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1. 发明授权

US07601400B2 Liquid electrostatic coating composition comprising corrosion resistant metal particulates and method for using same 失效
标题翻译：包含耐腐蚀金属微粒的液体静电涂层组合物及其使用方法
公开(公告)号：US07601400B2
公开(公告)日：2009-10-13
申请号：US11075799
申请日：2005-03-10
申请人： Matthew Bernard Buczek , Andrew Jay Skoog , Jane Ann Murphy , Brian Thomas Hazel
发明人： Matthew Bernard Buczek , Andrew Jay Skoog , Jane Ann Murphy , Brian Thomas Hazel
IPC分类号： B05D1/04
CPC分类号： C04B28/34 , C03C1/008 , C03C8/14 , C03C2207/00 , C03C2207/04 , C04B28/24 , C04B2111/00525 , C04B2111/90 , C09D5/084 , C23C4/123 , C23C22/74 , C23C26/02 , C23C28/022 , C23C28/027 , C23C28/321 , C23C28/3215 , C23C28/345 , F01D5/288 , F05D2230/90 , C04B14/34
摘要： A composition comprising a liquid mixture having: a corrosion resistant metal particulate component comprising aluminum-containing metal particulates, wherein the aluminum-containing metal particulates have a phosphate and/or silica-containing insulating layer; a glass-forming binder component; and a liquid carrier component. Also disclosed is a method comprising the following steps: (a) providing an article comprising a metal substrate; (b) imparting to the metal substrate an electrical charge; and (c) electrostatically applying a liquid coating composition to the electrically charged metal substrate, wherein the liquid coating composition comprises a liquid mixture having: a corrosion resistant metal particulate component comprising aluminum-containing metal particulates having a phosphate and/or silica-containing insulating layer; glass-forming binder component; and a liquid carrier component.
摘要翻译：一种包含液体混合物的组合物，其具有：包含含铝金属微粒的耐腐蚀金属颗粒组分，其中所述含铝金属微粒具有磷酸盐和/或二氧化硅的绝缘层; 玻璃形成粘合剂组分; 和液体载体组分。还公开了一种包括以下步骤的方法：（a）提供包含金属基底的制品; （b）向金属基板施加电荷; 和（c）将液体涂料组合物静电涂覆到带电的金属基底上，其中该液体涂料组合物包含一种液体混合物，该液体混合物具有：包含含磷金属和/或二氧化硅的绝缘的含铝金属微粒的耐腐蚀金属颗粒组分层; 玻璃形成粘合剂成分; 和液体载体组分。

2. 发明申请

US20110076480A1 STRAIN TOLERANT CORROSION PROTECTIVE COATING COMPOSITIONS AND COATED ARTICLES 审中-公开
标题翻译：耐腐蚀耐腐蚀涂料组合物和涂层制品
公开(公告)号：US20110076480A1
公开(公告)日：2011-03-31
申请号：US12570402
申请日：2009-09-30
申请人： Andrew Jay Skoog , Brian Thomas Hazel , Jane Ann Murphy
发明人： Andrew Jay Skoog , Brian Thomas Hazel , Jane Ann Murphy
IPC分类号： B32B15/04 , B32B5/16 , B32B3/26 , C09D5/08
CPC分类号： C04B26/30 , C04B28/34 , C04B2111/26 , C23C28/321 , C23C28/3215 , C23C28/324 , C23C28/34 , C23C28/341 , C23C28/345 , C23C28/3455 , C23C28/36 , F01D5/288 , Y02T50/67 , Y02T50/671 , Y02T50/673 , Y02T50/6765 , Y10T428/249967 , Y10T428/249969 , Y10T428/31678 , C04B14/30 , C04B14/303 , C04B14/304 , C04B14/305 , C04B14/306 , C04B14/307 , C04B20/0096
摘要： A coated article suitable for use at elevated temperature includes a metal substrate and a coating on the substrate. The coating includes a corrosion resistant particulate component having an average coefficient of thermal expansion (CTE) greater than alumina at 1200° F. (649° C.) dispersed in a binder matrix. An aspect ratio of at least a portion of the corrosion resistant particulate component is greater than about 2:1. The binder matrix includes a silicon-containing material and/or a phosphate-containing material.
摘要翻译：适合在高温下使用的涂覆制品包括金属基材和基材上的涂层。该涂层包括耐分散在粘合剂基质中的1200°F（649℃）下平均热膨胀系数（CTE）大于氧化铝的耐腐蚀颗粒组分。耐腐蚀性颗粒组分的至少一部分的纵横比大于约2:1。粘合剂基质包括含硅材料和/或含磷酸盐的材料。

