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1. 发明授权

US06579819B2 Silicon nitride sintered products and processes for their production 失效
标题翻译：氮化硅烧结产品及其生产工艺
公开(公告)号：US06579819B2
公开(公告)日：2003-06-17
申请号：US09796430
申请日：2001-03-02
申请人： Naoto Hirosaki , Toshiyuki Nishimura , Yoshinobu Yamamoto , Mamoru Mitomo
发明人： Naoto Hirosaki , Toshiyuki Nishimura , Yoshinobu Yamamoto , Mamoru Mitomo
IPC分类号： C04B35587
CPC分类号： C04B35/584 , C04B35/5935
摘要： A silicon nitride sintered product comprising silicon nitride grains and a grain boundary phase, wherein the grain boundary phase consists essentially of a single phase of a Lu4Si2O7N2 crystal phase, and the composition of the silicon nitride sintered product is a composition in or around a triangle ABC having point A: Si3N4, point B: 28 mol % SiO2-72 mol % Lu2O3 and point C: 16 mol % SiO2-84 mol % Lu2O3, as three apexes, in a ternary system phase diagram of a Si3N4—SiO2—Lu2O3 system. Also disclosed is a silicon nitride sintered product comprising silicon nitride grains and a grain boundary phase of an oxynitride, wherein the composition of the sintered product is a composition in a triangle having point A: Si3N4, point B: 40 mol % SiO2-60 mol % Lu2O3 and point C: 60 mol % SiO2-40 mol % Lu2O3, as three apexes, in a ternary system phase diagram of a Si3N4—SiO2—Lu2O3 system.
摘要翻译：一种包含氮化硅晶粒和晶界相的氮化硅烧结体，其中晶界相主要由Lu4Si2O7N2晶相的单相组成，氮化硅烧结体的组成是三角形ABC内或周围的组成在Si3N4-SiO2-Lu2O3体系的三元体系相图中，点A：Si 3 N 4，B点：28摩尔％SiO 2 -S72摩尔％Lu 2 O 3，点C：16摩尔％SiO 2 -S84摩尔％Lu 2 O 3作为三个顶点。还公开了包含氮化硅晶粒和氮氧化物的晶界相的氮化硅烧结体，其中烧结体的组成是具有点A：Si 3 N 4，点B：40摩尔％SiO 2〜60摩尔的三角形组成％Lu2O3和点C：60mol％SiO2-40mol％Lu2O3，作为三个顶点，在Si3N4-SiO2-Lu2O3体系的三元体系相图中。

2. 发明授权

US06737378B2 Silicon nitride sintered products and processes for their production 失效
标题翻译：氮化硅烧结产品及其生产工艺
公开(公告)号：US06737378B2
公开(公告)日：2004-05-18
申请号：US10260396
申请日：2002-10-01
申请人： Naoto Hirosaki , Toshiyuki Nishimura , Yoshinobu Yamamoto , Mamoru Mitomo
发明人： Naoto Hirosaki , Toshiyuki Nishimura , Yoshinobu Yamamoto , Mamoru Mitomo
IPC分类号： C04B35587
CPC分类号： C04B35/584 , C04B35/5935
摘要： A silicon nitride sintered product comprising silicon nitride grains and a grain boundary phase, wherein the grain boundary phase consists essentially of a single phase of a Lu4Si2O7N2 crystal phase, and the composition of the silicon nitride sintered product is a composition in or around a triangle ABC having point A: Si3N4, point B: 28 mol % SiO2-72 mol % Lu2O3 and point C: 16 mol % SiO2-84 mol % Lu2O3, as three apexes, in a ternary system phase diagram of a Si3N4—SiO2—Lu2O3 system. Also disclosed is a silicon nitride sintered product comprising silicon nitride grains and a grain boundary phase of an oxynitride, wherein the composition of the sintered product is a composition in a triangle having point A: Si3N4, point B: 40 mol % SiO2-60 mol % Lu2O3 and point C: 60 mol % SiO2-40 mol % Lu2O3, as three apexes, in a ternary system phase diagram of a Si3N4—SiO2—Lu2O3 system.
摘要翻译：一种包含氮化硅晶粒和晶界相的氮化硅烧结体，其中晶界相主要由Lu4Si2O7N2晶相的单相组成，氮化硅烧结体的组成是三角形ABC内或周围的组成在Si3N4-SiO2-Lu2O3体系的三元体系相图中，点A：Si 3 N 4，B点：28摩尔％SiO 2 -S72摩尔％Lu 2 O 3，点C：16摩尔％SiO 2 -S84摩尔％Lu 2 O 3作为三个顶点。还公开了包含氮化硅晶粒和氮氧化物的晶界相的氮化硅烧结体，其中烧结体的组成是具有点A：Si 3 N 4，点B：40摩尔％SiO 2〜60摩尔的三角形组成％Lu2O3和点C：60mol％SiO2-40mol％Lu2O3，作为三个顶点，在Si3N4-SiO2-Lu2O3体系的三元体系相图中。

