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1. 发明授权

US07989655B2 Thiol ester compositions and processes for making and using same 有权
标题翻译：硫醇酯组合物及其制备和使用方法
公开(公告)号：US07989655B2
公开(公告)日：2011-08-02
申请号：US11060675
申请日：2005-02-17
申请人： Mitchell D. Refvik , Daniel M. Hasenberg , Michael S. Hankinson , Michael S. Matson , Dale M. Solaas , Steven J. Herron , Jim D. Byers
发明人： Mitchell D. Refvik , Daniel M. Hasenberg , Michael S. Hankinson , Michael S. Matson , Dale M. Solaas , Steven J. Herron , Jim D. Byers
IPC分类号： C07C321/00 , G01N33/92
CPC分类号： C05C9/00 , C05G3/0023 , C05G3/0029 , C07C327/22 , C08G75/00 , C08G75/04 , C08G75/26 , C11C3/00 , C05G3/0035
摘要： Thiol ester compositions, methods of making the thiol ester compositions, and methods of using the thiol ester compositions are provided. In some embodiments, the thiol ester compositions include thiol esters, hydroxy thiol esters and cross-linked thiol esters. The thiol ester composition can be used to produce cross-linked thiol esters, sulfonic acid-containing esters, sulfonate containing esters and thioacrylate containing esters. The thiol ester compositions can be used to produce polythiourethanes. The polythiourethanes can be used in fertilizers and fertilizer coatings.
摘要翻译：提供硫醇酯组合物，制备硫羟酸酯组合物的方法，以及使用硫羟酸酯组合物的方法。在一些实施方案中，硫羟酸酯组合物包括硫醇酯，羟基硫羟酸酯和交联的硫羟酸酯。硫醇酯组合物可用于制备交联硫醇酯，含磺酸酯，含磺酸酯和含硫丙烯酸酯的酯。硫醇酯组合物可用于制备聚氨基甲酸乙酯。聚硫氨酯可用于肥料和肥料涂料。

2. 发明授权

US07326820B2 System and method for purifying heptane 失效
标题翻译：纯化庚烷的方法和系统
公开(公告)号：US07326820B2
公开(公告)日：2008-02-05
申请号：US10927908
申请日：2004-08-27
申请人： Daniel M. Hasenberg , Mitchell D. Refvik , Christopher Raymond Tully , Michael S. Hankinson , Clyde Stewart Denton , Dale Solaas
发明人： Daniel M. Hasenberg , Mitchell D. Refvik , Christopher Raymond Tully , Michael S. Hankinson , Clyde Stewart Denton , Dale Solaas
IPC分类号： C07C7/12 , C07C7/13 , C07C7/00 , C07C7/148 , C07C7/17
CPC分类号： C07C7/17 , C07C7/171 , C07C9/15
摘要： Removing impurities from a heptane stream by contacting the heptane stream with an acidic catalyst, wherein the contacting reduces a concentration of one or more close boiling impurities, one or more olefins, or both. The impurities are isomerized via contact with the acidic catalyst into species that possess lower octane levels or that do not possess boiling points as near to the boiling point of n-heptane, which promotes separation of the impurities via distillation. Close boiling impurities may include such compounds as cis-1,2-dimethylcyclopentane and methylcyclohexane or may be compounds having boiling points at a standard pressure of 760 Torr in the range of about 96.5 to about 100.5 degrees Celsius including such compounds as cis-1,2-dimethylcyclopentane and methylcyclohexane. The concentration of cis-1,2-dimethylcyclopentane and methylcyclohexane may be reduced by at least about 25 and 10 percent by weight, respectively. The concentration of olefins, as measured by the Bromine Index, may be reduced by at least about 25 percent by weight.
摘要翻译：通过使庚烷料流与酸性催化剂接触，从庚烷物流中除去杂质，其中接触降低了一种或多种近沸点杂质，一种或多种烯烃或两者的浓度。通过与酸性催化剂接触将杂质异构化为具有较低辛烷值或不具有接近正庚烷沸点的沸点的物质，这促进通过蒸馏分离杂质。接近沸腾的杂质可以包括诸如顺式-1,2-二甲基环戊烷和甲基环己烷的化合物，或者可以是在约96.5至约100.5摄氏度的标准压力为760托的沸点的化合物，包括顺式-1， 2-二甲基环戊烷和甲基环己烷。顺式-1,2-二甲基环戊烷和甲基环己烷的浓度可以分别降低至少约25重量％和10重量％。通过溴指数测量的烯烃浓度可以降低至少约25重量％。

