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1. 发明授权

US5426255A Methyl, substituted propyl-substituted pentamethyl indane derivatives, processes for producing same and perfumery uses thereof 失效
标题翻译：甲基取代的丙基取代的五甲基二氢化茚衍生物，其制备方法和香料用途
公开(公告)号：US5426255A
公开(公告)日：1995-06-20
申请号：US278962
申请日：1994-07-22
申请人： Mark A. Sprecker , Olivier J. Gillotin
发明人： Mark A. Sprecker , Olivier J. Gillotin
IPC分类号： C11B9/00 , C11D3/50 , C07C17/093
CPC分类号： C11B9/0049 , C11B9/0053 , C11B9/008 , C11D3/50
摘要： Described are processes for preparing methyl, substituted propyl-substituted pentamethyl indane derivatives using as a starting material the mixture of compounds defined according to the structure: ##STR1## also known as GALAXOLIDE.RTM. (trademark of International Flavors & Fragrances Inc.). Also described are mixtures of methyl, substituted propyl-substituted pentamethyl indane derivatives with other musk chemicals including but not limited to GALAXOLIDE.RTM. defined according to the structure: ##STR2##
摘要翻译：描述了使用根据以下结构定义的化合物的混合物制备甲基取代的丙基取代的五甲基二氢化茚衍生物的方法：也称为GALAXOLIDE TM（International Flavors＆amp; Fragrances Inc.的商标）。还描述了甲基，取代的丙基取代的五甲基二氢化茚衍生物与其它麝香化学品的混合物，包括但不限于根据以下结构定义的GALAXOLIDE TM：

2. 发明授权

US5494892A Methyl substituted propyl-substituted pentamethyl indane derivatives processes for producing same and perfumery uses thereof 失效
标题翻译：甲基取代的丙基取代的五甲基二氢茚衍生物的制备方法及其香料用途
公开(公告)号：US5494892A
公开(公告)日：1996-02-27
申请号：US310105
申请日：1994-09-22
申请人： Mark A. Sprecker , Olivier J. Gillotin
发明人： Mark A. Sprecker , Olivier J. Gillotin
IPC分类号： C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11B9/0053 , C11B9/0049 , C11B9/008 , C11D3/50
摘要： Described are methyl, substituted propyl-substituted pentamethyl indane derivatives defined according to the structure: ##STR1## wherein R.sub.1 represents hydroxyl or methyl; and R.sub.2 represents hydrogen, chloro or OR.sub.6 ; and R.sub.3 represents hydrogen or methyl with the provisos:(i) when R.sub.1 is hydroxyl, R.sub.2 is hydrogen and R.sub.3 is methyl; and(ii) when R.sub.1 is methyl, one of R.sub.2 is chloro or OR.sub.6 and R.sub.3 is hydrogenaugmenting, enhancing or imparting aromas in or to perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.Also described are processes for preparing such methyl, substituted propyl-substituted pentamethyl indane derivatives using as a starting material the mixture of compounds defined according to the structure: ##STR2## also know as GALAXOLIDE.RTM. (trademark of International Flavors & Fragrances Inc.).
摘要翻译：描述了根据以下结构定义的甲基取代的丙基取代的五甲基二氢化茚衍生物：其中R 1表示羟基或甲基; 并且R 2表示氢，氯或OR 6; 并且R 3表示氢或甲基，条件是：（ⅰ）当R 1是羟基时，R 2是氢，R 3是甲基; 和（ii）当R 1为甲基时，R 2为氯或OR 6，并且R 3为增氢，增强或赋予香料组合物，古龙水和香料制品中的香味，包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，加香聚合物，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。还描述了使用根据以下结构定义的化合物的混合物作为原料制备这种甲基取代的丙基取代的五甲基二氢化茚衍生物的方法：也称为GALAXOLIDE TM（International Flavors＆amp; Fragrances Inc.的商标）。

3. 发明授权

US5358930A 2-ethoxy-4-formyl phenyl ester of propionic acid and use in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles 失效
标题翻译：丙酸的2-乙氧基-4-甲酰基苯基酯，用于增强或增强香水组合物，古龙水和香水制品的香气
公开(公告)号：US5358930A
公开(公告)日：1994-10-25
申请号：US168349
申请日：1993-12-17
申请人： Mark A. Sprecker , Richard A. Weiss , Richard M. Boden , Olivier J. Gillotin
发明人： Mark A. Sprecker , Richard A. Weiss , Richard M. Boden , Olivier J. Gillotin
IPC分类号： C07C69/017 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0061 , C07C69/017
摘要： Described is 2-ethoxy-4-formyl phenyl ester of propionic acid of our invention defined according to the structure: ##STR1## and uses thereof in augmenting or enhancing the aroma of perfume compositions, perfumed articles and colognes.
摘要翻译：描述了根据本发明的丙酸的2-乙氧基-4-甲酰基苯基酯，其结构如下：＆lt; IMAGE＆gt;及其用于增强或增强香料组合物，香料制品和古龙水的香气的用途。

