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    • 9. 发明申请
    • Method and device for analyzing the hardening of hardenable formulations
    • 用于分析可硬化制剂硬化的方法和装置
    • US20050000274A1
    • 2005-01-06
    • US10491423
    • 2002-09-27
    • Wolfgang SchrofThorsten MullerSebastian KoltzenburgMatthias KronerStephan LehmannJoachim Hadeler
    • Wolfgang SchrofThorsten MullerSebastian KoltzenburgMatthias KronerStephan LehmannJoachim Hadeler
    • G01N11/00G01N3/00G01N3/06G01N3/42G01N3/48
    • G01N3/42G01N2203/0092G01N2203/0682
    • The invention relates to a process for the combinatorial investigation of the hardening of hardenable liquid or viscous formulations (a) in which n hardenable formulations are prepared in parallel in n containers, and (b) the degree of hardening is determined at least once on each of the n formulations by inserting a measurement tip into the formulation with a certain force and measuring the maximum penetration depth achieved as a measure of the degree of hardening of this formulation, and (c) for in each case one composition of the formulations, one or more parameters that are characteristic of the kinetics of hardening are determined from the measurement values for the penetration depth at various times after preparation of the formulations. Steps (a) to (c) are preferably carried out a number of times, and a dependence of the characteristic parameter(s) on the composition of the formulations is determined by analysis of the large number of individual values obtained in this way for the parameter(s) that is (are) characteristic of the kinetics of hardening, enabling the composition of the formulations to be optimized with respect to its hardening behavior.
    • 本发明涉及用于组合研究可硬化液体或粘性制剂(a)的硬化的方法,其中在n个容器中并行制备n个可硬化制剂,和(b)硬化程度每个至少确定一次 通过以一定的力将测量尖端插入制剂中并测量作为该制剂的硬化程度的度量而获得的最大穿透深度,以及(c)在每种情况下,制剂的一种组合物,一种 或者从制剂配制后的不同时刻的穿透深度的测定值求出硬化动力学特征的更多的参数。 步骤(a)至(c)优选进行多次,并且通过分析以这种方式获得的大量个体值来确定特征参数对制剂组成的依赖性 硬化动力学特征的参数,使组合物能够根据其硬化行为进行优化。