3. 发明申请

US20110076410A1 METHOD FOR MAKING STRAIN TOLERANT CORROSION PROTECTIVE COATING COMPOSITIONS AND COATED ARTICLES 审中-公开
标题翻译：制造耐腐蚀保护涂料组合物和涂层制品的方法
公开(公告)号：US20110076410A1
公开(公告)日：2011-03-31
申请号：US12570474
申请日：2009-09-30
申请人： Andrew Jay Skoog , Brian Thomas Hazel , Jane Ann Murphy
发明人： Andrew Jay Skoog , Brian Thomas Hazel , Jane Ann Murphy
IPC分类号： B05D7/14 , B05D5/00
CPC分类号： C04B26/30 , C04B28/34 , C04B2111/26 , C09D5/084 , C09D5/10 , C09D5/18 , C23C28/321 , C23C28/3215 , C23C28/324 , C23C28/34 , C23C28/341 , C23C28/345 , C23C28/3455 , C23C28/36 , C23C30/00 , F01D25/007 , Y02T50/67 , Y02T50/671 , Y02T50/6765 , C04B14/30 , C04B14/303 , C04B14/304 , C04B14/305 , C04B14/306 , C04B14/307 , C04B20/0096
摘要： Method comprising providing a coating precursor composition including a corrosion resistant particulate component having an average coefficient of thermal expansion (CTE) greater than alumina at 1200° F. (649° C.) dispersed in a binder matrix, wherein an aspect ratio of at least a portion of the corrosion resistant particulate component is greater than about 2:1, and wherein the binder matrix includes at least one member of the group consisting of a silicon-containing material and a phosphate-containing material; providing the coating precursor composition on at least a portion of a metal substrate, and; curing the coating precursor composition to provide a corrosion-resistant coating on at least the portion of the metal substrate.
摘要翻译：方法包括提供一种涂覆前体组合物，其包含分散在粘合剂基质中的1200°F（649℃）下平均热膨胀系数（CTE）大于氧化铝的耐腐蚀性颗粒组分，其中纵横比至少为耐腐蚀性颗粒组分的一部分大于约2:1，并且其中所述粘合剂基质包括由含硅材料和含磷酸盐材料组成的组中的至少一个; 在所述金属基材的至少一部分上提供所述涂料前体组合物，和固化涂料前体组合物以在金属基材的至少一部分上提供耐腐蚀涂层。

