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1. 发明申请

US20110287573A1 ATYPICAL KESTERITE COMPOSITIONS 失效
标题翻译：天然食品组合物
公开(公告)号：US20110287573A1
公开(公告)日：2011-11-24
申请号：US12784799
申请日：2010-05-21
申请人： Lynda Kaye Johnson , H. David Rosenfeld , Daniela Rodica Radu
发明人： Lynda Kaye Johnson , H. David Rosenfeld , Daniela Rodica Radu
IPC分类号： H01L31/18 , H01B1/10
CPC分类号： H01L31/0326 , C01B19/002 , C01G19/006 , C09D11/52 , C23C18/1204 , C23C18/1283 , H01L31/18 , Y02E10/50
摘要： This invention relates to processes for making kesterite compositions with atypical Cu:Zn:Sn:S ratios and/or kesterite compositions with unusually small coherent domain sizes. This invention also relates to these kesterite compositions and their use in preparing CZTS films.
摘要翻译：本发明涉及制备具有非常小的相干结构域尺寸的非典型Cu：Zn：Sn：S比和/或kesterite组合物的酯酶组合物的方法。本发明还涉及这些挥发油酯组合物及其在制备CZTS薄膜中的用途。

2. 发明申请

US20120055554A1 COPPER ZINC TIN CHALCOGENIDE NANOPARTICLES 审中-公开
标题翻译：铜箔锡纳米复合纳米粒子
公开(公告)号：US20120055554A1
公开(公告)日：2012-03-08
申请号：US13320156
申请日：2010-05-21
申请人： Daniela Rodica Radu , Jonathan V. Caspar , Lynda Kaye Johnson , H. David Rosenfeld , Irina Malajovich , Meijun Lu
发明人： Daniela Rodica Radu , Jonathan V. Caspar , Lynda Kaye Johnson , H. David Rosenfeld , Irina Malajovich , Meijun Lu
IPC分类号： H01L31/0264 , C09D11/00 , B05D3/02 , B05D7/24 , H01B1/02 , B05D3/00 , B82Y30/00
CPC分类号： B82Y30/00 , C09D11/03 , C09D11/52 , H01L31/0327 , H01L31/206 , Y02E10/50 , Y02P70/521
摘要： This invention relates to nanoparticles of kesterite (copper zinc tin sulfide) and copper zinc tin selenide nanoparticles, inks and devices thereof, and processes to prepare same. The nano-particles are useful to for the absorber layer as a p-type semiconductor in a thin film solar cell application.
摘要翻译：本发明涉及蛇毒石（铜锌锡硫化物）和铜锌锡硒纳米颗粒的纳米颗粒，油墨及其装置及其制备方法。在薄膜太阳能电池应用中，纳米颗粒可用作吸收层作为p型半导体。

3. 发明申请

US20140144500A1 SEMICONDUCTOR INKS FILMS, COATED SUBSTRATES AND METHODS OF PREPARATION 审中-公开
标题翻译：半导体墨盒，涂层基材和制备方法
公开(公告)号：US20140144500A1
公开(公告)日：2014-05-29
申请号：US13885286
申请日：2011-11-20
申请人： Yanyan Cao , John W. Catron, JR. , Lynda Kaye Johnson , Meijun Lu , Daniela Rodica Radu , Jonathan V. Caspar , Irina Malajovich , H. David Rosenfeld
发明人： Yanyan Cao , John W. Catron, JR. , Lynda Kaye Johnson , Meijun Lu , Daniela Rodica Radu , Jonathan V. Caspar , Irina Malajovich , H. David Rosenfeld
IPC分类号： H01L31/032 , H01L31/18
CPC分类号： H01L31/0322 , H01L21/0237 , H01L21/02422 , H01L21/02491 , H01L21/02568 , H01L21/02601 , H01L21/02628 , H01L31/0326 , H01L31/18 , Y02E10/50
摘要： This invention provides compositions useful for preparing films of CZTS and its selenium analogues on a coated substrate. This invention also provides processes for preparing films and coated substrates comprising CZTS/Se microparticles embedded in an inorganic matrix. This invention also provides processes for preparing photovoltaic cells comprising films of CZTS and its selenium analogues.
摘要翻译：本发明提供了可用于在涂覆的基底上制备CZTS及其硒类似物的膜的组合物。本发明还提供了制备包含嵌入无机基质中的CZTS / Se微粒的膜和涂覆基质的方法。本发明还提供了制备包含CZTS及其硒类似物的膜的光伏电池的方法。

