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1. 发明专利

JPS60194075A Manufacture of carbon film 失效
标题翻译：碳膜的制造
公开(公告)号：JPS60194075A
公开(公告)日：1985-10-02
申请号：JP4916684
申请日：1984-03-16
申请人： Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： YOSHIMURA SUSUMU , MURAKAMI MUTSUAKI
IPC分类号： C01B31/02 , C01B31/04 , C23C16/26
CPC分类号： C23C16/26
摘要： PURPOSE:To improve conditions during the manufacture of a carbon film and the electric conductivity of the resulting film by heating a compound such as poly-p-phenylene oxide in an atmosphere of a gas such as Ar to generate a gasified component and by depositing the component on a substrate heated to a prescribed temp. CONSTITUTION:A high molecular org. compound selected among poly-p-phenylene oxide, poly-p-phenylene sulfide, poly-p-xylene, polysulfone, polycarbonate, polyethylene terephthalate and derivs. of them each having an alkyl substituent in the aromatic ring is heated in vacuum or an atmosphere of a gas such as Ar, He, N2 or H2. A gasified component generated by the heating is deposited on a substrate heated to >=700 deg.C.
摘要翻译：目的：通过在诸如Ar的气体气氛中加热诸如聚对苯二酚的化合物来改善制备碳膜期间的条件和所得膜的电导率，以产生气化组分，并通过沉积在加热到规定温度的基板上的部件。构成：高分子组织。选自聚对苯二酚，聚对苯硫醚，聚对二甲苯，聚砜，聚碳酸酯，聚对苯二甲酸乙二醇酯和衍生物的化合物。在芳环中具有烷基取代基的各自在真空或诸如Ar，He，N 2或H 2的气体气氛中加热。通过加热产生的气化组分沉积在加热至> = 700℃的基底上。

2. 发明专利

JPS6155220A Production of carbonaceous fiber 失效
标题翻译：生产碳纤维
公开(公告)号：JPS6155220A
公开(公告)日：1986-03-19
申请号：JP17516384
申请日：1984-08-24
申请人： Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： MURAKAMI MUTSUAKI , YOSHIMURA SUSUMU
IPC分类号： D01F9/12 , D01F9/127
摘要： PURPOSE: To obtain carbonaceous fiber from a solid starting raw material, by molding an organic compound which is solid at normal temperature at normal pressure and is decomposed under heating, heating the molded article in an atmosphere of an inert gas, etc. in such a way that temperature difference is produced in the molded article, subjecting a decomposed product to gaseous- phase growth on the molded article.
CONSTITUTION: An organic compound (e.g., pyromellitic dianhydride, etc.) which is solid at normal temperature at normal pressure and is decomposed or partially decomposed under heating is molded into a film, etc., to give a molded article. Then, the molded article 2 is placed on the ceramic substrate 3, etc., put in the furnace 4. While the molded article is heated in an inert gas or under vacuum by the heater 1 in such a way that the temperature difference is produced in the molded article 2, and a decomposed product is subjected to gaseous-phase growth on the molded article, to give the aimed carbonaceous fiber.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：为了从固体起始原料中获得碳质纤维，通过在常压下常压固化并在加热下分解成型有机化合物，在惰性气体等的气氛中加热成型品在模制品中产生温差的方法，使分解产物在模塑制品上进行气相生长。构成：在常压常温下固化并在加热下分解或部分分解的有机化合物（例如均苯四酸二酐等）成型为薄膜等，得到成型品。然后，将模制品2放置在放置在炉4中的陶瓷基板3等上。当模制品在惰性气体中或在加热器1的真空下被加热，使得产生温度差在模塑制品2中，并将分解产物在模塑制品上进行气相生长，得到目标碳质纤维。