4. 发明申请

US20090098394A1 STRAIN TOLERANT CORROSION PROTECTING COATING AND TAPE METHOD OF APPLICATION 审中-公开
标题翻译：耐腐蚀耐腐蚀涂层和胶带应用方法
公开(公告)号：US20090098394A1
公开(公告)日：2009-04-16
申请号：US11616048
申请日：2006-12-26
申请人： Andrew Jay Skoog , Bryan Thomas Bojanowski , Brian Thomas Hazel , Jane Ann Murphy , Michael James Weimer , Timothy A. Doyle
发明人： Andrew Jay Skoog , Bryan Thomas Bojanowski , Brian Thomas Hazel , Jane Ann Murphy , Michael James Weimer , Timothy A. Doyle
IPC分类号： B32B15/04 , C09D1/00 , B05D3/12
CPC分类号： C23C26/00 , C23C28/321 , C23C28/3215 , C23C28/324 , C23C28/34 , C23C28/345 , C23C28/3455 , C23C28/36 , F01D5/28 , F01D5/288 , F05D2300/21 , F05D2300/2102 , F05D2300/211 , Y02T50/67 , Y02T50/6765
摘要： A corrosion resistant tape coating for gas turbine engine includes a glassy ceramic matrix wherein the glassy matrix is silica-based, and includes corrosion resistant particles selected from refractory particles and non-refractory MCrAlX particles, and combinations thereof. The corrosion resistant particles are substantially uniformly distributed within the matrix, and provide the coating with corrosion resistance. Importantly the coating of the present invention has a coefficient of thermal expansion (CTE) greater than that of alumina at engine operating temperatures. The CTE of the coating is sufficiently close to the substrate material such that the coating does not spall after frequent engine cycling at temperatures above 1200° F.
摘要翻译：用于燃气涡轮发动机的耐腐蚀胶带涂层包括玻璃质陶瓷基体，其中玻璃质基质是基于二氧化硅的，并且包括选自耐火颗粒和非难熔MCrAlX颗粒的耐腐蚀颗粒及其组合。耐腐蚀颗粒基本上均匀分布在基质内，并为涂层提供耐腐蚀性。重要的是，本发明的涂层在发动机工作温度下的热膨胀系数（CTE）大于氧化铝的热膨胀系数。涂层的CTE足够接近基底材料，使得涂层在高于1200°F的温度下经常发动机循环后不会分散。

5. 发明授权

US08658291B2 CMAS mitigation compositions, environmental barrier coatings comprising the same, and ceramic components comprising the same 有权
标题翻译： CMAS缓释组合物，包含其的环境屏障涂层和包含其的陶瓷组分
公开(公告)号：US08658291B2
公开(公告)日：2014-02-25
申请号：US12339974
申请日：2008-12-19
申请人： Glen Harold Kirby , Brett Allen Boutwell , Ming Fu , Bangalore Aswatha Nagaraj , Brian Thomas Hazel
发明人： Glen Harold Kirby , Brett Allen Boutwell , Ming Fu , Bangalore Aswatha Nagaraj , Brian Thomas Hazel
IPC分类号： B32B9/00 , B32B19/00 , B32B9/04 , B32B13/04 , F03B3/12 , F03B7/00 , F03D11/02
CPC分类号： C04B41/52 , C04B41/009 , C04B41/89 , C23C28/042 , F01D5/288 , F05D2300/611 , C04B41/5096 , C04B41/5035 , C04B41/5024 , C04B41/5037 , C04B41/522 , C04B41/524 , C04B41/5025 , C04B41/4582 , C04B35/10 , C04B35/00 , C04B35/14 , C04B35/18 , C04B35/185 , C04B35/565 , C04B35/584 , C04B35/806 , C04B35/803
摘要： Calcium magnesium aluminosilicate (CMAS) mitigation compositions selected from rare earth elements, rare earth oxides, zirconia, hafnia partially or fully stabilized with alkaline earth or rare earth elements, zirconia partially or fully stabilized with alkaline earth or rare earth elements, magnesium oxide, cordierite, aluminum phosphate, magnesium silicate, and combinations thereof when the CMAS mitigation composition is included as a separate CMAS mitigation layer in an environmental barrier coating for a high temperature substrate component.
摘要翻译：选自稀土元素，稀土氧化物，氧化锆，部分或完全用碱土金属或稀土元素稳定的镁铝硅酸钙（CMAS）缓蚀组合物，用碱土金属或稀土元素部分或完全稳定的氧化锆，氧化镁，堇青石，当将CMAS缓和组合物作为单独的CMAS缓解层包含在高温底物组分的环境屏障涂层中时，可以使用磷酸铝，硅酸镁及其组合。