4. 发明授权

US08366975B2 Atypical kesterite compositions 失效
标题翻译：非典型的Kesterite组合物
公开(公告)号：US08366975B2
公开(公告)日：2013-02-05
申请号：US12784799
申请日：2010-05-21
申请人： Lynda Kaye Johnson , H. David Rosenfeld , Daniela Rodica Radu
发明人： Lynda Kaye Johnson , H. David Rosenfeld , Daniela Rodica Radu
IPC分类号： H01B1/08 , C01B19/00 , C01G19/00 , C09D11/00 , C23C18/12
CPC分类号： H01L31/0326 , C01B19/002 , C01G19/006 , C09D11/52 , C23C18/1204 , C23C18/1283 , H01L31/18 , Y02E10/50
摘要： This invention relates to processes for making kesterite compositions with atypical Cu:Zn:Sn:S ratios and/or kesterite compositions with unusually small coherent domain sizes. This invention also relates to these kesterite compositions and their use in preparing CZTS films.
摘要翻译：本发明涉及制备具有非常小的相干结构域尺寸的非典型Cu：Zn：Sn：S比和/或kesterite组合物的酯酶组合物的方法。本发明还涉及这些挥发油酯组合物及其在制备CZTS薄膜中的用途。

5. 发明申请

US20110118514A1 Process for the Preparation of 1,1,1,3,3,3-Hexafluoro-Propane and at Least One Of 1,1,1,2,3,3-Hexafluoropropane, Hexafluoropropane and 1,1,1,2,3,3,3-Heptafluoropropane 失效
标题翻译： 1,1,1,3,3,3-六氟丙烷的制备方法和1,1,1,2,3,3-六氟丙烷，六氟丙烷和1,1,1,2,3 ，3,3-七氟丙烷
公开(公告)号：US20110118514A1
公开(公告)日：2011-05-19
申请号：US11988258
申请日：2006-08-04
申请人： Velliyur Nott Mallikarjuna Rao , H. David Rosenfeld , Allen Capron Sievert , Shekhar Subramoney
发明人： Velliyur Nott Mallikarjuna Rao , H. David Rosenfeld , Allen Capron Sievert , Shekhar Subramoney
IPC分类号： C07C17/23 , C07C17/20
CPC分类号： B01J37/26 , B01J23/868 , C07C17/21 , C07C17/23 , C07C19/08 , C07C21/18 , C07C19/10
摘要： A process is disclosed for the manufacture of 1,1,1,3,3,3-hexafluoropropane and 1,1,1,2,3,3-hexafluoropropane, hexafluoropropene and/or 1,1,1,2,3,3,3-heptafluoropropane. The process involves (a) reacting HF, Cl2, and at least one halopropene of the formula CX3CCI═CCIX (where each X is independently F or CI) to produce a product comprising CF3CCI2CF3 and CF3CCIFCCIF2; (b) reacting CF3CCI2CF3 and CF3CCIFCCIF2 produced in (a) with hydrogen, optionally in the presence of HF, to produce a product comprising CF3CH2CF3 and at least one of CHF2CHFCF3, CF3CF═CF2 and CF3CFHCF3; and (c) recovering from the product produced in (b), CF3CH2CF3 and at least one of CHF2CHFCF3, CF3CF═CF2 and CF3CFHCF3. In (a), the CF3CCI2CF3 and CF3CCIFCCIF2 are produced in the presence of a chlorofluorination catalyst including (i) a crystalline alpha-chromium oxide where at least 0.05 atom % of the chromium atoms in the alpha-chromium oxide lattice are replaced by divalent copper, and/or (ii) a chromium-containing composition of (i) which has been treated with a fluorinating agent.
摘要翻译：公开了用于制造1,1,1,3,3,3-六氟丙烷和1,1,1,2,3,3-六氟丙烷，六氟丙烯和/或1,1,1,2,3， 3,3-七氟丙烷。该方法包括（a）使HF，Cl 2和至少一种式CX3CCI = CCIX（其中每个X独立地为F或Cl）的卤代丙烯反应，以产生包含CF 3 CCl 2 CF 3和CF 3 CClFCCIF 2的产物; （b）任选地在HF存在下使（a）中产生的CF 3 CCl 2 CF 3和CF 3 CClF CIFF 2与氢反应，以产生包含CF 3 CH 2 CF 3和CHF 2 CHFCF 3，CF 3CF≡CF2和CF 3 CFHCF 3中的至少一种的产物; 和（c）从（b）中产生的产物，CF 3 CH 2 CF 3和CHF 2 CHFCF 3，CF 3CF≡CF2和CF 3 CFHCF 3中的至少一种中回收。在（a）中，CF 3 CCl 2 CF 3和CF 3 CClFCCIF 2在氯氟化催化剂存在下制备，包括（i）α-氧化铬晶格中至少0.05原子％的铬原子被二价铜取代的结晶α-氧化铬，和/或（ⅱ）已经用氟化剂处理的（ⅰ）的含铬组合物。