3. 发明专利

JPS60195014A Production of carbon coating film 失效
标题翻译：生产碳涂膜
公开(公告)号：JPS60195014A
公开(公告)日：1985-10-03
申请号：JP4916584
申请日：1984-03-16
申请人： Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： YOSHIMURA SUSUMU , MURAKAMI MUTSUAKI
IPC分类号： C04B35/52 , C01B31/02 , C01B31/04 , C23C14/06 , C23C16/26
摘要： PURPOSE: A support base is coated with a specific aromatic polymer compound, and carbon coating film is deposited on the support by decomposing the coating with heat under vacuum where by uniform carbon coating films with high electroconductivity and high hardness is formed at a relative temperature.
CONSTITUTION: An aromatic high polymer which has large amounts of components to be gasified on pyrolysis such as polyparaphenylene oxide, polyparaphenylene sulfide, polycarbonate or phenolic resin is used to coat the support base such as a plate of carbon, silicon, alumina, silicon carbide or boron nitride in the form of a solution and dried. A film of the high polymer may be held between the support bases. Then, the coated bases are heated in an inert atmosphere or under vacuum over 700°C to deposit the carbon formed on the base.
COPYRIGHT: (C)1985,JPO&Japio
摘要翻译：目的：用特定的芳族聚合物化合物涂覆支撑体，通过在真空下分解涂层，通过在相对温度下形成具有高导电性和高硬度的均匀碳涂膜，将碳涂膜沉积在载体上。构成：使用具有大量待热解气化成分的芳香族高分子聚合物，如聚对苯二酚，聚对苯硫醚，聚碳酸酯或酚醛树脂，以涂覆碳，硅，氧化铝，碳化硅等载体基溶液形式的氮化硼并干燥。高分子聚合物膜可以保持在支撑基底之间。然后，将涂覆的基材在惰性气氛中或真空下在700℃以上加热以沉积形成在基底上的碳。

4. 发明专利

JPS6155221A Production of carbonaceous or graphitic fiber having improved electrical conductivity 失效
标题翻译：生产具有改善电导率的碳纤维或纤维纤维
公开(公告)号：JPS6155221A
公开(公告)日：1986-03-19
申请号：JP17516284
申请日：1984-08-24
申请人： Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： MURAKAMI MUTSUAKI , YOSHIMURA SUSUMU
IPC分类号： D01F9/12 , D01F9/127 , D01F9/14 , D01F11/10 , H01B1/04
摘要： PURPOSE: To obtain the titled fiber having improved electricalconductivity, by vaporizing an aromatic 2 acid anhydride, an aromatic diimide compound, etc. in a gas atmosphere of argon, etc. under heating, subjecting it to gaseous-phase growth to give carbonaceous fiber, heat-treating the carbonaceous fiber, and doping it with a dopant.
CONSTITUTION: An aromatic 2 acid anhydride (e.g., 3,4,9,10-perylenetetracarboxylic acid dianhydride, etc.), an aromatic diimide compound, or a compound to produce the aromatic 2 acid anhydride or the aromatic diimide under heating is vaporized in an atmosphere of argon, nitrogen, helium, hydrogen, or their mixed gas or in vacuum under heating, and subjected to gaseous-phase growth, to give carbonaceous fiber. Then, the carbonaceous fiber or fiber obtained by graphitizing the carbonaceous fiber by heat treatment is doped with a dopant having acceptor or donor properties, to give the aimed fiber having improved electrical conductivity.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：为了获得具有改善的导电性的标题纤维，通过在氩气气氛下在加热下蒸发芳族二酸酐，芳族二酰亚胺化合物等，使其进行气相生长，得到碳质纤维，热处理碳质纤维，并掺杂掺杂剂。构成：在加热下，芳香族二酸酐（例如3,4,9,10-苝四羧酸二酐等），芳香族二酰亚胺化合物或芳香族二酸酐或芳香族二酰亚胺的化合物在氩气，氮气，氦气，氢气或其混合气体的气氛或加热下的真空中进行气相生长，得到碳质纤维。然后，通过热处理对碳质纤维进行石墨化而获得的碳质纤维或纤维掺杂有具有受体或者给体特性的掺杂剂，得到具有改善的导电性的目标纤维。