6. 发明授权

US07919187B2 Environmental barrier coating for silicon-containing substrates and process therefor 失效
标题翻译：含硅基材的环境阻隔涂层及其工艺
公开(公告)号：US07919187B2
公开(公告)日：2011-04-05
申请号：US11616361
申请日：2006-12-27
申请人： Brian Thomas Hazel , Christine Walston , Irene Spitsberg
发明人： Brian Thomas Hazel , Christine Walston , Irene Spitsberg
IPC分类号： B32B13/04 , B05D3/02
CPC分类号： C04B41/85 , C04B35/195 , C04B41/009 , C04B41/5024 , C04B41/52 , C04B41/89 , C04B2235/3213 , C04B2235/3215 , C04B2235/3217 , C04B2235/3481 , C04B2235/79 , C04B2235/80 , C23C4/11 , C23C4/18 , C23C28/04 , C23C30/00 , F01D5/288 , F05D2230/90 , F05D2300/211 , F05D2300/2112 , F23M2900/05004 , F23R3/007 , Y02T50/67 , Y02T50/672 , C04B41/4527 , C04B41/5096 , C04B41/5037 , C04B41/5042 , C04B35/565 , C04B35/584 , C04B35/806 , C04B41/0072 , C04B41/4519 , C04B2111/0025
摘要： A protective coating for use on a silicon-containing substrate, and deposition methods therefor. The coating has a strontium-aluminosilicate (SAS) composition that is less susceptible to degradation by volatilization and in corrosive environments as a result of having at least an outer surface region that consists essentially of one or more stoichiometric crystalline phases of SAS and is substantially free of a nonstoichiometric second crystalline phase of SAS that contains a substoichiometric amount of silica. The coating can be produced by carrying out deposition and heat treatment steps that result in the entire coating or just the outer surface region of the coating consisting essentially of the stoichiometric celsian phase.
摘要翻译：用于含硅基材的保护涂层及其沉积方法。涂层具有锶 - 硅铝酸盐（SAS）组合物，其通过挥发和腐蚀性环境中较不易于降解，因为至少具有由SAS的一个或多个化学计量结晶相组成的至少一个外表面区域，并且基本上没有的非化学计量的第二结晶相的SAS，其含有亚化学计量的二氧化硅。可以通过进行沉积和热处理步骤来产生涂层，所述沉积和热处理步骤导致整个涂层或仅基本上由化学计量的凝胶相组成的涂层的外表面区域。

7. 发明申请

US20100330295A1 METHOD FOR PROVIDING DUCTILE ENVIRONMENTAL COATING HAVING FATIGUE AND CORROSION RESISTANCE 审中-公开
标题翻译：提供具有耐疲劳性和耐腐蚀性的耐腐蚀环氧涂层的方法
公开(公告)号：US20100330295A1
公开(公告)日：2010-12-30
申请号：US12494813
申请日：2009-06-30
申请人： Brian Thomas Hazel , Ming Fu
发明人： Brian Thomas Hazel , Ming Fu
IPC分类号： C23C4/08 , B05D3/02 , C23C16/44 , C23C14/34
CPC分类号： C23C28/028 , C23C4/073 , C23C10/56 , C23C28/021 , C23C30/00
摘要： Method includes providing a superalloy substrate such as a turbine disk, a turbine seal, a turbine blade, a turbine nozzle, a turbine shroud, or a turbine frame or case having an under platform or non-gas path region; and providing a predominantly gamma-prime nickel aluminide intermetallic ductile corrosion and oxidation resistant coating disposed on at least a portion of the substrate. The coating comprises from about 15 to about 30 atomic % aluminum, up to about 20 atomic % chromium, optionally, up to about 30 atomic % of at least one platinum group metal, optionally, up to about 4 atomic % of at least one reactive element, and optionally, up to about 15 atomic % of at least one strengthening element, and a balance being essentially nickel or nickel and at least one of cobalt, iron, or cobalt and iron. A coating precursor composition may be applied to the substrate before or after optional plating with one or more platinum group metals.
摘要翻译：方法包括提供诸如涡轮盘，涡轮密封件，涡轮叶片，涡轮喷嘴，涡轮机罩或具有下平台或非气体路径区域的涡轮机框架或壳体的超级合金基板; 并且提供主要是γ-基铝酸镍金属间金属延性腐蚀和抗氧化涂层，其设置在所述基底的至少一部分上。涂层包含约15至约30原子％的铝，至多约20原子％的铬，任选的至多约30原子％的至少一种铂族金属，任选的至多约4原子％的至少一种反应性元素和任选地至多约15原子％的至少一种强化元素，余量基本上为镍或镍以及钴，铁或钴和铁中的至少一种。涂覆前体组合物可以在用一种或多种铂族金属任选镀覆之前或之后施加到基材上。

