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1. 发明授权

US4764266A Integrated hydroprocessing scheme for production of premium quality distillates and lubricants 失效
标题翻译：一体化加氢处理方案，用于生产优质馏出物和润滑油
公开(公告)号：US4764266A
公开(公告)日：1988-08-16
申请号：US19983
申请日：1987-02-26
申请人： Nai Y. Chen , Rene B. LaPierre , Randall D. Partridge , Stephen S. Wong
发明人： Nai Y. Chen , Rene B. LaPierre , Randall D. Partridge , Stephen S. Wong
IPC分类号： C10G65/10 , C10G45/50 , C10G45/64 , C10G47/12 , C10G65/12 , F02B3/06 , C10G69/02
CPC分类号： C10G65/12 , F02B3/06
摘要： An integrated refining scheme for hydroprocessing high boiling fractions such as gas oil and catalytically cracked cycle oils to produce premium quality distillates, especially jet fuels and naphthas suitable for reforming into high octane gasoline. In addition, unconverted, high boiling fractions suitable for processing by conventional refining techniques into high quality, low pour point lube base stocks are obtained. The integrated hydroprocessing comprises a first stage hydrocracking step employing an aromatic selective hydrocracking catalyst based on a large pore size acidic component such as amorphous alumina or silica alumina or a large pore size zeolite such as zeolite X or zeolite Y. The hydrocracking may be operated either in a naphtha directing mode under conditions of moderate to high severity or under conditions of low to moderate severity to produce a relatively higher proportion of product boiling in the middle distillate range. The unconverted fraction from the hydrocracking step is passed to a second step in which it is hydroprocessed over a zeolite beta catalyst with additional hydrogenation-dehydrogenation functionality. In this stage, the paraffins remaining in the feed are attacked by the zeolite beta to form isoparaffins and conditions may be controlled to favor hydroisomerization over hydrocracking so as to increase the yield of middle distillate product, especially of high isoparaffinic jet fuels and diesel fuel.

2. 发明授权

US4518485A Hydrotreating/isomerization process to produce low pour point distillate fuels and lubricating oil stocks 失效
标题翻译：加氢处理/异构化工艺生产低倾点馏出燃料和润滑油库存
公开(公告)号：US4518485A
公开(公告)日：1985-05-21
申请号：US557696
申请日：1983-12-02
申请人： Rene B. LaPierre , Randall D. Partridge , Nai Y. Chen , Stephen S. Wong
发明人： Rene B. LaPierre , Randall D. Partridge , Nai Y. Chen , Stephen S. Wong
IPC分类号： C10G29/06 , C10G45/64 , C10G65/12
CPC分类号： C10G45/64 , C10G29/06
摘要： A process for dewaxing a hydrocarbon feedstock with a relatively high pour point and containing paraffins selected from the group of normal paraffins and slightly branched paraffins and sulfur and nitrogen compounds which comprises subjecting said oil to hydrotreating in a hydrotreating zone operated at hydrotreating conditions sufficient to remove at least a portion of said sulfur and nitrogen compounds and subjecting said hydrotreated oil to catalytic dewaxing by contacting said oil with a catalyst comprising zeolite beta having a silica/alumina ratio of at least 30:1 and a hydrogenation/dehydrogenation component under isomerization conditions.
摘要翻译：一种使具有较高倾点的烃原料脱蜡并含有选自正构烷烃和轻支化链烷烃和硫和氮化合物的链烷烃的方法，其包括使所述油在加氢处理区中加氢处理，所述加氢处理区在加氢处理条件下操作，所述加氢处理条件足以除去所述硫和氮化合物的至少一部分，并使所述加氢处理的油通过使所述油与二氧化硅/氧化铝比为至少30:1的沸石β和在异构化条件下的氢化/脱氢组分接触的催化剂进行催化脱蜡。