4. 发明授权

US5583272A Methyl substituted propyl-substituted pentamethyl indane derivatives, processes for producing same and perfumery uses thereof 失效
标题翻译：甲基取代的丙基取代的五甲基二氢化茚衍生物，其制备方法和香料用途
公开(公告)号：US5583272A
公开(公告)日：1996-12-10
申请号：US428429
申请日：1995-04-25
申请人： Mark A. Sprecker , Olivier J. Gillotin
发明人： Mark A. Sprecker , Olivier J. Gillotin
IPC分类号： C11B9/00 , C11D3/50 , C07C17/093
CPC分类号： C11B9/0053 , C11B9/0049 , C11B9/008 , C11D3/50
摘要： Described are methyl, substituted propyl-substituted pentamethyl indane derivatives defined according to the structure: ##STR1## wherein R.sub.1 represents hydroxyl or methyl; and R.sub.2 represents hydrogen, chloro or OR.sub.6 ; and R.sub.3 represents hydrogen or methyl with the provisos:(i) when R.sub.1 is hydroxyl, R.sub.2 is hydrogen and R.sub.3 is methyl; and(ii) when R.sub.1 is methyl, one of R.sub.2 is chloro or OR.sub.6 and R.sub.3 is hydrogenand wherein the structure represents a mixture wherein in the mixture in one of the compounds R.sub.4 and R.sub.4 ' are both methyl and R.sub.7 is methyl (about 90% by weight); and in the other compounds one of R.sub.4 or R.sub.4 ' is methyl and the other is ethyl and R.sub.7 is hydrogen (about 10% by weight of the compounds); and wherein R.sub.6 is methyl, ethyl, n-propyl or i-propyl; and uses thereof in augmenting, enhancing or imparting aromas in or to perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述了根据以下结构定义的甲基取代的丙基取代的五甲基二氢化茚衍生物：其中R 1表示羟基或甲基; 并且R 2表示氢，氯或OR 6; 并且R 3表示氢或甲基，条件是：（ⅰ）当R 1是羟基时，R 2是氢，R 3是甲基; 和（ii）当R 1是甲基时，R 2是氯或OR 6，R 3是氢，并且其中该结构表示一种混合物，其中一种化合物R4和R4'的混合物都是甲基，而R7是甲基（约90 重量％）; 在其它化合物中，R4或R4'之一为甲基，另一个为乙基，R7为氢（约占该化合物的10重量％）; 其中R6是甲基，乙基，正丙基或异丙基; 包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，加香聚合物，织物柔软剂组合物，织物柔软剂制品，化妆品粉末，香料和香料和头发制剂。

5. 发明授权

US5502031A Methyl substituted propyl-substituted pentamethyl indane derivatives processes for producing same and perfumery uses thereof 失效
标题翻译：甲基取代的丙基取代的五甲基二氢茚衍生物的制备方法及其香料用途
公开(公告)号：US5502031A
公开(公告)日：1996-03-26
申请号：US309505
申请日：1994-09-22
申请人： Mark A. Sprecker , Olivier J. Gillotin
发明人： Mark A. Sprecker , Olivier J. Gillotin
IPC分类号： C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11B9/0049 , C11B9/0053 , C11B9/008 , C11D3/50
摘要： Described are methyl, substituted propyl-substituted pentamethyl indane derivatives defined according to the structure: ##STR1## wherein R.sub.1 represents chloro, hydroxyl or OR.sub.6 ; and R.sub.5 represents methyl or hydrogen with the proviso that when R.sub.1 is chloro, R.sub.5 is hydrogen, and wherein the structure represents a mixture wherein in the mixture in one of the compounds R.sub.4 and R.sub.4 ' are both methyl and R.sub.7 is methyl (about 90% by weight); and in the other compounds one of R.sub.4 or R.sub.4 ' is methyl and the other is ethyl (about 10% by weight of the compounds) and R.sub.7 is hydrogen; and uses thereof in augmenting, enhancing or imparting aromas in or to perfume compositions.Also described are processes for preparing such methyl, substituted propyl-substituted pentamethyl indane derivatives using as a starting material the mixture of compounds defined according to the structure: ##STR2## also know as GALAXOLIDE.RTM. (trademark of International Flavors & Fragrances Inc.).
摘要翻译：描述了根据以下结构定义的甲基取代的丙基取代的五甲基二氢茚衍生物：其中R 1表示氯，羟基或OR 6; 并且R 5表示甲基或氢，条件是当R 1是氯时，R 5是氢，并且其中该结构表示一种混合物，其中一种化合物R4和R4'的混合物都是甲基，R7是甲基（约90％重量）; 在其它化合物中，R4或R4'之一是甲基，另一个是乙基（约10重量％的化合物），而R7是氢; 及其用于增加，增强或赋予香料或香料组合物中的香味。还描述了使用根据以下结构定义的化合物的混合物作为原料制备这种甲基取代的丙基取代的五甲基二氢化茚衍生物的方法：也称为GALAXOLIDE TM（International Flavors＆amp; Fragrances Inc.的商标）。