3. 发明授权

US07399893B2 Process and catalyst for synthesis of mercaptans and sulfides from alcohols 有权
标题翻译：从醇合成硫醇和硫化物的方法和催化剂
公开(公告)号：US07399893B2
公开(公告)日：2008-07-15
申请号：US11302038
申请日：2005-12-13
申请人： Daniel M. Hasenberg , Mitchell D. Refvik
发明人： Daniel M. Hasenberg , Mitchell D. Refvik
IPC分类号： C07C921/00
CPC分类号： C07C319/08 , C07C319/14 , C07C321/04 , C07C321/22
摘要： A process and catalyst blend for selectively producing mercaptans and sulfides from alcohols. The alcohol is reacted with hydrogen sulfide, in the presence of a catalyst blend containing a hydrotreating catalyst and a dehydration catalyst to convert the alcohol to mercaptan or sulfide in one-pass. The alcohols can include primary and secondary alcohols. The mercaptan or sulfide having less than about 30% unreacted alcohol contained therein.
摘要翻译：用于从醇选择性地制备硫醇和硫化物的方法和催化剂共混物。在含有加氢处理催化剂和脱水催化剂的催化剂共混物存在下，使醇与硫化氢反应，将醇转化成硫醇或硫化物。醇可以包括伯醇和仲醇。其中含有少于约30％未反应的醇的硫醇或硫化物。

4. 发明授权

US07217843B2 Method of making 2-thiols 有权
标题翻译：制备2-硫醇的方法
公开(公告)号：US07217843B2
公开(公告)日：2007-05-15
申请号：US11115775
申请日：2005-04-27
申请人： Daniel M. Hasenberg , Mitchell D. Refvik
发明人： Daniel M. Hasenberg , Mitchell D. Refvik
IPC分类号： C07C319/00
CPC分类号： C07C319/04
摘要： A process for selectively making 2-thiols from alpha olefins is described. The process includes contacting a linear or branched alpha olefin having with H2S in the presence of a catalyst and recovering the 2-thiol from a product mixture. The catalyst includes a support and at least one metal selected from Group IIIA-VIIIA and the branched olefin is branched at the 3-position or higher with respect to the olefin double bond. Compositions wherein the 2-thiols are substantially free of 1-thiol and 3-thiol isomers are also described.
摘要翻译：描述了从α-烯烃选择性制备2-硫醇的方法。该方法包括在催化剂存在下使具有H 2 S的直链或支链α-烯烃接触并从产物混合物中回收2-硫醇。催化剂包括载体和选自IIIA-VIIIA族的至少一种金属，支化烯烃相对于烯烃双键在3位或更高分支。还描述了其中2-硫醇基本上不含1-硫醇和3-硫醇异构体的组合物。

5. 发明申请

US20080242894A1 Graded Catalyst Bed for Methyl Mercaptan Synthesis 有权
标题翻译：甲硫醇合成分级催化剂床
公开(公告)号：US20080242894A1
公开(公告)日：2008-10-02
申请号：US11691615
申请日：2007-03-27
申请人： Daniel M. Hasenberg , Mitchell D. Refvik
发明人： Daniel M. Hasenberg , Mitchell D. Refvik
IPC分类号： C07C319/00 , B01J23/00
CPC分类号： B01J35/0006 , B01J23/882 , B01J23/883 , B01J35/0026 , B01J2208/00805 , C07C319/08 , C07C321/04
摘要： A process and graded catalyst bed for selectively producing methyl mercaptan from methanol. The methanol is reacted with hydrogen sulfide, in the presence of a graded catalyst bed containing at least three types of nickel or cobalt molybdenum alumina catalysts to convert the methanol to methyl mercaptan in one-pass. At least one of the hydrotreating catalysts can contain aluminium phosphate. Use of the graded catalyst bed prevents the formation of a hot spot within the graded catalyst bed. The methyl mercaptan having less than about 30 wt. % unreacted methanol contained therein.
摘要翻译：一种用于从甲醇中选择性生产甲硫醇的工艺和分级催化剂床。在含有至少三种类型的镍或钴钼氧化铝催化剂的分级催化剂床的存在下，使甲醇与硫化氢反应，以一次通过将甲醇转化成甲硫醇。至少一种加氢处理催化剂可以含有磷酸铝。使用分级催化剂床防止在分级催化剂床内形成热点。甲硫醇的含量小于约30wt。％未反应的甲醇。