3. 发明授权

US4851109A Integrated hydroprocessing scheme for production of premium quality distillates and lubricants 失效
标题翻译：一体化加氢处理方案，用于生产优质馏出物和润滑剂
公开(公告)号：US4851109A
公开(公告)日：1989-07-25
申请号：US192072
申请日：1988-05-09
申请人： Nai Y. Chen , Rene B. LaPierre , Randall D. Partridge , Stephen S. Wong
发明人： Nai Y. Chen , Rene B. LaPierre , Randall D. Partridge , Stephen S. Wong
IPC分类号： C10G65/12 , F02B3/06
CPC分类号： C10G65/12 , C10G2300/1074 , C10G2400/02 , C10G2400/04 , C10G2400/08 , F02B3/06
摘要： An integrated refining scheme for hydroprocessing high boiling fractions such as gas oil and catalytically cracked cycle oils to produce premium quality distillates, especially jet fuels and naphthas suitable for reforming into high octane gasoline. In addition, unconverted, high boiling fractions suitable for processing by conventional refining techniques into high quality, low pour point lube base stocks are obtained. The integrated hydroprocessing comprises a first stage hydrocracking step employing an aromatic selective hydrocracking catalyst based on a large pore size acidic component such as amorphous alumina or silica alumina or a large pore size zeolite such as zeolite X or zeolite Y. The hydrocracking may be operated either in a naphtha directing mode under conditions of moderate to high severity or under conditions of low to moderate severity to produce a relatively higher proportion of product boiling in the middle distillate range. The unconverted fraction from the hydrocracking step is passed to a second step in which it is hydroprocessed over a zeolite beta catalyst with additional hydrogenation-dehydrogenation functionality. In this stage, the paraffins remaining in the feed are attacked by the zeolite beta to form isoparaffins and conditions may be controlled to favor hydroisomerization over hydrocracking so as to increase the yield of middle distillate product, especially of highly isoparaffinic jet fuels and diesel fuel.
摘要翻译：一种用于加氢处理高沸点馏分（如瓦斯油和催化裂解循环油）的综合精炼方案，以生产优质馏出物，特别是适用于重整为高辛烷值汽油的喷气燃料和石脑油。此外，获得了适用于通过常规精制技术加工成高质量低倾点润滑油基础油料的未转化的高沸点馏分。一体化加氢处理包括使用基于大孔径酸性组分如无定形氧化铝或二氧化硅氧化铝或大孔径沸石如沸石X或沸石Y的芳族选择性加氢裂化催化剂的第一阶段加氢裂化步骤。加氢裂化可以在中等至高严重度的条件下或在低至中等严重度的条件下以石脑油引导模式在中间馏分范围内产生相对较高比例的沸点产物。来自加氢裂化步骤的未转化的级分被传递到第二步骤，其中其在具有另外的氢化 - 脱氢官能团的沸石β催化剂上进行加氢处理。在这个阶段，剩余在饲料中的链烷烃被沸石β攻击以形成异链烷烃，并且可以控制条件以有利于加氢裂化加氢异构化，从而提高中间馏分产物，特别是高度异链烷烃喷气燃料和柴油燃料的产率。

4. 发明授权

US4962269A Isomerization process 失效
标题翻译：异构化过程
公开(公告)号：US4962269A
公开(公告)日：1990-10-09
申请号：US280399
申请日：1988-12-05
申请人： Rene B. LaPierre , Randall D. Partridge , Stephen S. Wong
发明人： Rene B. LaPierre , Randall D. Partridge , Stephen S. Wong
IPC分类号： B01J29/12 , B01J29/74 , C07C5/27 , C10G29/06 , C10G35/095 , C10G45/64
CPC分类号： C10G45/64 , C07C5/2791 , C10G29/06 , C10G35/095 , B01J2229/16 , B01J2229/37 , B01J29/126 , B01J29/7415
摘要： Long chain (C.sub.7+) paraffins are isomerized over a large pore, highly siliceous zeolite catalyst such as zeolite Y or ZSM-20 having a structural silica:alumina ratio of at least 10:1. The use of the highly siliceous zeolite inhibits the degree of cracking and also permits weaker hydrogenation components such as palladium to be used in the catalyst.
摘要翻译：长链（C7 +）链烷烃在大孔，高硅硅沸石催化剂如沸石Y或ZSM-20上异构化，其结构二氧化硅：氧化铝比至少为10:1。使用高度硅质的沸石抑制裂化的程度，并且还允许较弱的氢化组分如钯用于催化剂中。

