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1. 发明申请

US20080306316A1 Process for Reacting an Aromatic Hydrocarbon in the Presence of Hydrogen 审中-公开
标题翻译：在氢存在下反应芳烃的方法
公开(公告)号：US20080306316A1
公开(公告)日：2008-12-11
申请号：US12158730
申请日：2006-12-22
申请人： Michael Becker , Axel Salden , Bianca Stack , Jochem Henkelmann , Steffen Springmann , Frederik van Laar , Wilhelm Ruppel , Peter Resch , Michael Bender
发明人： Michael Becker , Axel Salden , Bianca Stack , Jochem Henkelmann , Steffen Springmann , Frederik van Laar , Wilhelm Ruppel , Peter Resch , Michael Bender
IPC分类号： C07C5/10
CPC分类号： C07C13/18 , C07C5/10 , C07C7/1485 , C07C2521/04 , C07C2521/08 , C07C2523/46 , C10G65/08 , C10G67/02 , C10G2300/1096 , C10G2300/202 , Y02P20/125
摘要： Processes comprising: providing a starting material comprising one or more aromatic hydrocarbons, and having an aromatic sulfur compound content and a total sulfur content; reducing the aromatic sulfur compound content and the total sulfur content in the starting material; and hydrogenating the one or more aromatic hydrocarbons in the presence of a supported ruthenium catalyst and hydrogen.
摘要翻译：方法包括：提供包含一种或多种芳族烃并具有芳族硫化合物含量和总硫含量的原料; 降低原料中芳香族硫化合物含量和总硫含量; 在负载的钌催化剂和氢气的存在下氢化一种或多种芳族烃。

2. 发明申请

US20110196181A1 PROCESS FOR REACTING AN AROMATIC HYDROCARBON IN THE PRESENCE OF HYDROGEN 审中-公开
标题翻译：在氢存在下反应芳烃的方法
公开(公告)号：US20110196181A1
公开(公告)日：2011-08-11
申请号：US13088627
申请日：2011-04-18
申请人： Michael Becker , Axel Salden , Bianca Stäck , Jochem Henkelmann , Steffen Springmann , Frederik van Laar , Wilhelm Ruppel , Peter Resch , Michael Bender
发明人： Michael Becker , Axel Salden , Bianca Stäck , Jochem Henkelmann , Steffen Springmann , Frederik van Laar , Wilhelm Ruppel , Peter Resch , Michael Bender
IPC分类号： C07C5/10 , C07C1/32
CPC分类号： C07C13/18 , C07C5/10 , C07C7/1485 , C07C2521/04 , C07C2521/08 , C07C2523/46 , C10G65/08 , C10G67/02 , C10G2300/1096 , C10G2300/202 , Y02P20/125
摘要： Processes comprising: providing a starting material comprising one or more aromatic hydrocarbons, and having an aromatic sulfur compound content and a total sulfur content; reducing the aromatic sulfur compound content and the total sulfur content in the starting material; and hydrogenating the one or more aromatic hydrocarbons in the presence of a supported ruthenium catalyst and hydrogen.
摘要翻译：方法包括：提供包含一种或多种芳族烃并具有芳族硫化合物含量和总硫含量的原料; 降低原料中芳香族硫化合物含量和总硫含量; 在负载的钌催化剂和氢气的存在下氢化一种或多种芳族烃。