3. 发明授权

US07910023B2 Lithium-containing sialon phosphor and method of manufactring the same 有权
标题翻译：含锂锡隆荧光粉及其制造方法
公开(公告)号：US07910023B2
公开(公告)日：2011-03-22
申请号：US11919237
申请日：2006-04-27
申请人： Rong-Jun Xie , Mamoru Mitomo , Naoto Hirosaki , Yoshinobu Yamamoto
发明人： Rong-Jun Xie , Mamoru Mitomo , Naoto Hirosaki , Yoshinobu Yamamoto
IPC分类号： C09K11/08 , C09K11/66 , C09K11/02 , C09K11/77
CPC分类号： C09K11/0883 , C04B35/597 , C04B35/62675 , C04B2235/3203 , C04B2235/3208 , C04B2235/3224 , C04B2235/3852 , C04B2235/3865 , C04B2235/3873 , C04B2235/766 , C09K11/7734 , H01L33/502
摘要： According to the invention, a highly crystalline α-sialon is synthesized to emit highly intense light and a white LED showing an excellent color rendering characteristic is provided by shifting emitted light to the short wavelength side (blue shift). Such an α-sialon is designed so as to be expressed by general formula (Lix, Cay, Euz) (Si12−(m+n)Alm+n) (OnN16−n) wherein the numerical ranges of x, y, z, m and n are respectively 0
摘要翻译：根据本发明，合成高结晶性α-赛隆发射高强度光，并且通过将发射光移动到短波长侧（蓝移）来提供显示出优异显色特性的白色LED。这样的α赛隆被设计成通过通式（Lix，Cay，Euz）（Si12-（m + n）Alm + n）（OnN16-n）表示，其中x，y，z， m和n分别为0

4. 发明申请

US20100072498A1 Lithium-containing sialon phosphor and method of manufactring the same 有权
标题翻译：含锂锡隆荧光粉及其制造方法
公开(公告)号：US20100072498A1
公开(公告)日：2010-03-25
申请号：US11919237
申请日：2006-04-27
申请人： Rong Jun Xie , Mamoru Mitomo , Naoto Hirosaki , Yoshinobu Yamamoto
发明人： Rong Jun Xie , Mamoru Mitomo , Naoto Hirosaki , Yoshinobu Yamamoto
IPC分类号： H01L33/00 , C09K11/64
CPC分类号： C09K11/0883 , C04B35/597 , C04B35/62675 , C04B2235/3203 , C04B2235/3208 , C04B2235/3224 , C04B2235/3852 , C04B2235/3865 , C04B2235/3873 , C04B2235/766 , C09K11/7734 , H01L33/502
摘要： According to the invention, a highly crystalline α-sialon is synthesized to emit highly intense light and a white LED showing an excellent color rendering characteristic is provided by shifting emitted light to the short wavelength side (blue shift). Such an α-sialon is designed so as to be expressed by general formula (Lix, Cay, Euz) (Si12-(m+n)Alm+n) (OnN16-n) wherein the numerical ranges of x, y, z, m and n are respectively 0
摘要翻译：根据本发明，合成高结晶性α-赛隆发射高强度光，并且通过将发射光移动到短波长侧（蓝移）来提供显示出优异显色特性的白色LED。这样的α赛隆被设计成通过通式（Lix，Cay，Euz）（Si12-（m + n）Alm + n）（OnN16-n）表示，其中x，y，z， m和n分别为0