5. 发明授权

US5419830A Method for controlling hydrocracking and isomerization dewaxing 失效
标题翻译：控制加氢裂化和异构脱蜡的方法
公开(公告)号：US5419830A
公开(公告)日：1995-05-30
申请号：US102675
申请日：1993-08-05
申请人： Tai-Sheng Chou , Nai Y. Chen , Grant G. Karsner , Clinton R. Kennedy , Rene B. LaPierre , Melcon G. Melconian , Richard J. Quann , Stephen S. Wong
发明人： Tai-Sheng Chou , Nai Y. Chen , Grant G. Karsner , Clinton R. Kennedy , Rene B. LaPierre , Melcon G. Melconian , Richard J. Quann , Stephen S. Wong
IPC分类号： C10G45/64 , C10G47/16 , C10G47/36
CPC分类号： C10G45/64 , C10G47/16 , C10G47/36 , Y10S208/01
摘要： Nitrogenous compounds especially bases such as ammonia vapor are used to control the operation of a hydrocracker or catalytic dewaxer. Catalyst activity and selectivity may be controlled by addition of the base to the feed, for example, to control the balance between isomerization and hydrocracking in an operation using a zeolite beta catalyst. Runaway conditions may be controlled by the addition of nitrogenous compounds to regulate the temperature profile within the reactor.
摘要翻译：氮化合物尤其是碱例如氨蒸汽用于控制加氢裂化器或催化脱蜡机的运行。催化剂活性和选择性可以通过向进料添加碱来控制，例如在使用沸石β催化剂的操作中控制异构化和加氢裂化之间的平衡。失控条件可以通过加入含氮化合物来控制，以调节反应器内的温度分布。

6. 发明授权

US06416654B1 Method for controlling hydrocracking and isomerization dewaxing operations 失效
标题翻译：控制加氢裂化和异构脱蜡操作的方法
公开(公告)号：US06416654B1
公开(公告)日：2002-07-09
申请号：US08367418
申请日：1994-12-30
申请人： Tai-Sheng Chou , Nai Yuen Chen , Grant G. Karsner , Clinton R. Kennedy , Rene B. LaPierre , Melcon G. Melconian , Richard J. Quann , Stephen S. Wong
发明人： Tai-Sheng Chou , Nai Yuen Chen , Grant G. Karsner , Clinton R. Kennedy , Rene B. LaPierre , Melcon G. Melconian , Richard J. Quann , Stephen S. Wong
IPC分类号： C10G7342
CPC分类号： C10G45/64 , C10G47/16 , C10G47/36 , Y10S208/01
摘要： Nitrogenous compounds especially bases such as ammonia vapor are used to control the operation of a hydrocracker or catalytic dewaxer. Catalyst activity and selectivity may be controlled by addition of the base to the feed, for example, to control the balance between isomerization and hydrocracking in an operation using a zeolite beta catalyst. Runaway conditions may be controlled by the addition of nitrogenous compounds to regulate the temperature profile within the reactor.
摘要翻译：氮化合物尤其是碱例如氨蒸汽用于控制加氢裂化器或催化脱蜡机的运行。催化剂活性和选择性可以通过向进料添加碱来控制，例如在使用沸石β催化剂的操作中控制异构化和加氢裂化之间的平衡。失控条件可以通过加入含氮化合物来控制，以调节反应器内的温度分布。