6. 发明授权

US07932425B2 Method of enhancing an aromatization catalyst 有权
标题翻译：增强芳构化催化剂的方法
公开(公告)号：US07932425B2
公开(公告)日：2011-04-26
申请号：US11780693
申请日：2007-07-20
申请人： Christopher D. Blessing , Scott H. Brown , Tin-Tack Peter Cheung , David J. Glova , Daniel M. Hasenberg , Dennis L. Holtermann , Gyanesh P. Khare , Daniel B. Knorr, Jr.
发明人： Christopher D. Blessing , Scott H. Brown , Tin-Tack Peter Cheung , David J. Glova , Daniel M. Hasenberg , Dennis L. Holtermann , Gyanesh P. Khare , Daniel B. Knorr, Jr.
IPC分类号： C07C2/52 , C10G35/06
CPC分类号： C10G35/095 , C10G2300/4081 , C10G2400/30
摘要： A hydrocarbon aromatization process comprising adding a nitrogenate, an oxygenate, or both to a hydrocarbon stream to produce an enhanced hydrocarbon stream, and contacting the enhanced hydrocarbon stream with an aromatization catalyst, thereby producing an aromatization reactor effluent comprising aromatic hydrocarbons, wherein the catalyst comprises a non-acidic zeolite support, a group VIII metal, and one or more halides. Also disclosed is a hydrocarbon aromatization process comprising monitoring the presence of an oxygenate, a nitrogenate, or both in an aromatization reactor, monitoring at least one process parameter that indicates the activity of the aromatization catalyst, modifying the amount of the oxygenate, the nitrogenate, or both in the aromatization reactor, thereby affecting the parameter.
摘要翻译：烃芳构化方法包括将氮化物，含氧化合物或二者加入到烃流中以产生增强的烃流，以及使增强的烃流与芳构化催化剂接触，从而产生包含芳族烃的芳构化反应器流出物，其中催化剂包含非酸性沸石载体，VIII族金属和一种或多种卤化物。还公开了一种烃芳构化方法，其包括在芳构化反应器中监测含氧物，氮酸盐或二者的存在，监测指示芳构化催化剂的活性的至少一个工艺参数，改变含氧化合物的量，或二者在芳构化反应器中，从而影响参数。

7. 发明授权

US5182330A Process for the copolymerization of 4-methyl-1-pentene 失效
标题翻译： 4-甲基-1-戊烯共聚方法
公开(公告)号：US5182330A
公开(公告)日：1993-01-26
申请号：US745021
申请日：1991-08-13
申请人： Phil M. Stricklen , Daniel M. Hasenberg , Patrick Rooney
发明人： Phil M. Stricklen , Daniel M. Hasenberg , Patrick Rooney
IPC分类号： C08F4/64 , C08F4/60 , C08F10/14 , C08F110/14 , C08F210/14 , C08F297/08
CPC分类号： C08F210/14 , C08F297/08 , C08F110/14
摘要： In the copolymerization of 4-methyl-1-pentene and at least one alpha olefin under batch polymerization conditions at a temperature of at least about 50.degree. C. wherein 4-methyl-1-pentene is initially polymerized in the absence of comonomer and then comonomer is added to the reaction vessel to permit copolymer formation, the improvement comprising initially forming 4-methyl-1-pentene homopolymer in an amount sufficient to reduce the solubility of the later formed copolymer at the polymerization temperature, said homopolymer being no more than about 5 weight percent of the end product copolymer. Also the products of such polymerizations are disclosed.

8. 发明授权

US09085736B2 System and method for on stream catalyst replacement 有权
标题翻译：在线催化剂更换的系统和方法
公开(公告)号：US09085736B2
公开(公告)日：2015-07-21
申请号：US13282066
申请日：2011-10-26
申请人： Scott G. Morrison , Tin-Tack Peter Cheung , Joe Bergmeister, III , Vincent D. McGahee , Bruce D. Murray , Daniel M. Hasenberg
发明人： Scott G. Morrison , Tin-Tack Peter Cheung , Joe Bergmeister, III , Vincent D. McGahee , Bruce D. Murray , Daniel M. Hasenberg
IPC分类号： C10G59/02 , C10G35/04
CPC分类号： C10G35/095 , B01J8/02 , B01J8/0285 , B01J2208/00548 , B01J2208/00893 , B01J2208/02 , C10G35/04 , C10G35/06 , C10G2300/701 , C10G2400/30
摘要： A process for operating a reforming reactor system comprising operating a plurality of reactors until at least one reactor is deemed to have an operational issue, wherein each of the plurality of reactors contains a catalyst capable of converting at least a portion of a hydrocarbon stream to aromatic hydrocarbons, isolating the at least one reactor deemed to have the operational issue from a remaining plurality of reactors that continue to operate to convert at least the portion of the hydrocarbon stream to aromatic hydrocarbons while the at least one reactor deemed to have the operational issue is isolated from the plurality of remaining reactors, addressing the operational issues, returning the at least one reactor to the hydrocarbon stream by connecting the reactor to the remaining plurality of reactors, and resuming operations of the reforming reactor system to convert at least the portion of the hydrocarbon stream to aromatic hydrocarbons.
摘要翻译：一种用于操作重整反应器系统的方法，包括操作多个反应器，直到至少一个反应器被认为具有操作问题，其中所述多个反应器中的每一个都包含能够将至少一部分烃流转化为芳族化合物的催化剂碳氢化合物，将被认为具有操作问题的至少一个反应器从剩余的多个反应器中分离出来，其余的多个反应器继续操作以将至少一部分烃流转化为芳烃，同时被认为具有操作问题的至少一个反应器是从多个剩余的反应器中分离出来，解决操作问题，通过将反应器连接到剩余的多个反应器将至少一个反应器返回到烃流中，并且重新开始重整反应器系统的操作以将至少一部分反应器烃流到芳烃。