5. 发明授权

US08883039B2 Fluorophor and method for production thereof and illuminator 有权
标题翻译：氟荧光体及其制造方法及照明装置
公开(公告)号：US08883039B2
公开(公告)日：2014-11-11
申请号：US11994391
申请日：2006-06-28
申请人： Naoto Hirosaki , Rong-Jun Xie , Mamoru Mitomo
发明人： Naoto Hirosaki , Rong-Jun Xie , Mamoru Mitomo
IPC分类号： C09K11/08 , C09K11/66 , H01K1/62 , H01J63/04 , C09K11/77 , H01L33/50 , H01L51/50
CPC分类号： C09K11/7734 , C09K11/0883 , H01L33/502 , H01L51/5036 , H01L2224/45144 , H01L2224/48091 , H01L2224/48247 , H01L2224/73265 , H01L2224/8592 , H01L2924/181 , H01L2924/00014 , H01L2924/00 , H01L2924/00012
摘要： A fluorophor which comprises as a main component, an α type sialon crystal containing at least Li, A element (wherein A represents one or more elements selected from among Mn, Ce, Pr, Nd, Sm, Eu, Tb, Dy, Er, Tm and Yb), M element (wherein M represents one or more metal elements except Li and the A element), Si, Al, oxygen and nitrogen. The fluorophor has an a type sialon crystal structure which is represented by the general formulae: (Lix1, Ax2, Mx3)(Si12−(m+n)Alm+n)(OnN16−n) 1.2≦x1≦2.4 (1) 0.001≦x2≦0.4 (2) and 0≦x3≦1.0 (3), and has a luminescence peak at a wavelength in the range of 400 to 700 nm. The above phosphor is reduced in the lowering of brightness, and can be suitably used for a white LED and the like.
摘要翻译：含有至少Li，A元素的α型赛隆晶体（其中A表示选自Mn，Ce，Pr，Nd，Sm，Eu，Tb，Dy，Er中的一种或多种元素的荧光体， Tm和Yb），M元素（其中M表示除了Li和A元素之外的一种或多种金属元素），Si，Al，氧和氮。荧光体具有由以下通式表示的类型的赛隆晶体结构：（Lix1，Ax2，Mx3）（Si12-（m + n）Alm + n）（OnN16-n）1.2＆nlE; x1＆nlE; 2.4（1） 0.001＆nlE; x2＆nlE; 0.4（2）和0＆nlE; x3＆nlE; 1.0（3），并且在400-700nm的波长处具有发光峰。上述荧光体在亮度降低方面降低，可适用于白色LED等。