3. 发明授权

US08889936B2 Method of regenerating ruthenium catalysts for the hydrogenation of benzene 有权
标题翻译：再生用于氢化苯的钌催化剂的方法
公开(公告)号：US08889936B2
公开(公告)日：2014-11-18
申请号：US12375759
申请日：2007-07-27
申请人： Jochem Henkelmann , Michael Becker , Michael Schönherr , Wilhelm Ruppel , Ulrike Wegerle , Bianca Stäck
发明人： Jochem Henkelmann , Michael Becker , Michael Schönherr , Wilhelm Ruppel , Ulrike Wegerle , Bianca Stäck
IPC分类号： C07C5/10 , B01J23/46 , B01J23/96 , B01J38/04 , B01J23/75 , B01J23/40 , B01J23/755
CPC分类号： B01J38/04 , B01J23/40 , B01J23/462 , B01J23/75 , B01J23/755 , B01J23/96 , C07C5/10 , C07C2523/46 , Y02P20/584 , Y10S585/906 , C07C13/18
摘要： The present patent application describes a method of regenerating a ruthenium catalyst for the hydrogenation of benzene, which comprises flushing the catalyst with inert gas in a regeneration step until the original activity or part of the original activity has been attained.
摘要翻译：本专利申请描述了一种再生用于苯氢化的钌催化剂的方法，其包括在再生步骤中用惰性气体冲洗催化剂直到达到原始活性或部分原始活性。

4. 发明申请

US20090259083A1 METHOD OF REGENERATING RUTHENIUM CATALYSTS FOR THE HYDROGENATION OF BENZENE 有权
标题翻译：再生苯乙烯氢化催化剂的方法
公开(公告)号：US20090259083A1
公开(公告)日：2009-10-15
申请号：US12375759
申请日：2007-07-27
申请人： Jochem Henkelmann , Michael Becker , Michael Schönherr , Wilhelm Ruppel , Ulrike Wegerle , Bianca Stäck
发明人： Jochem Henkelmann , Michael Becker , Michael Schönherr , Wilhelm Ruppel , Ulrike Wegerle , Bianca Stäck
IPC分类号： C07C5/10
CPC分类号： B01J38/04 , B01J23/40 , B01J23/462 , B01J23/75 , B01J23/755 , B01J23/96 , C07C5/10 , C07C2523/46 , Y02P20/584 , Y10S585/906 , C07C13/18
摘要： The present patent application describes a method of regenerating a ruthenium catalyst for the hydrogenation of benzene, which comprises flushing the catalyst with inert gas in a regeneration step until the original activity or part of the original activity has been attained.
摘要翻译：本专利申请描述了一种再生用于苯氢化的钌催化剂的方法，其包括在再生步骤中用惰性气体冲洗催化剂直到达到原始活性或部分原始活性。

5. 发明申请

US20060183627A1 Method for regenerating re2o7 doped catalyst supports 审中-公开
标题翻译：再生Re2o7掺杂催化剂载体的方法
公开(公告)号：US20060183627A1
公开(公告)日：2006-08-17
申请号：US10547293
申请日：2004-02-16
申请人： Jurgen Stephan , Markus Schubert , Christian Weichert , Wilhelm Ruppel , Peter Resch , Soeren Zimdahl , Frank Mrzena , Andreas Molitor , Stefan Berg , Mathias Fohrmann
发明人： Jurgen Stephan , Markus Schubert , Christian Weichert , Wilhelm Ruppel , Peter Resch , Soeren Zimdahl , Frank Mrzena , Andreas Molitor , Stefan Berg , Mathias Fohrmann
IPC分类号： B01J38/12
CPC分类号： B01J23/92 , B01J23/36 , B01J38/12 , B01J38/14 , C07C6/04 , Y02P20/584
摘要： Method of regenerating an Re2O7-doped supported catalyst which has been deactivated by use in the metathesis of a hydrocarbon mixture comprising C2-C6-olefins (C2-6= feed) (deactivated catalyst), which comprises treating the deactivated catalyst with an inert gas (regeneration gas K1) at from 400 to 800° C. and subsequently treating the deactivated catalyst which has been pretreated with regeneration gas K1 with an oxygen-containing gas (regeneration gas K2).
摘要翻译：通过在包含C 2 -C 6烷基的烃混合物的复分解中使用已经失活的Re 2 O 2 O 7重掺合载体催化剂的再生方法， C 6 - 6 - 烯烃（C 2-6）进料）（失活催化剂），其包括用惰性气体处理失活的催化剂（再生气体K 1），然后用含氧气体（再生气体K 2）处理已经用再生气体K 1预处理的失活催化剂。

