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1. 发明专利

JPS6224522B2 JPS6224522B2 - 失效
公开(公告)号：JPS6224522B2
公开(公告)日：1987-05-28
申请号：JP4916784
申请日：1984-03-16
申请人： Shingijutsu Kaihatsu Jigyodan , Mutsuaki Murakami
发明人： MURAKAMI MUTSUAKI
IPC分类号： D01F9/12 , D01F9/127

2. 发明专利

JPS60194075A Manufacture of carbon film 失效
标题翻译：碳膜的制造
公开(公告)号：JPS60194075A
公开(公告)日：1985-10-02
申请号：JP4916684
申请日：1984-03-16
申请人： Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： YOSHIMURA SUSUMU , MURAKAMI MUTSUAKI
IPC分类号： C01B31/02 , C01B31/04 , C23C16/26
CPC分类号： C23C16/26
摘要： PURPOSE:To improve conditions during the manufacture of a carbon film and the electric conductivity of the resulting film by heating a compound such as poly-p-phenylene oxide in an atmosphere of a gas such as Ar to generate a gasified component and by depositing the component on a substrate heated to a prescribed temp. CONSTITUTION:A high molecular org. compound selected among poly-p-phenylene oxide, poly-p-phenylene sulfide, poly-p-xylene, polysulfone, polycarbonate, polyethylene terephthalate and derivs. of them each having an alkyl substituent in the aromatic ring is heated in vacuum or an atmosphere of a gas such as Ar, He, N2 or H2. A gasified component generated by the heating is deposited on a substrate heated to >=700 deg.C.
摘要翻译：目的：通过在诸如Ar的气体气氛中加热诸如聚对苯二酚的化合物来改善制备碳膜期间的条件和所得膜的电导率，以产生气化组分，并通过沉积在加热到规定温度的基板上的部件。构成：高分子组织。选自聚对苯二酚，聚对苯硫醚，聚对二甲苯，聚砜，聚碳酸酯，聚对苯二甲酸乙二醇酯和衍生物的化合物。在芳环中具有烷基取代基的各自在真空或诸如Ar，He，N 2或H 2的气体气氛中加热。通过加热产生的气化组分沉积在加热至> = 700℃的基底上。

3. 发明专利

JPS6155220A Production of carbonaceous fiber 失效
标题翻译：生产碳纤维
公开(公告)号：JPS6155220A
公开(公告)日：1986-03-19
申请号：JP17516384
申请日：1984-08-24
申请人： Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： MURAKAMI MUTSUAKI , YOSHIMURA SUSUMU
IPC分类号： D01F9/12 , D01F9/127
摘要： PURPOSE: To obtain carbonaceous fiber from a solid starting raw material, by molding an organic compound which is solid at normal temperature at normal pressure and is decomposed under heating, heating the molded article in an atmosphere of an inert gas, etc. in such a way that temperature difference is produced in the molded article, subjecting a decomposed product to gaseous- phase growth on the molded article.
CONSTITUTION: An organic compound (e.g., pyromellitic dianhydride, etc.) which is solid at normal temperature at normal pressure and is decomposed or partially decomposed under heating is molded into a film, etc., to give a molded article. Then, the molded article 2 is placed on the ceramic substrate 3, etc., put in the furnace 4. While the molded article is heated in an inert gas or under vacuum by the heater 1 in such a way that the temperature difference is produced in the molded article 2, and a decomposed product is subjected to gaseous-phase growth on the molded article, to give the aimed carbonaceous fiber.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：为了从固体起始原料中获得碳质纤维，通过在常压下常压固化并在加热下分解成型有机化合物，在惰性气体等的气氛中加热成型品在模制品中产生温差的方法，使分解产物在模塑制品上进行气相生长。构成：在常压常温下固化并在加热下分解或部分分解的有机化合物（例如均苯四酸二酐等）成型为薄膜等，得到成型品。然后，将模制品2放置在放置在炉4中的陶瓷基板3等上。当模制品在惰性气体中或在加热器1的真空下被加热，使得产生温度差在模塑制品2中，并将分解产物在模塑制品上进行气相生长，得到目标碳质纤维。