6. 发明申请

US20090085465A1 FLUOROPHOR AND METHOD FOR PRODUCTION THEREOF AND ILLUMINATOR 有权
标题翻译：荧光剂及其生产方法和照明器
公开(公告)号：US20090085465A1
公开(公告)日：2009-04-02
申请号：US11994383
申请日：2006-06-28
申请人： Naoto Hirosaki , Rong-Jun Xie , Mamoru Mitomo
发明人： Naoto Hirosaki , Rong-Jun Xie , Mamoru Mitomo
IPC分类号： H01J1/62 , C09K11/59
CPC分类号： C09K11/7734 , C01B21/082 , C01P2002/54 , C01P2002/84 , C01P2004/03 , C01P2004/61 , C01P2004/62 , C01P2006/60 , C04B35/597 , C04B35/6262 , C04B35/6268 , C04B2235/3201 , C04B2235/3203 , C04B2235/3206 , C04B2235/3208 , C04B2235/3217 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3262 , C04B2235/3852 , C04B2235/3878 , C04B2235/3895 , C04B2235/40 , C04B2235/442 , C04B2235/465 , C04B2235/5296 , C04B2235/5409 , C04B2235/5436 , C04B2235/5445 , C04B2235/766 , C04B2235/79 , C04B2235/9646 , C09K11/0883 , H01L33/502 , H01L51/5036 , H01L2224/45144 , H01L2224/48091 , H01L2224/73265 , H01L2924/181 , H05B33/14 , H01L2924/00014 , H01L2924/00 , H01L2924/00012
摘要： A fluorophor comprising, as a main component, an α-type sialon crystal which contains at least an A element (wherein A represents one or more elements selected from among Mn, Ce, Pr, Nd, Sm, Eu, Tb, Dy, Er, Tm and Yb), an M element (wherein M represents one or more elements selected from among Li, Na, Mg, Ca, Y, La, Gd and Lu), Si, Al, oxygen and nitrogen, and is represented by the general formulae: (Mx, Ay)(Si12−(m+n)Alm+n)(OnN16−n) (1) m=δM×x+δA×y (2) 0.2≦x≦2.4 (3) 0.001≦y≦0.4 (4) and 0.5×m
摘要翻译：含有至少含有A元素（其中A表示选自Mn，Ce，Pr，Nd，Sm，Eu，Tb，Dy，Er中的一种或多种元素作为主要成分的荧光体），Tm和Yb），M元素（其中M表示选自Li，Na，Mg，Ca，Y，La，Gd和Lu中的一种或多种元素），Si，Al，氧和氮，并且由通式：（Mx，Ay）（Si12-（m + n）Alm + n）（OnN16-n）（1）m = deltaMxx + deltaAxy（2）0.2 <= x <= 2.4（3）0.001 <= y <= 0.4（4）和0.5×m

7. 发明授权

US5472919A .beta.-silicon nitride sintered body 失效
标题翻译： β-氮化硅烧结体
公开(公告)号：US5472919A
公开(公告)日：1995-12-05
申请号：US335967
申请日：1994-11-03
申请人： Mamoru Mitomo , Naoto Hirosaki , Motohide Ando
发明人： Mamoru Mitomo , Naoto Hirosaki , Motohide Ando
IPC分类号： C04B35/584 , C04B35/593 , C04B35/587
CPC分类号： C04B35/5935 , C04B35/584
摘要： A high strength and toughness .beta.-silicon nitride sintered body suitable for the material of a variety of structural parts. The sintered body contains .beta.-silicon nitride (Si.sub.3 N.sub.4) in an amount not less than 95% by weight of total silicon nitride; oxygen in a total amount not more than 3% by weight of the sintered body; and columnar grains each of which has a diameter not less than 5 .mu.m and an aspect ratio not less than 5, the columnar grains being in an amount not less than 0.5% by volume of total of raw materials in the sintered body; the sintered body having a bulk density not less than 96% of a theoretical density. Such a sintered body is produced by a method comprising the following steps in the sequence set forth: preparing powder of a starting material including .beta.-silicon nitride in an amount not less than 80% by weight of the starting material; adding oxide of at least one element selected from the group IIIa of the periodic table of elements in an amount ranging from 0.2% to 6% by weight (as a sintering assistant) to the starting material powder to form a mixture powder; compacting the mixture powder to form a compact; firing the compact under a nitrogen gas pressure ranging from 1 to 500 atm. at a temperature ranging from 1700.degree. to 2100 .degree. C. to form the sintered body; and continuing the firing step until a bulk density of the sintered body reaches a value not less than 96% of a theoretical density of the sintered body.
摘要翻译：高强度和韧性的β-氮化硅烧结体适用于各种结构部件的材料。烧结体含有不小于总氮化硅的95重量％的β-氮化硅（Si 3 N 4）。氧的总量不超过烧结体的3重量％; 柱状晶粒各自具有不小于5μm的直径和不小于5的纵横比，柱状晶粒的量不小于烧结体中原料总量的0.5体积％; 所述烧结体的体积密度不小于理论密度的96％。这样的烧结体通过包括下列步骤的方法制备：制备起始材料的粉末，该原料包括起始材料重量不小于80重量％的β-氮化硅; 添加选自元素周期表第IIIa族元素中的至少一种元素的氧化物，其量为0.2％至6％（重量）（作为烧结助剂）至原料粉末以形成混合物粉末; 压制混合粉末以形成紧凑型; 在1〜500atm的氮气压力下烧结压块。在1700〜2100℃的温度下形成烧结体; 继续烧成工序直到烧结体的体积密度达到烧结体的理论密度的96％以上。