8. 发明申请

US20100159150A1 METHODS FOR MAKING ENVIRONMENTAL BARRIER COATINGS AND CERAMIC COMPONENTS HAVING CMAS MITIGATION CAPABILITY 有权
标题翻译：制备环境阻隔涂层的方法和具有CMAS缓解能力的陶瓷组件
公开(公告)号：US20100159150A1
公开(公告)日：2010-06-24
申请号：US12340013
申请日：2008-12-19
申请人： GLEN HAROLD KIRBY , Brett Allen Boutwell , Ming Fu , Bangalore Aswatha Nagaraj , Brian Thomas Hazel
发明人： GLEN HAROLD KIRBY , Brett Allen Boutwell , Ming Fu , Bangalore Aswatha Nagaraj , Brian Thomas Hazel
IPC分类号： C23C4/10 , B32B9/04 , B05D1/36 , C23C14/34
CPC分类号： C23C28/042 , C04B41/009 , C04B41/4584 , C04B41/52 , C04B41/89 , C23C4/11 , C04B41/5096 , C04B41/5035 , C04B41/5024 , C04B41/5037 , C04B41/4539 , C04B41/5027 , C04B41/4582 , C04B41/4531 , C04B41/4537 , C04B35/195 , C04B35/565 , C04B35/584 , C04B35/806
摘要： Methods of making components having calcium magnesium aluminosilicate (CMAS) mitigation capability involving providing a component; applying an environmental barrier coating to the component, the environmental barrier coating having a separate CMAS mitigation layer including a CMAS mitigation composition selected from rare earth elements, rare earth oxides, zirconia, hafnia partially or fully stabilized with alkaline earth or rare earth elements, zirconia partially or fully stabilized with alkaline earth or rare earth elements, magnesium oxide, cordierite, aluminum phosphate, magnesium silicate, and combinations thereof.
摘要翻译：制备具有钙镁铝硅酸盐（CMAS）减轻能力的组分的方法涉及提供组分; 将环境屏障涂层施加到部件上，环境屏障涂层具有单独的CMAS缓解层，其包括选自稀土元素，稀土氧化物，氧化锆，部分或完全用碱土金属或稀土元素稳定的半导体材料的CMAS缓和组合物，氧化锆部分或完全用碱土金属或稀土元素稳定，氧化镁，堇青石，磷酸铝，硅酸镁及其组合。

