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1. 发明授权

US08153052B2 High-temperature composite articles and associated methods of manufacture 有权
标题翻译：高温复合制品及相关制造方法
公开(公告)号：US08153052B2
公开(公告)日：2012-04-10
申请号：US10671851
申请日：2003-09-26
申请人： Melvin Robert Jackson , Bernard Patrick Bewlay , Judson Sloan Marte , Pazhayannur Ramanathan Subramanian , Ji-Cheng Zhao , Ann Melinda Ritter
发明人： Melvin Robert Jackson , Bernard Patrick Bewlay , Judson Sloan Marte , Pazhayannur Ramanathan Subramanian , Ji-Cheng Zhao , Ann Melinda Ritter
IPC分类号： B22F1/02
CPC分类号： C22C27/02 , B22F3/23 , C22C1/058 , C22C29/18 , C22C32/0078
摘要： The present invention provides a method for forming a refractory metal-intermetallic composite. The method includes providing a first powder comprising a refractory metal suitable for forming a metal phase; providing a second powder comprising a silicide precursor suitable for forming an intermetallic phase; blending the first powder and the second powder to form a powder blend; consolidating and mechanically deforming the powder blend at a first temperature; and reacting the powder blend at a second temperature to form the metal phase and the intermetallic phase of the refractory metal-intermetallic composite, wherein the second temperature is higher than the first temperature.
摘要翻译：本发明提供了形成难熔金属 - 金属间复合材料的方法。该方法包括提供包含适于形成金属相的难熔金属的第一粉末; 提供包含适于形成金属间相的硅化物前体的第二粉末; 混合第一粉末和第二粉末以形成粉末混合物; 在第一温度下固化和机械地使粉末混合物变形; 和在第二温度下使粉末混合物反应以形成难熔金属 - 金属间化合物的金属相和金属间相，其中第二温度高于第一温度。

2. 发明授权

US5743322A Method for forming an article extension by casting using a ceramic mold 失效
标题翻译：使用陶瓷模具通过铸造形成制品延伸的方法
公开(公告)号：US5743322A
公开(公告)日：1998-04-28
申请号：US672160
申请日：1996-06-27
申请人： Melvin Robert Jackson , Bernard Patrick Bewlay , Ann Melinda Ritter
发明人： Melvin Robert Jackson , Bernard Patrick Bewlay , Ann Melinda Ritter
IPC分类号： B22D19/00 , B22C9/22 , B22D19/10 , B22D27/04 , C30B11/00
CPC分类号： B22D27/045 , B22D19/10 , C30B11/00 , C30B29/52 , Y10T29/49318
摘要： An extension is formed directly on an article by casting a compatible material into a ceramic mold that is attached on an end of the article, followed by cooling of the end under controlled conditions sufficient to cause an integral extension to solidify on the article. A ceramic mold is utilized over the end of the article, with a mold cavity that generally defines the shape of the extension to be formed. The mold may be formed in situ on the mandrel, or preformed and attached to the subject article over the mandrel. Extensions formed by the method of this invention have a microstructure that is continuous and compatible with that of the article. Such microstructures may include epitaxial growth of the extension from the microstructure of the article. The method establishes a temperature gradient within the article during solidification that may be further controlled by auxiliary heating and/or cooling of the article and/or extension during the practice of the method.
摘要翻译：通过将相容的材料浇铸到附着在制品末端上的陶瓷模具中，直接在制品上形成延伸部分，然后在足以使制品上产生整体延伸的固化条件的受控条件下进行冷却。在制品的端部使用陶瓷模具，其中模腔通常限定待形成的延伸部的形状。模具可以在心轴上原位形成，或者通过心轴预成型并附着到主体制品上。通过本发明的方法形成的延伸部具有与制品的连续且兼容的微结构。这种微结构可以包括从制品的微观结构延伸的外延生长。该方法在固化期间在制品内建立温度梯度，其可以在该方法的实践期间通过辅助加热和/或冷却制品和/或延伸来进一步控制。