5. 发明专利

JPS59199754A Manufacture of conductive polymer 失效
标题翻译：导电聚合物的制造
公开(公告)号：JPS59199754A
公开(公告)日：1984-11-12
申请号：JP7411283
申请日：1983-04-28
申请人： Yoshitsugu Isamoto , Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： ISAMOTO YOSHITSUGU , MURAKAMI MUTSUAKI , YOSHIMURA SUSUMU
IPC分类号： C08L79/08 , C08L65/00 , C08L65/02 , C08L77/00 , C08L79/04 , C08L81/00 , H01B1/12
CPC分类号： C08G2261/312
摘要： PURPOSE: To obtain a flexible conductive polymer with high thermal and chemical stability, by heat treatment, in an inert gas or a vacuum, of a heat-resistant polymer capable of forming polycyclic aromatic structure by heating, pyrolysis, and recombination, followed by chemically doping.
CONSTITUTION: A heat-resistant polymer capable of forming polycyclic aromatic structure by heating, pyrolysis, and recombination, is heat-treated, in an inert gas or a vacuum, under such a condition as to form said structure while retaining flexibility. The resulting product is subjected to chemical doping with a dopant serving as an acceptor. Said heat-resistant polymer is e.g., an aromatic polyamide, aromatic polyamideimide, being heat-treated normally at ≥200°C. Said dopant is pref. H
2 SO
4 or SO
3 gas, enabling the objective polymer to be improved in its electrical conductivity up to 10
12 order; however, I
2 , HF, FeCl
3 , etc. are also effective.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过加热，热解和再结合能形成多环芳族结构的耐热聚合物，通过在惰性气体或真空中热处理，获得具有高热稳定性和化学稳定性的柔性导电聚合物，然后化学掺杂。构成：通过加热，热解和复合形成多环芳族结构的耐热聚合物，在惰性气体或真空中，在形成所述结构同时保持柔韧性的条件下进行热处理。将所得产物用作为受体的掺杂剂进行化学掺杂。所述耐热聚合物是例如芳族聚酰胺，芳族聚酰胺酰亚胺，在≥200℃下通常进行热处理。所述掺杂剂是优选的。 H2SO4或SO3气体，使目标聚合物的电导率提高到10 12阶; 然而，I2，HF，FeCl3等也是有效的。

6. 发明专利

JPS59105029A Polymeric conductor 失效
标题翻译：聚合物导体
公开(公告)号：JPS59105029A
公开(公告)日：1984-06-18
申请号：JP21462982
申请日：1982-12-09
申请人： Yoshitsugu Isamoto , Shigeaki Mizogami , Mutsuaki Murakami , Res Dev Corp Of Japan , Hiroyuki Yasujima , Susumu Yoshimura
发明人： YOSHIMURA SUSUMU , MURAKAMI MUTSUAKI , ISAMOTO YOSHITSUGU , MIZOGAMI SHIGEAKI , YASUJIMA HIROYUKI
IPC分类号： C08G73/00 , C08G73/06 , C08G73/08 , C08G85/00 , H01B1/12
摘要： PURPOSE: A polymeric conductor excellent in heat stability and suitable for use in electronic circuits elements, sensor materials, etc., obtained by heat-treating poly(p-phenylene-1,3,4-oxadiazole) under a specified condition.
CONSTITUTION: A film, 25W50μ thick, is obtained by casting poly(p-phenylene-1, 3,4-oxadiazole) which is obtained by polycondensing terephthalic acid with hydrazine and then ring-closing the obtained polyhydrazine by dehydration. The obtained film is supported on an alumina carrier or the like and heat-treated at 520W1,400°C in vacuum or an inert gas to form a nitrogen-containing condensed polycyclic ring structure.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过在特定条件下热处理聚（对亚苯基-1,3,4-恶二唑）而获得的热稳定性优异且适用于电子电路元件，传感器材料等的聚合物导体。构成：通过将对苯二甲酸与肼缩聚而得到的聚（对亚苯基-1,3,4-恶二唑）浇铸，然后通过脱水闭环所得多肼，得到25-50μm厚的薄膜。将得到的膜负载在氧化铝载体等上，在真空或惰性气体中在520-1,400℃进行热处理，形成含氮缩合多环结构。

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