7. 发明授权

US5100535A Method for controlling hydrocracking operations 失效
标题翻译：控制加氢裂化作业的方法
公开(公告)号：US5100535A
公开(公告)日：1992-03-31
申请号：US279748
申请日：1988-12-05
申请人： Nai Yuen Chen , Tai-Sheng Chou , Grant G. Karsner , Clinton R. Kennedy , Rene B. LaPierre , Melcon G. Melconian , Richard J. Quann , Stephen S. Wong
发明人： Nai Yuen Chen , Tai-Sheng Chou , Grant G. Karsner , Clinton R. Kennedy , Rene B. LaPierre , Melcon G. Melconian , Richard J. Quann , Stephen S. Wong
IPC分类号： C10G45/64 , C10G47/16 , C10G47/36
CPC分类号： C10G47/36 , C10G45/64 , C10G47/16 , Y10S208/01
摘要： Nitrogenous compounds especially bases such as amines are used to control the operation of a hydrocracker. Catalyst activity and selectivity may be controlled by addition of the base to the feed, for example, to control the balance between isomerization and conversion in an operation using a zeolite beta catalyst. Runaway conditions may be controlled by the addition of nitrogenous compounds and if they are added at intermediate points along the length of the reactor, the temperature profile within the reactor can be effectively regulated.
摘要翻译：氮化合物特别是碱例如胺用于控制加氢裂化器的操作。催化剂活性和选择性可以通过向进料添加碱来控制，例如在使用沸石β催化剂的操作中控制异构化和转化之间的平衡。失控条件可以通过加入含氮化合物来控制，并且如果它们在反应器长度的中间点加入，则反应器内的温度曲线可被有效地调节。

8. 发明授权

US4500417A Conversion of Fischer-Tropsch products 失效
标题翻译：费托产品的转化
公开(公告)号：US4500417A
公开(公告)日：1985-02-19
申请号：US453970
申请日：1982-12-28
申请人： Nai Y. Chen , Werner O. Haag , Tracy J. Huang , Stephen S. Wong
发明人： Nai Y. Chen , Werner O. Haag , Tracy J. Huang , Stephen S. Wong
IPC分类号： C10G45/64 , B01J29/00 , B01J29/74 , B01J29/78 , C07C1/00 , C07C1/04 , C07C9/00 , C07C67/00 , C10G47/16 , C10G49/08 , C10G47/20
CPC分类号： C10G47/16 , B01J2229/37 , B01J29/7415 , B01J29/7815 , Y10S208/95
摘要： The high boiling fraction of Fischer-Tropsch synthesis is upgraded by contact with a catalyst comprising a high-silica, large pore zeolite and a hydrogenation component. The products are a distillate fraction characterized by low sulfur and nitrogen content, high isoparaffin content and low pour point and a lube fraction characterized by its high viscosity index and low pour point.
摘要翻译：通过与包含高二氧化硅，大孔沸石和氢化组分的催化剂接触来提高费 - 托合成的高沸点馏分。该产品是以低硫和氮含量，高异链烷烃含量和低倾点为特征的馏出物部分，其特征在于其高粘度指数和低倾点。

