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    • 2. 发明授权
    • Continuous process for the production of polyacrylonitrile filaments and
fibers
    • 连续生产聚丙烯腈长丝和纤维的方法
    • US4622195A
    • 1986-11-11
    • US586578
    • 1984-03-06
    • Michael BuebDieter PauliniEdgar MuschelknautzWolfram WagnerHerbert Groschel
    • Michael BuebDieter PauliniEdgar MuschelknautzWolfram WagnerHerbert Groschel
    • D01D5/04D01F6/18D01F6/38D02G1/12D02G1/16D02J1/00
    • D01F6/18D02G1/122
    • Polyacrylonitrile filaments and fibers may be obtained without interruption by spinning the spinning solution into a hot-air spinning duct, washing, drawing, crimping, preparing, steaming, drying cooling and, optionally, cutting at a take-off rate kept at 150 to 400 m/minute and for a tow weight of from 10 to 100 g/m when(a) the washing process is carried out in several stages on the countercurrent principle and a vibrating duct is used for transporting the spun tow through the washing process,(b) drawing is carried out before and/or after washing in a steam atmosphere at 100.degree. to 120.degree. C.,(c) crimping is carried out in an aerodynamic crimping unit using a hot, gaseous medium under a pressure of from 5 to 16 bars and at a temperature in the range from 50.degree. to 210.degree. C.,(d) the preparation is continuously applied to the tow before, during or after crimping,(e) for steaming, the tow is transported through a steaming apparatus in folded form and in the absence of tension on a vibrating duct and, at the same time, treated with steam at 100.degree. to 120.degree. C.,(f) finally, the tow is dried in folded form on a belt dryer using hot air at 60.degree. to 180.degree. C., subsequently cooled with cold air to temperatures below 50.degree. C. and, optionally, delivered to a cutting machine.
    • 可以通过将纺丝溶液旋转成热风纺丝管,洗涤,拉伸,卷曲,制备,蒸煮,干燥冷却和任选地以保持在150至400的起飞速率进行切割而获得聚丙烯腈长丝和纤维 (a)按照逆流原理在数个阶段进行洗涤过程,并且使用振动管道通过洗涤过程输送纺丝丝束(m / min,丝束重量为10-100g / m 2) b)在100-120℃的蒸汽气氛中洗涤之前和/或之后进行拉伸,(c)在空气动力学压接单元中使用热气体介质在5〜 16巴,温度范围为50至210℃,(d)在卷曲之前,期间或之后将制品连续施加到丝束上,(e)蒸汽时,丝束通过蒸汽装置 以折叠的形式和在没有紧张的情况下 振动管道,同时用100-120℃的蒸汽处理,(f)最后,使用60℃至180℃的热空气将丝束以折叠形式在带式干燥机上干燥,随后 用冷空气冷却到低于50℃的温度,并且任选地被输送到切割机。