8. 发明授权

US5401450A .beta.-silicon nitride sintered body and method of producing same 失效
标题翻译： β-氮化硅烧结体及其制造方法
公开(公告)号：US5401450A
公开(公告)日：1995-03-28
申请号：US992657
申请日：1992-12-18
申请人： Mamoru Mitomo , Naoto Hirosaki , Motohide Ando
发明人： Mamoru Mitomo , Naoto Hirosaki , Motohide Ando
IPC分类号： C04B35/584 , C04B35/593 , C04B35/58
CPC分类号： C04B35/5935 , C04B35/584
摘要： A high strength and toughness .beta.-silicon nitride sintered body suitable for the material of a variety of structural parts. The sintered body contains .beta.-silicon nitride (Si.sub.3 N.sub.4) in an amount not less than 95% by weight of total silicon nitride; oxygen in a total amount not more than 3% by weight of the sintered body; and columnar grains each of which has a diameter not less than 5 .mu.m and an aspect ratio not less than 5, the columnar grains being in an amount not less than 0.5% by volume of total of raw materials in the sintered body; the sintered body having a bulk density not less than 96% of a theoretical density. Such a sintered body is produced by a method comprising the following steps in the sequence set forth: preparing powder of a starting material including .beta.-silicon nitride in an amount not less than 80% by weight of the starting material; adding oxide of at least one element selected from the group IIIa of the periodic table of elements in an amount ranging from 0.2% to 6% by weight (as a sintering assistant) to the starting material powder to form a mixture powder; compacting the mixture powder to form a compact; firing the compact under a nitrogen gas pressure ranging from 1 to 500 atm. at a temperature ranging from 1700.degree. to 2100.degree. C. to form the sintered body; and continuing the firing step until a bulk density of the sintered body reaches a value not less than 96% of a theoretical density of the sintered body.
摘要翻译：高强度和韧性的β-氮化硅烧结体适用于各种结构部件的材料。烧结体含有不小于总氮化硅的95重量％的β-氮化硅（Si 3 N 4）。氧的总量不超过烧结体的3重量％; 柱状晶粒各自具有不小于5μm的直径和不小于5的纵横比，柱状晶粒的量不小于烧结体中原料总量的0.5体积％; 所述烧结体的体积密度不小于理论密度的96％。这样的烧结体通过包括下列步骤的方法制备：制备起始材料的粉末，该原料包括起始材料重量不小于80重量％的β-氮化硅; 添加选自元素周期表第IIIa族元素中的至少一种元素的氧化物，其量为0.2％至6％（重量）（作为烧结助剂）至原料粉末以形成混合物粉末; 压制混合粉末以形成紧凑型; 在1〜500atm的氮气压力下烧结压块。在1700〜2100℃的温度下形成烧结体; 继续烧成工序直到烧结体的体积密度达到烧结体的理论密度的96％以上。