3. 发明授权

US5676191A Solidification of an article extension from a melt using an integral mandrel and ceramic mold 失效
标题翻译：使用一体式心轴和陶瓷模具从熔体固化制品延伸
公开(公告)号：US5676191A
公开(公告)日：1997-10-14
申请号：US669793
申请日：1996-06-27
申请人： Bernard Patrick Bewlay , Melvin Robert Jackson , Ann Melinda Ritter , Wayne Alan Demo , Stephen Joseph Ferrigno
发明人： Bernard Patrick Bewlay , Melvin Robert Jackson , Ann Melinda Ritter , Wayne Alan Demo , Stephen Joseph Ferrigno
IPC分类号： F01D5/18 , B22D19/00 , B22D19/10 , B22D27/04 , F01D5/28 , B22D23/06
CPC分类号： B22D19/10 , C30B11/00 , C30B29/52 , Y10T29/49318
摘要： An extension is formed directly on an article by dipping a portion or end of the article having an attached integral mandrel into a molten bath of a compatible alloy, followed by withdrawal of the end under controlled conditions sufficient to cause an integral extension to solidify on the article. A ceramic mold is utilized over the dipped end of the article and the integral mandrel with a mold cavity that generally defines the shape of the extension to be formed. The mold may be formed in situ on the mandrel, or preformed and attached to the subject article over the mandrel. The integral mandrel is melted within the mold by dipping the mandrel into the molten alloy. The mandrel acts as a buffer between the molten material and the article while permitting melting of the article end and solidification of the integral extension. Extensions formed by the method of this invention have a microstructure that is continuous and compatible with that of the article. Such microstructures may include epitaxial growth of the extension from the microstructure of the article. The method establishes a temperature gradient within the article during solidification that may be further controlled by auxiliary heating and/or cooling of the article and/or extension during the practice of the method.
摘要翻译：通过将具有附接的整体心轴的制品的一部分或端部浸入相容合金的熔池中，直接在制品上形成延伸部，然后在足以引起整体延伸固化的受控条件下将端部取出文章。陶瓷模具被利用在制品的浸入端上，并且整体心轴具有通常限定待形成的延伸部的形状的模腔。模具可以在心轴上原位形成，或者通过心轴预成型并附着到主体制品上。通过将心轴浸入熔融合金中，整体心轴在模具内熔化。心轴作为熔融材料和制品之间的缓冲液，同时允许制品端部熔化并且整体延伸部分的固化。通过本发明的方法形成的延伸部具有与制品的连续且兼容的微结构。这种微结构可以包括从制品的微观结构延伸的外延生长。该方法在固化期间在制品内建立温度梯度，其可以在该方法的实践期间通过辅助加热和/或冷却制品和/或延伸来进一步控制。

4. 发明授权

US5673745A Method for forming an article extension by melting of an alloy preform in a ceramic mold 失效
标题翻译：通过在陶瓷模具中熔化合金预制件来形成制品延伸的方法
公开(公告)号：US5673745A
公开(公告)日：1997-10-07
申请号：US672156
申请日：1996-06-27
申请人： Melvin Robert Jackson , Bernard Patrick Bewlay , Ann Melinda Ritter
发明人： Melvin Robert Jackson , Bernard Patrick Bewlay , Ann Melinda Ritter
IPC分类号： F01D5/18 , B22D19/00 , B22D19/10 , B22D23/06 , B22D27/04 , C30B11/00 , F01D5/28
CPC分类号： B22D23/06 , B22D19/10 , B23P6/007 , C30B11/00 , C30B29/52 , Y10T29/49318
摘要： An extension is formed directly on an article by melting a compatible alloy preform within a ceramic mold, followed by cooling of the end under controlled conditions sufficient to cause an integral extension to solidify on the article. A ceramic mold is attached on the end of the article with a mold cavity that generally defines the shape of the extension to be formed. The mold may be formed in situ on a removable mandrel, or preformed and attached to the subject article. Extensions formed by the method of this invention have a microstructure that is continuous and compatible with that of the article. Such microstructures may include epitaxial growth of the extension from the microstructure of the article. The method establishes a temperature gradient within the article during solidification that may be further controlled by auxiliary heating and/or cooling of the article and/or extension during the practice of the method.
摘要翻译：通过在陶瓷模具内熔化相容的合金预成型件，然后在足以使整体延伸固化在制品上的受控条件下冷却端部，直接在制品上形成延伸部。陶瓷模具附着在具有通常限定待形成的延伸部的形状的模腔的物品端部上。模具可以在可移除的心轴上原位形成，或者预成型并附着到主体制品上。通过本发明的方法形成的延伸部具有与制品的连续且兼容的微结构。这种微结构可以包括从制品的微观结构延伸的外延生长。该方法在固化期间在制品内建立温度梯度，其可以在该方法的实践期间通过辅助加热和/或冷却制品和/或延伸来进一步控制。