6. 发明授权

US09174192B2 Tube bundle reactor for uncatalyzed or homogeneously catalyzed reactions 有权
标题翻译：用于未催化或均匀催化反应的管束反应器
公开(公告)号：US09174192B2
公开(公告)日：2015-11-03
申请号：US13380207
申请日：2010-01-19
申请人： Joaquim Henrique Teles , Peter Resch , Wilhelm Ruppel , Ulrike Wegerle , Wolfgang Gerlinger , Beatrice Röβler-Feigel , Anton Meier , Christian Müller
发明人： Joaquim Henrique Teles , Peter Resch , Wilhelm Ruppel , Ulrike Wegerle , Wolfgang Gerlinger , Beatrice Röβler-Feigel , Anton Meier , Christian Müller
IPC分类号： B01J19/24 , B01J19/00 , B01J4/00 , F28D7/16 , F28F9/02
CPC分类号： B01J19/2425 , B01J4/001 , B01J19/006 , B01J2219/00085 , B01J2219/00166 , F28D7/16 , F28F9/0265 , F28F9/0275 , F28F9/0278 , Y02P20/582
摘要： The invention relates to a tube bundle reactor with a flat feed hood. Alternatively, the release hood may also have a flat design. The flat design reduces the heat of reaction which arises in the hood in the case of reaction types which take place not only in the tube bundle (uncatalyzed reactions and reactions with homogeneously distributed catalyst). This greatly suppresses undesired reactions which already take place in the hood owing to accumulated heat, which achieves a higher selectivity in the case of thermally sensitive reactions. In addition, the thermal distribution within the hoods can be controlled precisely.The tube bundle reactor comprises a tube bundle which has a feed end which is connected to a feed hood of the tube bundle reactor, wherein the feed hood is configured in a flat design with a cross-sectional area at the feed end and an internal volume, and the ratio of internal volume to cross-sectional area is less than 0.35 m. The invention is further implemented by means of a process for operating a tube bundle reactor, comprising: introducing a reactant mixture into a tube bundle and converting at least a proportion of the reactant mixture within the tube bundle to a product. The introducing comprises: feeding the reactant mixture into an interior of a feed hood of the tube bundle reactor and passing the reactant mixture on into a feed end of the tube bundle in the form of a fluid stream. The fluid stream has a cross-sectional area on entry into the feed end, and the interior of the feed hood through which the fluid stream flows has an internal volume; where the ratio of internal volume to cross-sectional area is less than 0.35 m.
摘要翻译：本发明涉及具有扁平进料罩的管束反应器。或者，释放罩也可以具有平坦的设计。在反应类型不仅在管束（未催化的反应和具有均匀分布的催化剂的反应）的情况下，扁平设计减少了发动机罩中产生的反应热。这大大地抑制了由于积热而在罩中发生的不期望的反应，这在热敏反应的情况下实现了更高的选择性。此外，可以精确地控制罩内的热分布。管束反应器包括管束，其具有连接到管束反应器的进料罩的进料端，其中进料罩构造成平坦设计，在进料端具有横截面积，内部体积，内部体积与横截面积的比值小于0.35μm。通过用于操作管束反应器的方法进一步实现本发明，其包括：将反应物混合物引入管束并将至少一部分管束内的反应物混合物转化成产物。引入包括：将反应物混合物进料到管束反应器的进料罩的内部，并将反应物混合物以流体流的形式送入管束的进料端。流体流在进入进料端时具有横截面面积，流体流流过的进料罩的内部具有内部容积; 其中内部体积与横截面积的比值小于0.35μm。