9. 发明授权

US4919788A Lubricant production process 失效
标题翻译：润滑油生产过程
公开(公告)号：US4919788A
公开(公告)日：1990-04-24
申请号：US260857
申请日：1988-10-21
申请人： Nai Y. Chen , William E. Garwood , Tracy J. Huang , Quang N. Le , Stephen S. Wong
发明人： Nai Y. Chen , William E. Garwood , Tracy J. Huang , Quang N. Le , Stephen S. Wong
IPC分类号： C10G45/64 , C10G65/04 , C10G67/04
CPC分类号： C10G67/04 , C10G45/64 , C10G65/043
摘要： A process for producing lubricant oils of low pour point and high viscosity index by first carrying out a partial dewaxing of a lubricant base stock in an initial catalytic dewaxing operation, followed by a selective dewaxing step. The initial catalytic dewaxing step is carried out using a large pore, high silica zeolite dewaxing catalyst such as high silica Y or zeolite beta which dewaxes by isomerizing the waxy components of the base stock to less waxy brance chain isoparaffins but the severity of the operation is controlled so as to effect only a partial removal of the waxy components. Further removal of the waxy components is effected during the subsequent dewaxing step which is selective for the removal of the more waxy n-paraffin components, leaving the branched chain isoparaffins which contribute to a high VI in the product. The selective dewaxing step may be either a solvent, e.g. MEK dewaxing operation or a catalytic dewaxing using a highly shape selective zeolite such as ZSM-22 or ZSM-23. The severity of the initial catalytic dewaxing operation may be controlled so as to effect a net increase in the content of isoparaffins and because of the selective nature of the solvent dewaxing step, this increased isoparaffins concentration may be retained, producing a product of high VI. The pour point of the feedstock is preferably reduced during the initial catalytic dewaxing step to a value which is no lower than 10.degree. F. and preferably no lower than 20.degree. F., above the target pour point for the products. Generally, this will entail a reduction of at least 10.degree. F. and preferably at least 20.degree. F. in the pour point of the feed.
摘要翻译：首先在初始催化脱蜡操作中进行润滑剂原料的部分脱蜡，然后进行选择性脱蜡步骤，生产低倾点和高粘度指数的润滑油的方法。初始催化脱蜡步骤使用大孔，高二氧化硅沸石脱蜡催化剂如高二氧化硅Y或沸石β进行，该脱蜡通过使基础油料的蜡质组分异构化成较少的蜡状分支链异链烷烃，但操作的严重性是被控制以仅影响蜡组分的部分去除。在随后的脱蜡步骤中进一步除去蜡状组分，该脱蜡步骤选择性地除去更多的蜡状正链烷烃组分，留下有助于产物中高VI的支链异链烷烃。选择性脱蜡步骤可以是溶剂，例如 MEK脱蜡操作或使用ZSM-22或ZSM-23等高选择性沸石的催化脱蜡。可以控制初始催化脱蜡操作的严重性，以便实现异链烷烃含量的净增加，并且由于溶剂脱蜡步骤的选择性，可以保留这种增加的异链烷烃浓度，从而产生高VI的产物。原料的倾点优选在初始催化脱蜡步骤期间降低至不低于产物的目标倾点的10°F，优选不低于20°F的值。通常，这将导致在进料的倾点下降至少10°F，优选至少降低20°F。

10. 发明授权

US5620590A Hydrocracking process using small crystal size zeolite Y 失效
标题翻译：使用小晶体尺寸的沸石Y进行加氢裂化处理
公开(公告)号：US5620590A
公开(公告)日：1997-04-15
申请号：US236872
申请日：1994-04-29
申请人： Robert P. L. Absil , James R. Katzer , Daria N. Lissy , Robert A. Ware , Stephen S. Wong
发明人： Robert P. L. Absil , James R. Katzer , Daria N. Lissy , Robert A. Ware , Stephen S. Wong
IPC分类号： B01J29/16 , C10G47/16 , C10G47/20
CPC分类号： C10G47/20 , B01J29/166 , C10G47/16
摘要： There is provided a process and a catalyst for hydrocracking hydrocarbons, such as gas oils. The catalyst comprises a hydrogenating metal and small crystal size zeolite Y. The zeolite Y may have a crystal size of less than one micron. Examples of hydrogenating metals include nickel and tungsten.
摘要翻译：提供了用于烃类加氢裂化（如瓦斯油）的方法和催化剂。催化剂包括氢化金属和小晶体尺寸的沸石Y.沸石Y可以具有小于1微米的晶体尺寸。氢化金属的实例包括镍和钨。

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