6. 发明授权

US5376630A Methyl, substituted propyl-substituted pentamethyl indane derivatives, processes for producing same and perfumery uses thereof 失效
标题翻译：甲基取代的丙基取代的五甲基二氢化茚衍生物，其制备方法和香料用途
公开(公告)号：US5376630A
公开(公告)日：1994-12-27
申请号：US214229
申请日：1994-03-17
申请人： Mark A. Sprecker , Olivier J. Gillotin
发明人： Mark A. Sprecker , Olivier J. Gillotin
IPC分类号： C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11B9/0049 , C11B9/0053 , C11B9/008 , C11D3/50
摘要： Described are methyl, substituted propyl-substituted pentamethyl indane derivatives defined according to the structure: ##STR1## wherein R.sub.1 represents hydroxyl or methyl; R.sub.2 represents hydrogen, chloro or OR.sub.6 ; and R.sub.3 represents hydrogen or methyl with the provisos:(i) when R.sub.1 is hydroxyl, R.sub.2 is hydrogen and R.sub.3 is methyl; and(ii) when R.sub.1 is methyl, one of R.sub.2 is chloro or OR.sub.6 and R.sub.3 is hydrogenand wherein the structure represents a mixture wherein in the mixture in one of the compounds R.sub.4 and R.sub.4 ' are both methyl (about 90% by weight); and in the other compounds one of R.sub.4 or R.sub.4 ' is methyl and the other is ethyl (about 10% by weight of the compounds); and wherein R.sub.6 is methyl, ethyl, n-propyl or i-propyl; and uses thereof in augmenting, enhancing or imparting aromas in or to perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations. Also described are processes for preparing such methyl, substituted propyl-substituted pentamethyl indane derivatives using as a starting material the mixture of compounds defined according to the structure: ##STR2## also known as GALAXOLIDE.RTM. (trademark of International Flavors & Fragrances Inc.). Also described are mixtures of methyl, substituted propyl-substituted pentamethyl indane derivatives with other musk chemicals including but not limited to GALAXOLIDE.RTM. defined according to the structure: ##STR3##
摘要翻译：描述了根据以下结构定义的甲基取代的丙基取代的五甲基二氢化茚衍生物：其中R 1表示羟基或甲基; R2代表氢，氯或OR6; 并且R 3表示氢或甲基，条件是：（ⅰ）当R 1是羟基时，R 2是氢，R 3是甲基; 和（ii）当R 1为甲基时，R 2为氯或OR 6，R 3为氢，其中该结构为混合物，其中化合物R4和R4'之一的混合物均为甲基（约90重量％）， ; 在其它化合物中，R 4或R 4'中的一个是甲基，另一个是乙基（约10重量％的化合物）; 其中R6是甲基，乙基，正丙基或异丙基; 包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，加香聚合物，织物柔软剂组合物，织物柔软剂制品，化妆品粉末，香料和香料和头发制剂。还描述了使用根据以下结构定义的化合物的起始原料制备这种甲基取代的丙基取代的五甲基二氢化茚衍生物的方法：也称为GALAXOLIDE TM（International Flavors＆amp; Fragrances Inc.的商标）。还描述了甲基，取代的丙基取代的五甲基二氢化茚衍生物与其它麝香化学品的混合物，包括但不限于根据以下结构定义的GALAXOLIDE TM：

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