7. 发明授权

US08461392B2 Process for preparing cyclic ketones 有权
标题翻译：制备环酮的方法
公开(公告)号：US08461392B2
公开(公告)日：2013-06-11
申请号：US13060545
申请日：2009-08-26
申请人： Joaquim Henrique Teles , Wilhelm Ruppel , Ulrike Wegerle , Anton Meier , Thomas Genger , Michael Schelper , Peter Resch
发明人： Joaquim Henrique Teles , Wilhelm Ruppel , Ulrike Wegerle , Anton Meier , Thomas Genger , Michael Schelper , Peter Resch
IPC分类号： C07C45/78
CPC分类号： C07C45/28 , C07C45/82 , C07C2601/08 , Y02P20/582 , C07C49/403 , C07C49/395 , C07C49/413
摘要： The present invention relates to a process for preparing at least one monocyclic ketone having from 4 to 20 carbon atoms by reacting a mixture G1 comprising at least one monocyclic olefin having from 4 to 20 carbon atoms with a mixture G2 comprising at least dinitrogen monoxide, wherein said reaction is performed adiabatically.
摘要翻译：本发明涉及一种制备至少一种具有4-20个碳原子的单环酮的方法，该方法是使包含至少一种具有4-20个碳原子的单环烯烃的混合物G1与至少包含一氧化二氮的混合物G2反应，其中所述反应是绝热的。

8. 发明申请

US20110152576A1 PROCESS FOR PREPARING CYCLIC KETONES 有权
标题翻译：制备循环克氏酮的方法
公开(公告)号：US20110152576A1
公开(公告)日：2011-06-23
申请号：US13060545
申请日：2009-08-26
申请人： Joaquim Henrique Teles , Wilhelm Ruppel , Ulrike Wegerle , Anton Meier , Thomas Genger , Michael Schelper , Peter Resch
发明人： Joaquim Henrique Teles , Wilhelm Ruppel , Ulrike Wegerle , Anton Meier , Thomas Genger , Michael Schelper , Peter Resch
IPC分类号： C07C45/28 , C07C45/78
CPC分类号： C07C45/28 , C07C45/82 , C07C2601/08 , Y02P20/582 , C07C49/403 , C07C49/395 , C07C49/413
摘要： The present invention relates to a process for preparing at least one monocyclic ketone having from 4 to 20 carbon atoms by reacting a mixture G1 comprising at least one monocyclic olefin having from 4 to 20 carbon atoms with a mixture G2 comprising at least dinitrogen monoxide, wherein said reaction is performed adiabatically.
摘要翻译：本发明涉及一种制备至少一种具有4-20个碳原子的单环酮的方法，该方法是使包含至少一种具有4-20个碳原子的单环烯烃的混合物G1与至少包含一氧化二氮的混合物G2反应，其中所述反应是绝热的。

9. 发明授权

US06479680B1 Method for reacting an organic compound with a hydroperoxide 有权
标题翻译：使有机化合物与氢过氧化物反应的方法
公开(公告)号：US06479680B1
公开(公告)日：2002-11-12
申请号：US09762290
申请日：2001-02-07
申请人： Peter Bassler , Wolfgang Harder , Peter Resch , Norbert Rieber , Wilhelm Ruppel , Joaquim Henrique Teles , Andreas Walch , Anne Wenzel , Peter Zehner
发明人： Peter Bassler , Wolfgang Harder , Peter Resch , Norbert Rieber , Wilhelm Ruppel , Joaquim Henrique Teles , Andreas Walch , Anne Wenzel , Peter Zehner
IPC分类号： C07D30112
CPC分类号： C07D301/12 , C07B33/00
摘要： A process for the reaction of an organic compound with a hydroperoxide comprises at least the steps (i) to (iii) below: (i) reaction of the hydroperoxide with the organic compound to give a mixture comprising the reacted organic compound and unreacted hydroperoxide, (ii) separation of the unreacted hydroperoxide from the mixture resulting from step (i), (iii) reaction of the hydroperoxide separated off in step (ii) with the organic compound.
摘要翻译：有机化合物与氢过氧化物反应的方法至少包括以下步骤（i）至（iii）：（i）氢过氧化物与有机化合物的反应，得到包含反应的有机化合物和未反应的氢过氧化物的混合物，（ii）从步骤（i），（iii）中得到的混合物中分离未反应的氢过氧化物，（iii）步骤（ii）中分离出的氢过氧化物与有机化合物的反应。