9. 发明授权

US08362310B2 Method of enhancing an aromatization catalyst 有权
标题翻译：增强芳构化催化剂的方法
公开(公告)号：US08362310B2
公开(公告)日：2013-01-29
申请号：US13078524
申请日：2011-04-01
申请人： Christopher D. Blessing , Scott H. Brown , Tin-Tack Peter Cheung , David J. Glova , Daniel M. Hasenberg , Dennis L. Holtermann , Gyanesh P. Khare , Daniel B. Knorr, Jr.
发明人： Christopher D. Blessing , Scott H. Brown , Tin-Tack Peter Cheung , David J. Glova , Daniel M. Hasenberg , Dennis L. Holtermann , Gyanesh P. Khare , Daniel B. Knorr, Jr.
IPC分类号： C07C2/42 , C10G35/06
CPC分类号： C10G35/095 , C10G2300/4081 , C10G2400/30
摘要： A hydrocarbon aromatization process comprising adding a nitrogenate, an oxygenate, or both to a hydrocarbon stream to produce an enhanced hydrocarbon stream, and contacting the enhanced hydrocarbon stream with an aromatization catalyst, thereby producing an aromatization reactor effluent comprising aromatic hydrocarbons, wherein the catalyst comprises a non-acidic zeolite support, a group VIII metal, and one or more halides. Also disclosed is a hydrocarbon aromatization process comprising monitoring the presence of an oxygenate, a nitrogenate, or both in an aromatization reactor, monitoring at least one process parameter that indicates the activity of the aromatization catalyst, modifying the amount of the oxygenate, the nitrogenate, or both in the aromatization reactor, thereby affecting the parameter.
摘要翻译：烃芳构化方法包括将氮化物，含氧化合物或二者加入到烃流中以产生增强的烃流，以及使增强的烃流与芳构化催化剂接触，从而产生包含芳族烃的芳构化反应器流出物，其中催化剂包含非酸性沸石载体，VIII族金属和一种或多种卤化物。还公开了一种烃芳构化方法，其包括在芳构化反应器中监测含氧物，氮酸盐或二者的存在，监测指示芳构化催化剂的活性的至少一个工艺参数，改变含氧化合物的量，或二者在芳构化反应器中，从而影响参数。

10. 发明授权

US5034479A Process for reducing sheeting during polymerization of alpha-olefins 失效
标题翻译：在α-烯烃聚合过程中降低片材的方法
公开(公告)号：US5034479A
公开(公告)日：1991-07-23
申请号：US559699
申请日：1990-07-30
申请人： Ronald S. Eisinger , Mark G. Goode , Daniel M. Hasenberg , Kiu H. Lee
发明人： Ronald S. Eisinger , Mark G. Goode , Daniel M. Hasenberg , Kiu H. Lee
IPC分类号： B01J8/24 , C08F2/34 , C08F10/00
CPC分类号： C08F10/00 , B01J8/24 , Y10S526/901
摘要： A process for reducing sheeting during gas phase polymerization of alpha-olefins utilizing catalysts prone to cause sheeting wherein the gaseous feed stream containing monomer comonomer hydrogen and inert gas is introduced into the reactor through the recycle stream to the reactor at a point prior to cooling the recycle stream.
摘要翻译：一种利用易于引起片材的催化剂在α-烯烃的气相聚合期间降低片材的方法，其中将含有单体共聚单体氢气和惰性气体的气态进料流通过循环物流引入反应器，在冷却前循环流。

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