5. 发明授权

US5673744A Method for forming an article extension by melting of a mandrel in a ceramic mold 失效
标题翻译：通过在陶瓷模具中熔化心轴来形成制品延伸的方法
公开(公告)号：US5673744A
公开(公告)日：1997-10-07
申请号：US672154
申请日：1996-06-27
申请人： Bernard Patrick Bewlay , Melvin Robert Jackson , Ann Melinda Ritter
发明人： Bernard Patrick Bewlay , Melvin Robert Jackson , Ann Melinda Ritter
IPC分类号： F01D5/18 , B22D19/00 , B22D19/10 , B22D23/06 , B22D27/04 , C30B11/00 , F01D5/28
CPC分类号： B22D23/06 , B22D19/10 , B23P6/007 , C30B11/00 , C30B29/52 , Y10T29/49318
摘要： An extension is formed directly on an article by melting a portion or end of the article having an attached integral mandrel within a ceramic mold, followed by cooling of the end under controlled conditions sufficient to cause an integral extension to solidify on the article. A ceramic mold is attached on the end of the article over the integral mandrel with a mold cavity that generally defines the shape of the extension to be formed. The mold may be formed in situ on the mandrel, or preformed and attached to the subject article over the mandrel. Extensions formed by the method of this invention have a microstructure that is continuous and compatible with that of the article. Such microstructures may include epitaxial growth of the extension from the microstructure of the article. The method establishes a temperature gradient within the article during solidification that may be further controlled by auxiliary heating and/or cooling of the article and/or extension during the practice of the method.
摘要翻译：通过在陶瓷模具内熔化具有附接的整体心轴的制品的一部分或端部，然后在足以使制品上一体化延伸固化的受控条件下将端部冷却，直接在制品上形成延伸部。陶瓷模具通过一体式心轴连接在制品的端部上，模具腔通常限定待形成的延伸部的形状。模具可以在心轴上原位形成，或者通过心轴预成型并附着到主体制品上。通过本发明的方法形成的延伸部具有与制品的连续且兼容的微结构。这种微结构可以包括从制品的微观结构延伸的外延生长。该方法在固化期间在制品内建立温度梯度，其可以在该方法的实践期间通过辅助加热和/或冷却制品和/或延伸来进一步控制。

6. 发明授权

US06644917B2 Smart coating system with chemical taggants for coating condition assessment 有权
标题翻译：具有化学标签的智能涂层系统用于涂层状况评估
公开(公告)号：US06644917B2
公开(公告)日：2003-11-11
申请号：US09682282
申请日：2001-08-14
申请人： Ji-Cheng Zhao , James Anthony Ruud , John Eric Tkaczyk , Ann Melinda Ritter , Melvin Robert Jackson , Jerome Johnson Tiemann
发明人： Ji-Cheng Zhao , James Anthony Ruud , John Eric Tkaczyk , Ann Melinda Ritter , Melvin Robert Jackson , Jerome Johnson Tiemann
IPC分类号： F01D2100
CPC分类号： F02C9/00 , C23C30/00 , F05D2260/80 , Y02T50/67
摘要： A on-line method is provided for detecting wear and/or damage to gas turbine parts. Preferred embodiments of the invention provide a gas turbine comprising parts with smart coatings and collection and detection means to measure wear and erosion of gas turbine parts. In other preferred embodiments, smart coatings are provided comprising chemical taggants that can be collected and detected downstream, thus providing an on-line or in situ evaluation technology for wear and damage to gas turbine parts.
摘要翻译：提供在线方法来检测燃气轮机部件的磨损和/或损坏。本发明的优选实施例提供一种燃气轮机，其包括具有智能涂层的部件和用于测量燃气轮机部件的磨损和侵蚀的收集和检测装置。在其它优选实施例中，提供智能涂层，其包括可以在下游收集和检测的化学标签，从而为燃气轮机部件的磨损和损坏提供在线或原位评估技术。