10. 发明授权

US6133482A Method for producing carbonyl compounds 失效
标题翻译：生产羰基化合物的方法
公开(公告)号：US6133482A
公开(公告)日：2000-10-17
申请号：US331063
申请日：1999-06-16
申请人： Thomas Fetzer , Dirk Demuth , Heinz Rutter , Helmuth Menig , Peter Resch , Wilhelm Ruppel , Harro Wache
发明人： Thomas Fetzer , Dirk Demuth , Heinz Rutter , Helmuth Menig , Peter Resch , Wilhelm Ruppel , Harro Wache
IPC分类号： B01J23/72 , C07C45/38 , C07C45/39 , C07C47/127 , C07C45/29
CPC分类号： C07C45/39 , C07C45/38
摘要： In a process for preparing carbonyl compounds of the formula ##STR1## where R.sup.1 is a hydrogen atom or an alkyl radical having from 1 to 3 carbon atoms, R.sup.2 is a hydrogen atom or a radical of the formula ##STR2## where R.sup.3 is a hydrogen atom or together with R.sup.4 is an oxygen atom, R.sup.4 is the radical OR.sup.6 or together with R.sup.3 is an oxygen atom, R.sup.5 is a hydrogen atom, an alkyl radical having from 1 to 8 carbon atoms or a cyclohexyl or cyclopentyl radical and R.sup.6 is an alkyl radical having from 1 to 4 carbon atoms, a cyclohexyl or cyclopentyl radical or a radical of the formula --CH.sub.2 --CHO or --CH.sub.2 --CH.sub.2 --O--CH.sub.2 --CHO, by gas-phase oxidation of methanol or alcohols of the formula ##STR3## where R.sup.1 and R.sup.5 are as defined above and R.sup.7 is a hydrogen atom or a radical OR.sup.8 and R.sup.8 is a hydrogen atom, an alkyl radical having from 1 to 4 carbon atoms, a cyclohexyl or cyclopentyl radical or a radical for the formula --CH.sub.2 --CH.sub.2 --OH or --CH.sub.2 --CH.sub.2 --O--CH.sub.2 --CH.sub.2 --OH, using an oxygen-containing gas in the presence of copper- and/or silver-containing catalysts and an amount of a phosphorus compound which is volatile under the reaction conditions which is such that the amount of phosphorus (calculated as P) is up to 20 ppm, based on the weight of alcohol used, the phosphorus is introduced within the catalyst bed.
摘要翻译： PCT No.PCT / EP97 / 06856 Sec。 371日期1999年6月16日第 102（e）日期1999年6月16日PCT 1997年12月23日PCT公布。公开号WO98 / 28251 日期1998年7月2日在制备下式的羰基化合物的方法中，其中R 1是氢原子或具有1至3个碳原子的烷基，R 2是氢原子或下式的基团，其中R 3是氢原子或与R4一起为氧原子，R4为基团OR6或与R3为氧原子一起，R5为氢原子，具有1至8个碳原子的烷基或环己基或环戊基，R6为烷基具有1至4个碳原子的基团，环己基或环戊基或式-CH2-CHO或-CH2-CH2-O-CH2-CHO的基团，通过下式的甲醇或醇的气相氧化其中R1 R 5为氢原子或OR 8，R 8为氢原子，碳原子数为1〜4的烷基，环己基或环戊基或式-CH 2 -CH 2 - 的基团， OH或-CH 2 -CH 2 -O-CH 2 -CH 2 -OH，使用含铜气体在铜和/或银-co 在催化剂和一定量的磷化合物中，在反应条件下挥发的量为磷（根据P计算）高达20ppm，基于所使用的醇的重量，磷被引入催化剂床。

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