6. 发明授权

US07129383B2 Processes for the preparation of 2-chloro-1,1,1,2,3,3,3-heptafluoropropane, hexafluoropropene and 1,1,1,2,3,3,3-heptafluoropropane 失效
标题翻译：制备2-氯-1,1,1,2,3,3,3-七氟丙烷，六氟丙烯和1,1,1,2,3,3,3-七氟丙烷的方法
公开(公告)号：US07129383B2
公开(公告)日：2006-10-31
申请号：US10523223
申请日：2003-08-21
申请人： Mario J. Nappa , Velliyur Nott Mallikarjuna Rao , H. David Rosenfeld , Sekhar Subramoney , Munirpallam A. Subramanian , Allen C. Sievert
发明人： Mario J. Nappa , Velliyur Nott Mallikarjuna Rao , H. David Rosenfeld , Sekhar Subramoney , Munirpallam A. Subramanian , Allen C. Sievert
IPC分类号： C07C17/00 , C07C17/266 , C07C17/10
CPC分类号： C07C19/08 , B01J23/26 , B01J23/866 , B01J35/002 , B01J37/0236 , B01J37/03 , B01J37/26 , C07C17/206 , C07C17/21 , C07C17/23 , C07C17/25 , C07C19/10 , C07C21/18
摘要： A process for the preparation of 2-chloro-1,1,1,3,3,3-heptafluoropropane is disclosed which involves (a) contacting a mixture comprising hydrogen fluoride, chlorine, and at least one starting material selected from the group consisting of halopropenes of the formula CX3CCI═CX2 and halopropanes of the formula the CX3CCIYCX3, wherein each X is independently F or Cl, and Y is H, Cl or F (provided that the number of X and Y which are F totals no more than six) with a chlorofluorination catalyst in a reaction zone to produce a product mixture comprising CF3CCIFCF3, HCI, HF. and underfluorinated halogenated hydrocarbon intermediates. The process is characterized by said chlorofluorination catalyst comprising at least one chromium-containing component selected from (i) a crystalline alpha-chromium oxide where at least 0.05 atom % of the chromium atoms in the alpha-chromium oxide lattice are replaced by nickel, trivalent cobalt or both nickel and trivalent cobalt, provided that no more than 2 atom % of the chromium atoms in the alpha-chromium oxide lattice are replaced by nickel and that the total amount of chromium atoms in the alpha-chromium oxide lattice that are replaced by nickel and trivalent cobalt is no more than 6 atom %, and (ii) a fluorinated crystalline oxide of (i). Also disclosed is a process for the manufacture of a mixture of HFC-227ea and hexafluoropropene by reacting a starting mixture comprising CFC-217ba and hydrogen in the vapor phase at an elevated temperature, optionally in the presence of a hydrogenation catalyst. This process involves preparing the CFC-217ba by the process described above.
摘要翻译：公开了一种制备2-氯-1,1,1,3,3,3-七氟丙烷的方法，其涉及（a）使包含氟化氢，氯和至少一种起始原料的混合物接触，所述起始材料选自的式CX3CCI-CX2的卤代丙烯和式CX3CCIYCX3的卤代丙烷，其中每个X独立地为F或Cl，Y为H，Cl或F（条件是总计X不超过6的X和Y的数目）与反应区中的氯氟化催化剂反应以产生包含CF 3 CClF 3，HCl，HF的产物混合物。和不完全氟化的卤代烃中间体。该方法的特征在于所述氯氟化催化剂包含至少一种含铬组分，其选自（i）α-氧化铬晶格中至少0.05原子％的铬原子被镍取代的结晶α-氧化铬，三价钴或镍和三价钴，条件是α-铬氧化物晶格中不超过2原子％的铬原子被镍代替，并且α-氧化铬晶格中的铬原子的总量被镍和三价钴不超过6原子％，和（ii）（i）的氟化结晶氧化物。还公开了通过在升高的温度下，任选地在氢化催化剂存在下，使包含CFC-217ba和氢的起始混合物在气相中反应制备HFC-227ea和六氟丙烯的混合物的方法。该方法包括通过上述方法制备CFC-217ba。