4. 发明专利

JPS60195014A Production of carbon coating film 失效
标题翻译：生产碳涂膜
公开(公告)号：JPS60195014A
公开(公告)日：1985-10-03
申请号：JP4916584
申请日：1984-03-16
申请人： Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： YOSHIMURA SUSUMU , MURAKAMI MUTSUAKI
IPC分类号： C04B35/52 , C01B31/02 , C01B31/04 , C23C14/06 , C23C16/26
摘要： PURPOSE: A support base is coated with a specific aromatic polymer compound, and carbon coating film is deposited on the support by decomposing the coating with heat under vacuum where by uniform carbon coating films with high electroconductivity and high hardness is formed at a relative temperature.
CONSTITUTION: An aromatic high polymer which has large amounts of components to be gasified on pyrolysis such as polyparaphenylene oxide, polyparaphenylene sulfide, polycarbonate or phenolic resin is used to coat the support base such as a plate of carbon, silicon, alumina, silicon carbide or boron nitride in the form of a solution and dried. A film of the high polymer may be held between the support bases. Then, the coated bases are heated in an inert atmosphere or under vacuum over 700°C to deposit the carbon formed on the base.
COPYRIGHT: (C)1985,JPO&Japio
摘要翻译：目的：用特定的芳族聚合物化合物涂覆支撑体，通过在真空下分解涂层，通过在相对温度下形成具有高导电性和高硬度的均匀碳涂膜，将碳涂膜沉积在载体上。构成：使用具有大量待热解气化成分的芳香族高分子聚合物，如聚对苯二酚，聚对苯硫醚，聚碳酸酯或酚醛树脂，以涂覆碳，硅，氧化铝，碳化硅等载体基溶液形式的氮化硼并干燥。高分子聚合物膜可以保持在支撑基底之间。然后，将涂覆的基材在惰性气氛中或真空下在700℃以上加热以沉积形成在基底上的碳。

5. 发明专利

JPS60194119A Production of carbon fiber 失效
标题翻译：生产碳纤维
公开(公告)号：JPS60194119A
公开(公告)日：1985-10-02
申请号：JP4916784
申请日：1984-03-16
申请人： Mutsuaki Murakami , Res Dev Corp Of Japan
发明人： MURAKAMI MUTSUAKI
IPC分类号： D01F9/12 , D01F9/127
摘要： PURPOSE: An aromatic dianhydride is vaporized with heat in a gas atmosphere of Ar, N
2 or H
2 or under vacuum to effect gas-phase growth to enable the production of carbon fiber of fine thickness (0.1W5μ) and uniform thickness at low temperature (300W1,000°C).
CONSTITUTION: An aromatic dianhydride or a compound forming the same by heating such as pyromellitic dianhydride and 1,4,5,8-naphthalene tetracarboxylic acid dianhydride is heated for vaporization in a gas atmosphere selected from Ar, N
2 , He, H
2 or their mixed gas or under vacuum, when needed, using Fe or Co as a catalyst to effect gas-phase growth to give the objective carbon fiber useful as a material for resist, heater or electrode and reinforcing material for composite such as FRP.
COPYRIGHT: (C)1985,JPO&Japio
摘要翻译：目的：芳香族二酐在Ar，N2或H2的气体气氛中进行加热或真空蒸发，以实现气相生长，使得能够在低温下生产细小的厚度（0.1-5μm）的碳纤维和均匀的厚度（ 300-1,000℃）。构成：通过加热形成芳香族二酐或其混合物，例如均苯四甲酸二酐和1,4,5,8-萘四羧酸二酐，在选自Ar，N 2，He，H 2的气氛气氛中进行加热，或者混合气体或真空下，当需要时，使用Fe或Co作为催化剂进行气相生长，以使目标碳纤维用作抗蚀剂，加热器或电极的材料以及用于复合材料如FRP的增强材料。

6. 发明专利

JPS6155221A Production of carbonaceous or graphitic fiber having improved electrical conductivity 失效
标题翻译：生产具有改善电导率的碳纤维或纤维纤维
公开(公告)号：JPS6155221A
公开(公告)日：1986-03-19
申请号：JP17516284
申请日：1984-08-24
申请人： Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： MURAKAMI MUTSUAKI , YOSHIMURA SUSUMU
IPC分类号： D01F9/12 , D01F9/127 , D01F9/14 , D01F11/10 , H01B1/04
摘要： PURPOSE: To obtain the titled fiber having improved electricalconductivity, by vaporizing an aromatic 2 acid anhydride, an aromatic diimide compound, etc. in a gas atmosphere of argon, etc. under heating, subjecting it to gaseous-phase growth to give carbonaceous fiber, heat-treating the carbonaceous fiber, and doping it with a dopant.
CONSTITUTION: An aromatic 2 acid anhydride (e.g., 3,4,9,10-perylenetetracarboxylic acid dianhydride, etc.), an aromatic diimide compound, or a compound to produce the aromatic 2 acid anhydride or the aromatic diimide under heating is vaporized in an atmosphere of argon, nitrogen, helium, hydrogen, or their mixed gas or in vacuum under heating, and subjected to gaseous-phase growth, to give carbonaceous fiber. Then, the carbonaceous fiber or fiber obtained by graphitizing the carbonaceous fiber by heat treatment is doped with a dopant having acceptor or donor properties, to give the aimed fiber having improved electrical conductivity.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：为了获得具有改善的导电性的标题纤维，通过在氩气气氛下在加热下蒸发芳族二酸酐，芳族二酰亚胺化合物等，使其进行气相生长，得到碳质纤维，热处理碳质纤维，并掺杂掺杂剂。构成：在加热下，芳香族二酸酐（例如3,4,9,10-苝四羧酸二酐等），芳香族二酰亚胺化合物或芳香族二酸酐或芳香族二酰亚胺的化合物在氩气，氮气，氦气，氢气或其混合气体的气氛或加热下的真空中进行气相生长，得到碳质纤维。然后，通过热处理对碳质纤维进行石墨化而获得的碳质纤维或纤维掺杂有具有受体或者给体特性的掺杂剂，得到具有改善的导电性的目标纤维。