7. 发明授权

US07654734B2 Methods and devices for evaluating the thermal exposure of a metal article 失效
标题翻译：用于评估金属制品的热暴露的方法和装置
公开(公告)号：US07654734B2
公开(公告)日：2010-02-02
申请号：US11126793
申请日：2005-05-10
申请人： Liang Jiang , Lawrence Bernard Kool , Melvin Robert Jackson , Canan Uslu Hardwicke , Ji-Cheng Zhao , Ann Melinda Ritter , Ching-Pang Lee
发明人： Liang Jiang , Lawrence Bernard Kool , Melvin Robert Jackson , Canan Uslu Hardwicke , Ji-Cheng Zhao , Ann Melinda Ritter , Ching-Pang Lee
IPC分类号： G01N25/72 , G01N17/00 , G01K3/00
CPC分类号： G01N17/00 , G01K7/02
摘要： A method for evaluating the thermal exposure of a selected metal component which has been exposed to changing temperature conditions is described. The voltage distribution on a surface of the metal component, or on a metallic layer which lies over the component, is first obtained. The voltage distribution usually results from a compositional change in the metal component. The voltage distribution is then compared to a thermal exposure-voltage model which expresses voltage distribution as a function of exposure time and exposure temperature for a reference standard corresponding to the metal component. In this manner, the thermal exposure of the selected component can be obtained. A related device for evaluating the thermal exposure of a selected metal component is also described.
摘要翻译：描述了已经暴露于变化的温度条件下的所选金属组分的热暴露评估方法。首先获得金属部件的表面上或位于部件上的金属层上的电压分布。电压分布通常由金属组分的组成变化引起。然后将电压分布与表示与对应于金属组分的参考标准的曝光时间和曝光温度的函数的电压分布的热暴露电压模型进行比较。以这种方式，可以获得所选择的部件的热曝光。还描述了用于评估所选金属组分的热暴露的相关装置。

8. 发明申请

US20060256833A1 Methods and devices for evaluating the thermal exposure of a metal article 失效
标题翻译：用于评估金属制品的热暴露的方法和装置
公开(公告)号：US20060256833A1
公开(公告)日：2006-11-16
申请号：US11126793
申请日：2005-05-10
申请人： Liang Jiang , Lawrence Bernard Kool , Melvin Robert Jackson , Canan Uslu Hardwicke , Ji-Cheng Zhao , Ann Melinda Ritter , Ching-Pang Lee
发明人： Liang Jiang , Lawrence Bernard Kool , Melvin Robert Jackson , Canan Uslu Hardwicke , Ji-Cheng Zhao , Ann Melinda Ritter , Ching-Pang Lee
IPC分类号： G01N17/00 , G01K3/00
CPC分类号： G01N17/00 , G01K7/02
摘要： A method for evaluating the thermal exposure of a selected metal component which has been exposed to changing temperature conditions is described. The voltage distribution on a surface of the metal component, or on a metallic layer which lies over the component, is first obtained. The voltage distribution usually results from a compositional change in the metal component. The voltage distribution is then compared to a thermal exposure-voltage model which expresses voltage distribution as a function of exposure time and exposure temperature for a reference standard corresponding to the metal component. In this manner, the thermal exposure of the selected component can be obtained. A related device for evaluating the thermal exposure of a selected metal component is also described.
摘要翻译：描述了已经暴露于变化的温度条件下的所选金属组分的热暴露评估方法。首先获得金属部件的表面上或位于部件上的金属层上的电压分布。电压分布通常由金属组分的组成变化引起。然后将电压分布与表示与对应于金属组分的参考标准的曝光时间和曝光温度的函数的电压分布的热暴露电压模型进行比较。以这种方式，可以获得所选择的部件的热曝光。还描述了用于评估所选金属组分的热暴露的相关装置。

