macromonomer being 70 mol % or more, (c) a weight-average molecular weight of the macromonomer in terms of a polyethylene measured by a GPC being in the range of 100 to 20,000.
摘要翻译： PCT No.PCT / JP94 / 01792 Sec。 371日期：1996年04月28日 102（e）日期1996年4月28日PCT 1994年10月26日PCT公布。公开号WO95 / 11931 日期：1993年10月26日具有通过使用支化乙烯性大分子单体和选自乙烯，碳原子数3〜20的α-烯烃，环状烯烃和苯乙烯的共聚单体得到的优异的成型性和工作性的共聚物。本发明的支链乙烯性大分子单体可单独衍生自乙烯或可衍生自乙烯和另一种烯烃的乙烯基，（a）大分子单体中的末端甲基/乙烯基的摩尔比在1〜100的范围内，大分子单体具有直接衍生自其它烯烃的分支以外的分支，（b）大分子单体中乙烯基与总不饱和基团的比例为70摩尔％以上，（c）大分子单体的重均分子量通过GPC测量的聚乙烯的用量在100至20,000的范围内。

9. 发明授权

US06169154A Branched ethylenic macromonomer and its polymer 失效
标题翻译：分支乙烯大分子单体及其聚合物
公开(公告)号：US06169154A
公开(公告)日：2001-01-02
申请号：US09344806
申请日：1999-06-25
申请人： Shuji Machida , Masahiro Mitani , Masami Watanabe , Nobuhiro Yabunouchi
发明人： Shuji Machida , Masahiro Mitani , Masami Watanabe , Nobuhiro Yabunouchi
IPC分类号： C08F11002
CPC分类号： C08F10/02 , C08F4/65912 , C08F4/6592 , C08F8/04 , C08F10/00 , C08F110/02 , C08F210/02 , C08F210/16 , Y10S526/943 , C08F4/65927 , C08F210/14 , C08F2500/02 , C08F2500/23 , C08F212/08 , C08F2500/17 , C08F2500/03 , C08F210/08 , C08F2500/14
摘要： There are herein disclosed a branched ethylenic macromonomer which can function as a comonomer to provide a copolymer having excellent molding and working properties and which can be hydrogenated to provide a hydrogenated product as a wax useful in various uses, a copolymer having the excellent molding and working properties obtainable by using this macromonomer as a comonomer, and a branched ethylenic polymer having a low-molecular weight obtainable by hydrogenating the macromonomer. The branched ethylenic macromonomer of the present invention is derivable from ethylene singly or derivable from ethylene and another olefin, (a) a molar ratio of a terminal methyl group/a vinyl group in the macromonomer being in the range of 1 to 100, the macromonomer having a branch other than the branch directly derived from the other olefin, (b) a ratio of vinyl groups to the total unsaturated groups in the macromonomer being 70 mol % or more, (c) a weight-average molecular weight of the macromonomer in terms of a polyethylene measured by a GPC being in the range of 100 to 20,000.
摘要翻译：本文公开了一种支链乙烯性大分子单体，其可以用作共聚单体以提供具有优异的模塑和加工性能的共聚物，并且其可以被氢化以提供可用于各种用途的蜡的氢化产物，具有优异的模塑和加工的共聚物通过使用该大分子单体作为共聚单体可获得的性质，以及通过氢化大分子单体可获得的具有低分子量的支链烯属聚合物。本发明的支链乙烯性大分子单体可单独衍生自乙烯或可衍生自乙烯和另一种烯烃的乙烯基，（a）大分子单体中的末端甲基/乙烯基的摩尔比在1〜100的范围内，大分子单体具有直接衍生自其它烯烃的分支以外的分支，（b）大分子单体中乙烯基与总不饱和基团的比例为70摩尔％以上，（c）大分子单体的重均分子量通过GPC测量的聚乙烯的用量在100至20,000的范围内。

10. 发明授权

US09139522B2 Aromatic amine derivative and organic electroluminescent device using the same 有权
标题翻译：芳香族胺衍生物和使用其的有机电致发光器件
公开(公告)号：US09139522B2
公开(公告)日：2015-09-22
申请号：US13124759
申请日：2008-10-17
申请人： Nobuhiro Yabunouchi , Michiru Sekiguchi , Takahiko Ochi , Yoshiyuki Totani
发明人： Nobuhiro Yabunouchi , Michiru Sekiguchi , Takahiko Ochi , Yoshiyuki Totani
IPC分类号： H01L51/54 , C07D209/82 , C07D209/86 , C07D209/56 , C09K11/06 , H05B33/14 , C09B57/00 , H01L51/00 , H01L51/50
CPC分类号： C07D209/86 , C07D209/56 , C09B57/00 , C09B57/008 , C09K11/06 , C09K2211/1011 , C09K2211/1029 , H01L51/006 , H01L51/0061 , H01L51/0072 , H01L51/5048 , H05B33/14
摘要： Disclosed is a long-life organic EL device having high luminous efficiency even after storage at high temperatures. Also disclosed is an aromatic amine derivative which enables to realize such an organic EL device. The aromatic amine derivative is represented by the following general formula (1). (In the formula (1), Ar1 is represented by the general formula (2) below, and Ar2 is represented by the general formula (3) below.)
摘要翻译：公开了即使在高温下保存后也具有高发光效率的长寿命有机EL器件。还公开了能够实现这种有机EL器件的芳族胺衍生物。芳香族胺衍生物由以下通式（1）表示。（式（1）中，Ar 1由下述通式（2）表示，Ar 2表示通式（3））。

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