7. 发明专利

JPS59199754A Manufacture of conductive polymer 失效
标题翻译：导电聚合物的制造
公开(公告)号：JPS59199754A
公开(公告)日：1984-11-12
申请号：JP7411283
申请日：1983-04-28
申请人： Yoshitsugu Isamoto , Mutsuaki Murakami , Res Dev Corp Of Japan , Susumu Yoshimura
发明人： ISAMOTO YOSHITSUGU , MURAKAMI MUTSUAKI , YOSHIMURA SUSUMU
IPC分类号： C08L79/08 , C08L65/00 , C08L65/02 , C08L77/00 , C08L79/04 , C08L81/00 , H01B1/12
CPC分类号： C08G2261/312
摘要： PURPOSE: To obtain a flexible conductive polymer with high thermal and chemical stability, by heat treatment, in an inert gas or a vacuum, of a heat-resistant polymer capable of forming polycyclic aromatic structure by heating, pyrolysis, and recombination, followed by chemically doping.
CONSTITUTION: A heat-resistant polymer capable of forming polycyclic aromatic structure by heating, pyrolysis, and recombination, is heat-treated, in an inert gas or a vacuum, under such a condition as to form said structure while retaining flexibility. The resulting product is subjected to chemical doping with a dopant serving as an acceptor. Said heat-resistant polymer is e.g., an aromatic polyamide, aromatic polyamideimide, being heat-treated normally at ≥200°C. Said dopant is pref. H
2 SO
4 or SO
3 gas, enabling the objective polymer to be improved in its electrical conductivity up to 10
12 order; however, I
2 , HF, FeCl
3 , etc. are also effective.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过加热，热解和再结合能形成多环芳族结构的耐热聚合物，通过在惰性气体或真空中热处理，获得具有高热稳定性和化学稳定性的柔性导电聚合物，然后化学掺杂。构成：通过加热，热解和复合形成多环芳族结构的耐热聚合物，在惰性气体或真空中，在形成所述结构同时保持柔韧性的条件下进行热处理。将所得产物用作为受体的掺杂剂进行化学掺杂。所述耐热聚合物是例如芳族聚酰胺，芳族聚酰胺酰亚胺，在≥200℃下通常进行热处理。所述掺杂剂是优选的。 H2SO4或SO3气体，使目标聚合物的电导率提高到10 12阶; 然而，I2，HF，FeCl3等也是有效的。

8. 发明专利

JPS59105029A Polymeric conductor 失效
标题翻译：聚合物导体
公开(公告)号：JPS59105029A
公开(公告)日：1984-06-18
申请号：JP21462982
申请日：1982-12-09
申请人： Yoshitsugu Isamoto , Shigeaki Mizogami , Mutsuaki Murakami , Res Dev Corp Of Japan , Hiroyuki Yasujima , Susumu Yoshimura
发明人： YOSHIMURA SUSUMU , MURAKAMI MUTSUAKI , ISAMOTO YOSHITSUGU , MIZOGAMI SHIGEAKI , YASUJIMA HIROYUKI
IPC分类号： C08G73/00 , C08G73/06 , C08G73/08 , C08G85/00 , H01B1/12
摘要： PURPOSE: A polymeric conductor excellent in heat stability and suitable for use in electronic circuits elements, sensor materials, etc., obtained by heat-treating poly(p-phenylene-1,3,4-oxadiazole) under a specified condition.
CONSTITUTION: A film, 25W50μ thick, is obtained by casting poly(p-phenylene-1, 3,4-oxadiazole) which is obtained by polycondensing terephthalic acid with hydrazine and then ring-closing the obtained polyhydrazine by dehydration. The obtained film is supported on an alumina carrier or the like and heat-treated at 520W1,400°C in vacuum or an inert gas to form a nitrogen-containing condensed polycyclic ring structure.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过在特定条件下热处理聚（对亚苯基-1,3,4-恶二唑）而获得的热稳定性优异且适用于电子电路元件，传感器材料等的聚合物导体。构成：通过将对苯二甲酸与肼缩聚而得到的聚（对亚苯基-1,3,4-恶二唑）浇铸，然后通过脱水闭环所得多肼，得到25-50μm厚的薄膜。将得到的膜负载在氧化铝载体等上，在真空或惰性气体中在520-1,400℃进行热处理，形成含氮缩合多环结构。