9. 发明授权

US06287644B1 Continuously-graded bond coat and method of manufacture 失效
标题翻译：连续分级粘结涂层及其制造方法
公开(公告)号：US06287644B1
公开(公告)日：2001-09-11
申请号：US09346915
申请日：1999-07-02
申请人： Melvin Robert Jackson , Ann Melinda Ritter , Michael Francis Xavier Gigliotti, Jr. , Ji-Cheng Zhao
发明人： Melvin Robert Jackson , Ann Melinda Ritter , Michael Francis Xavier Gigliotti, Jr. , Ji-Cheng Zhao
IPC分类号： B05D306
CPC分类号： C23C28/321 , C23C14/025 , C23C14/027 , C23C28/325 , C23C28/345 , C23C28/3455 , Y02T50/67
摘要： A continuously-graded bond coat comprises a gradient of at least one material characteristic value. The gradient extends from a first material characteristic value at a first surface region to a second material characteristic value at a second surface region. The continuously-graded bond coat can be used in a thermal barrier coating system. A source ingot for forming the continuously-graded bond coat comprises aluminum, in an atomic percent range from about 50.0 to less than about 100.0; chromium in an atomic percent range from about 5.0 to about 40.0; silicon in an atomic percent range from about 1.0 to about 17.0; zirconium in an atomic percent range from about a trace to about a 0.5, yttrium in an atomic percent range from a trace to about 2.0; and hafnium in an atomic percent range from about 0.5 to about 2.0. A method for forming the continuously-graded bond coat with the gradient is also provided by the invention.
摘要翻译：连续分级的粘合涂层包括至少一种材料特性值的梯度。梯度从第一表面区域处的第一材料特性值延伸到第二表面区域处的第二材料特性值。连续分级的粘合涂层可用于热障涂层体系。用于形成连续梯度粘合涂层的源锭包括铝，其原子百分比范围为约50.0至小于约100.0; 原子百分比范围为约5.0至约40.0的铬; 原子百分比范围为约1.0至约17.0的硅; 原子百分比范围从约痕量至约0.5的锆，原子百分比范围从痕量至约2.0的钇; 和铪的原子百分比范围为约0.5至约2.0。通过本发明也提供了用梯度形成连续梯度粘结涂层的方法。

10. 发明授权

US07296616B2 Shell mold for casting niobium-silicide alloys, and related compositions and processes 有权
标题翻译：用于铸造铌 - 硅化物合金的壳模，以及相关组合物和工艺
公开(公告)号：US07296616B2
公开(公告)日：2007-11-20
申请号：US11020519
申请日：2004-12-22
申请人： Bernard Patrick Bewlay , Laurent Cretegny , Michael Francis Xavier Gigliotti, Jr. , Roger John Petterson , Ann Melinda Ritter , Stephen Francis Rutkowski
发明人： Bernard Patrick Bewlay , Laurent Cretegny , Michael Francis Xavier Gigliotti, Jr. , Roger John Petterson , Ann Melinda Ritter , Stephen Francis Rutkowski
IPC分类号： B22C1/00
CPC分类号： B22C1/186
摘要： A shell mold for casting molten material to form an article is described. The mold includes a shell for containing the molten material, formed from at least one of yttrium silicates, zirconium silicates, hafnium silicates, and rare earth silicates. The mold also includes a facecoat disposed on an inner surface of the shell that contacts the molten material. The facecoat can be made from the materials described above. A method of casting a niobium-silicide article is also described, using the shell mold described herein. A method of making the ceramic shell mold is described as well, along with a slurry composition used in the manufacture of the shell mold.
摘要翻译：描述了用于铸造熔融材料以形成制品的壳模。模具包括用于容纳由硅酸钇，硅酸锆，硅酸铪和稀土硅酸盐中的至少一种形成的熔融材料的壳体。模具还包括设置在壳体的内表面上并与熔融材料接触的面涂层。面漆可以由上述材料制成。还描述了使用本文所述的壳模具来铸造硅化铌制品的方法。还描述了制造陶瓷壳模的方法，以及用于制造壳模的浆料组合物。

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