9. 发明授权

US07442444B2 Bond coat for silicon-containing substrate for EBC and processes for preparing same 有权
标题翻译：用于EBC的含硅基材的粘合剂涂层及其制备方法
公开(公告)号：US07442444B2
公开(公告)日：2008-10-28
申请号：US11150098
申请日：2005-06-13
申请人： Brian Thomas Hazel , Irene Spitsberg , Brett Allen Boutwell
发明人： Brian Thomas Hazel , Irene Spitsberg , Brett Allen Boutwell
IPC分类号： B32B15/04 , B32B18/00 , F01D5/14
CPC分类号： C04B35/806 , C04B35/16 , C04B35/185 , C04B35/195 , C04B35/573 , C04B35/58085 , C04B35/584 , C04B35/62863 , C04B41/52 , C04B41/89 , C04B2235/3208 , C04B2235/3213 , C04B2235/3215 , C04B2235/3225 , C04B2235/3427 , C04B2235/3463 , C04B2235/3481 , C04B2235/5244 , C04B2235/5248 , C23C4/02 , C23C28/042 , C23C28/048 , C23C28/322 , C23C28/345 , C23C28/3455 , C23C28/36 , C23C30/00 , F01D5/288 , F05D2230/90 , F05D2260/95 , F05D2300/222 , F05D2300/611 , Y10T428/12611 , Y10T428/12674 , Y10T428/264 , C04B41/5071 , C04B41/53 , C04B41/0072 , C04B41/4558 , C04B41/5035 , C04B41/5024 , C04B41/5037 , C04B41/4529 , C04B41/5031 , C04B41/4527 , C04B41/5042 , C04B41/522
摘要： An article comprising a silicon-containing substrate, a silicide-containing bond coat layer overlying the substrate, and typically an environmental barrier coating overlaying the bond coat layer. An article is also provided wherein the environmental barrier coating comprises: (1) an optional inner silica scale layer overlaying the bond coat layer; (2) intermediate layer overlaying the inner silica scale layer, or the bond coat layer in the absence of the inner silica scale layer, and comprising mullite, or a combination of mullite with a barium strontium aluminosilicate, a yttrium silicate, or a calcium aluminosilicate; and (3) an outer steam-resistant barrier layer overlaying the intermediate layer and consisting essentially of an alkaline earth silicate/aluminosilicate. Processes are also provided for forming the silicide-containing bond coat layer over the substrate, followed by forming the environmental barrier coating over the bond coat layer.
摘要翻译：包括含硅基材，覆盖在基材上的含硅化物粘合涂层的物品，通常是覆盖粘合涂层的环境阻挡涂层。还提供了一种制品，其中所述环境保护涂层包括：（1）覆盖所述粘合涂层的任选的内部二氧化硅刻度层; （2）覆盖内部二氧化硅刻度层的中间层或不存在内部二氧化硅刻度层的粘合涂层，并且包含莫来石或莫来石与铝酸钡锶钡，硅酸钇或硅铝酸钙的组合 ; 和（3）覆盖中间层并基本上由碱土金属硅酸盐/硅铝酸盐组成的外部耐蒸汽阻挡层。还提供了用于在衬底上形成含硅化物粘合涂层的工艺，然后在粘合涂层上形成环境阻挡涂层。

10. 发明申请

US20080220172A1 Sintering resistant, low conductivity, high stability thermal barrier coating/environmental barrier coating system for a ceramic-matrix composite (CMC) article to improve high temperature capability 有权
公开(公告)号：US20080220172A1
公开(公告)日：2008-09-11
申请号：US11977336
申请日：2007-10-23
申请人： Brett Allen Rohrer Boutwell , Irene Spitsberg , Christine Govern , Bangalore A. Nagaraj , Brian Thomas Hazel
发明人： Brett Allen Rohrer Boutwell , Irene Spitsberg , Christine Govern , Bangalore A. Nagaraj , Brian Thomas Hazel
IPC分类号： B05D1/36
CPC分类号： C04B41/009 , C04B41/52 , C04B41/89 , C23C28/042 , F01D5/288 , F05D2230/90 , F05D2300/2118 , F05D2300/50211 , F05D2300/611 , C04B41/4527 , C04B41/5096 , C04B41/5024 , C04B41/5037 , C04B41/5042 , C04B41/5031 , C04B41/522 , C04B41/4529 , C04B35/565 , C04B35/584 , C04B35/806 , C04B35/597
摘要： In accordance with an embodiment of the invention, a thermal barrier coating (TBC) for inclusion in a thermal barrier coating/environmental barrier coating system (TBC/EBC system) for use on a silicon containing material substrate is provided. The TBC comprises a compound having a primary constituent portion and a stabilizer portion stabilizing said primary constituent. The primary constituent portion of the TBC comprises hafnia present in an amount of at least about 5 mol % of the primary constituent. The stabilizer portion of said thermal barrier coating comprises at least one metal oxide comprised of cations with a +2 or +3 valence present in the amount of about 10 to about 40 mol % of the thermal barrier coating.

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