9. 发明授权

US07906040B2 α-Sialon, α-sialon phosphor and method for producing the same 有权
标题翻译： α-赛隆，α-赛隆荧光体及其制造方法
公开(公告)号：US07906040B2
公开(公告)日：2011-03-15
申请号：US11629467
申请日：2005-06-14
申请人： Mamoru Mitomo , Naoto Hirosaki , Hideyuki Emoto , Masahiro Ibukiyama
发明人： Mamoru Mitomo , Naoto Hirosaki , Hideyuki Emoto , Masahiro Ibukiyama
IPC分类号： C09K11/08 , C09K11/66 , C09K11/61 , C09K11/02 , C09K11/77
CPC分类号： C09K11/7734 , C04B35/597 , C04B35/6262 , C04B2235/3203 , C04B2235/3206 , C04B2235/3208 , C04B2235/3215 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3865 , C04B2235/3873 , C04B2235/442 , C04B2235/445 , C04B2235/5436 , C04B2235/549 , C04B2235/658 , C04B2235/724 , C04B2235/766 , C04B2235/9646 , C09K11/0883
摘要： An α-sialon is offered which is represented by general formula: (M1)X(M2)Y(Si, Al)12(O, N)16 (wherein M1 represents one or more elements selected from the group which consists of Li, Mg, Ca, Y and lanthanoid (except La and Ce) and M2 represents one or more elements selected from the group which consists of Ce, Pr, Eu, Tb, Yb and Er and wherein 0.3
摘要翻译：提供α-sialon，其通式为：（M1）X（M2）Y（Si，Al）12（O，N）16（其中M1表示选自Li， Mg，Ca，Y和镧系元素（La和Ce除外），M2表示选自Ce，Pr，Eu，Tb，Yb和Er中的一种或多种元素，其中0.3

10. 发明授权

US07825580B2 Fluorophor and method for production thereof and illuminator 有权
标题翻译：氟荧光体及其制造方法及照明装置
公开(公告)号：US07825580B2
公开(公告)日：2010-11-02
申请号：US11994383
申请日：2006-06-28
申请人： Naoto Hirosaki , Rong-Jun Xie , Mamoru Mitomo
发明人： Naoto Hirosaki , Rong-Jun Xie , Mamoru Mitomo
IPC分类号： H01J1/63 , C09K11/66
CPC分类号： C09K11/7734 , C01B21/082 , C01P2002/54 , C01P2002/84 , C01P2004/03 , C01P2004/61 , C01P2004/62 , C01P2006/60 , C04B35/597 , C04B35/6262 , C04B35/6268 , C04B2235/3201 , C04B2235/3203 , C04B2235/3206 , C04B2235/3208 , C04B2235/3217 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3262 , C04B2235/3852 , C04B2235/3878 , C04B2235/3895 , C04B2235/40 , C04B2235/442 , C04B2235/465 , C04B2235/5296 , C04B2235/5409 , C04B2235/5436 , C04B2235/5445 , C04B2235/766 , C04B2235/79 , C04B2235/9646 , C09K11/0883 , H01L33/502 , H01L51/5036 , H01L2224/45144 , H01L2224/48091 , H01L2224/73265 , H01L2924/181 , H05B33/14 , H01L2924/00014 , H01L2924/00 , H01L2924/00012
摘要： A fluorophor comprising, as a main component, an α-type sialon crystal which contains at least an A element (wherein A represents one or more elements selected from among Mn, Ce, Pr, Nd, Sm, Eu, Tb, Dy, Er, Tm and Yb), an M element (wherein M represents one or more elements selected from among Li, Na, Mg, Ca, Y, La, Gd and Lu), Si, Al, oxygen and nitrogen, and is represented by the general formula: (Mx, Ay)(Si12−(m+n)Alm+n)(OnN16−n) (1) m=δM×x+δA×y (2) 0.2≦x≦2.4 (3) 0.001≦y≦0.4 (4) and 0.5×m
摘要翻译：含有至少含有A元素（其中A表示选自Mn，Ce，Pr，Nd，Sm，Eu，Tb，Dy，Er中的一种或多种元素作为主要成分的荧光体），Tm和Yb），M元素（其中M表示选自Li，Na，Mg，Ca，Y，La，Gd和Lu中的一种或多种元素），Si，Al，氧和氮，并且由通式（Mx，Ay）（Si12-（m + n）Alm + n）（OnN16-n）（1）m =δM×x +δA×y（2）0.2＆nlE; x＆nlE; 2.4（3）0.001 ＆nlE; y＆nlE; 0.4（4）和0.5×m

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