9. 发明授权

US08758656B2 Process for producing graphite film and graphite film produced thereby 有权
标题翻译：由此生产石墨膜和石墨膜的方法
公开(公告)号：US08758656B2
公开(公告)日：2014-06-24
申请号：US13044010
申请日：2011-03-09
申请人： Yasushi Nishikawa , Shuhei Wakahara , Mutsuaki Murakami
发明人： Yasushi Nishikawa , Shuhei Wakahara , Mutsuaki Murakami
IPC分类号： B32B37/06
CPC分类号： C01B32/20 , B32B37/1018 , B32B43/006 , B32B2313/04 , H01G11/34 , H05K9/0081 , Y02E60/13 , Y10T156/10 , Y10T428/24479 , Y10T428/24942
摘要： In order to obtain a graphite film having an excellent thermal diffusivity, a high density, and excellent flatness without flaws, recesses and wrinkles on the surface, the process for producing a graphite film according to the present invention comprises the graphitization step for a raw material film made of a polymer film and/or a carbonized polymer film and/or the post-planar pressurization step for the film in this order to prepare a graphite film, wherein the graphitization step is a step of thermally treating two or more stacked raw material films at a highest temperature of 2,000° C. and includes a method of electrically heating the raw material films themselves and/or a method of thermally treating the films while applying pressure to the films planarly, and the post-planar pressurization step includes a method of planarly pressurizing the one raw material film or the multiple stacked raw material films after graphitization by single-plate press or vacuum press.
摘要翻译：为了获得具有优异的热扩散率，高密度和优异的平面度的石墨膜，在表面上没有缺陷，凹陷和皱纹，根据本发明的石墨膜的制造方法包括用于原料的石墨化步骤由此制成石墨膜，由聚合物膜和/或碳化聚合物膜制成的薄膜和/或后平面加压步骤，其中石墨化步骤是热处理两种或更多层叠原料膜的最高温度为2000℃，并且包括对原料膜本身进行电加热的方法和/或对膜均匀加压的热处理方法，并且后平面加压步骤包括：通过单板压机或真空压机在石墨化之后对一个原料膜或多个堆叠的原料膜进行平面加压。

10. 发明授权

US08067523B2 Thermosetting resin composition, laminated body using it, and circuit board 有权
标题翻译：热固性树脂组合物，使用它的层压体和电路板
公开(公告)号：US08067523B2
公开(公告)日：2011-11-29
申请号：US11542229
申请日：2006-10-04
申请人： Shigeru Tanaka , Kanji Shimoohsako , Takashi Ito , Mutsuaki Murakami
发明人： Shigeru Tanaka , Kanji Shimoohsako , Takashi Ito , Mutsuaki Murakami
IPC分类号： C08G65/00
CPC分类号： B32B27/38 , B32B15/092 , B32B15/20 , B32B27/281 , B32B2270/00 , B32B2307/206 , B32B2307/306 , B32B2457/08 , C08G59/4042 , H05K1/0353 , H05K2201/0154
摘要： It is an object of the present invention to provide a thermosetting resin composition having satisfactory adhesiveness, good processability, high heat resistance, and excellent dielectric characteristics in the GHz band; and a laminate and a circuit board including the thermosetting resin composition.The present invention provides a thermosetting resin composition including an imide oligomer component (A) containing at least one imide oligomer having a specific structure and an epoxy resin component (B) containing at least one epoxy resin. Furthermore, the present invention provides the thermosetting resin composition further including a polyimide resin component (C).
摘要翻译：本发明的目的是提供一种在GHz频带中具有令人满意的粘合性，良好的加工性，高耐热性和优异的介电特性的热固性树脂组合物; 以及包含所述热固性树脂组合物的层压体和电路板。本发明提供一种包含含有至少一种具有特定结构的酰亚胺低聚物的酰亚胺低聚物组分（A）和含有至少一种环氧树脂的环氧树脂组分（B）的热固性树脂组合物。此外，本发明还提供还包含聚酰亚胺树脂组分（C）的热固性树脂组合物。

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