7. 发明申请

US20130078358A1 STIGMASTEROL-RICH PHYTOSTEROL COMPOSITION AND USE 有权
公开(公告)号：US20130078358A1
公开(公告)日：2013-03-28
申请号：US13423371
申请日：2012-03-19
申请人： Daniel Albert Green , H. David Rosenfeld , Michael Jonathan Doby , Scott Winston , Harry Levine , Louise Slade , Dennis Brooks
发明人： Daniel Albert Green , H. David Rosenfeld , Michael Jonathan Doby , Scott Winston , Harry Levine , Louise Slade , Dennis Brooks
IPC分类号： C07J13/00 , A23G9/04 , C07J75/00
CPC分类号： C07J13/00 , A23G9/045 , A23G9/42 , A23G9/52 , A23G2200/14 , A23L2/52 , A23L33/11 , C07J75/00
摘要： A stigmasterol-rich phytosterol composition is prepared wherein the composition comprises at least 50% stigmasterol, based on the total weight of phytosterols, no more than 1000 ppm water, no more than 50 ppm ethanol, and wherein stigmasterol is at least 98% in the anhydrous form. A ready-to-freeze beverage is provided comprising the stigmasterol-rich composition and water, with optional additives. A frozen beverage is prepared from the ready-to-freeze beverage as a pourable slush. There are further provided processes to prepare the ready-to-freeze beverage and the frozen slush beverage.
摘要翻译：制备富含豆甾醇的植物甾醇组合物，其中所述组合物包含至少50％的豆甾醇，基于植物甾醇的总重量，不超过1000ppm的水，不超过50ppm的乙醇，并且其中豆甾醇在至少98％无水形式。提供包含富含豆甾醇的组合物和水的可冷却饮料和可选的添加剂。冷冻饮料由即将冷冻的饮料制成，作为可倾倒的泥浆。还提供了制备即冻即饮料和冷冻冷冻饮料的方法。

8. 发明授权

US07074973B2 Process for the preparation of 1,1,1,2,2-pentafluoroethane 失效
标题翻译：制备1,1,1,2,2-五氟乙烷的方法
公开(公告)号：US07074973B2
公开(公告)日：2006-07-11
申请号：US10523227
申请日：2003-08-21
申请人： Mario J. Nappa , Velliyur Nott Mallikarjuna Rao , H. David Rosenfeld , Shekhar Subramoney , Munirpallam A. Subramanian , Allen C. Sievert
发明人： Mario J. Nappa , Velliyur Nott Mallikarjuna Rao , H. David Rosenfeld , Shekhar Subramoney , Munirpallam A. Subramanian , Allen C. Sievert
IPC分类号： C07C17/00
CPC分类号： C07C17/206 , B01J23/864 , B01J35/002 , B01J37/0236 , B01J37/03 , B01J37/26 , C07C17/21 , Y02P20/582 , C07C19/08
摘要： A process for the preparation of pentafluoroethane is disclosed which involves contacting a mixture comprising hydrogen fluoride and at least one starting material selected from haloethanes of the formula CX3CHX2 and haloethanes of the formula CX2═CX2, where each X is independently selected from the group consisting of F and Cl (provided that no more than four of X are F), with a fluorination catalyst in a reaction zone to produce a product mixture comprising HF, HCl, pentafluoroethane, underfluorinated halogenated hydrocarbon intermediates and less than 0.2 mole percent chloropentafluoroethane based on the total moles of halogenated hydrocarbons in the product mixture. The process is characterized by the fluorination catalyst comprising (i) a crystalline cobalt-substituted alpha-chromium oxide where from about 0.05 atom % to about 6 atom % of the chromium atoms in the alpha-chromium oxide lattice are replaced by trivalent cobalt (Co+3) and/or (ii) a fluorinated crystalline oxide of (i).
摘要翻译：公开了一种制备五氟乙烷的方法，其涉及将包含氟化氢和至少一种选自式CX 3 CHX 2 2的卤代乙烷的起始物质和式CX 2 -CX 2 X，其中每个X独立地选自F和Cl（条件是不超过四个X为F），与反应区中的氟化催化剂，以产生基于产物混合物中卤代烃总摩尔数的HF，HCl，五氟乙烷，过氟化卤代烃中间体和小于0.2摩尔％氯五氟乙烷的产物混合物。该方法的特征在于氟化催化剂，其包含（i）结晶钴取代的α-氧化铬，其中α-氧化铬晶格中约0.05原子％至约6原子％的铬原子被三价钴（Co （ⅰ））和/或（ⅱ）氟化结晶氧化物。

9. 发明授权

US08920859B2 Stigmasterol-rich phytosterol composition and use 有权
标题翻译：豆甾醇丰富的植物甾醇组成和用途
公开(公告)号：US08920859B2
公开(公告)日：2014-12-30
申请号：US13423371
申请日：2012-03-19
申请人： Daniel Albert Green , H. David Rosenfeld , Michael Jonathan Doby , Scott Winston , Harry Levine , Louise Slade , Dennis Brooks
发明人： Daniel Albert Green , H. David Rosenfeld , Michael Jonathan Doby , Scott Winston , Harry Levine , Louise Slade , Dennis Brooks
IPC分类号： A23B4/03 , A23B4/044 , C07J9/00 , C07J13/00 , A23G9/04 , A23L1/30 , A23L2/52 , A23G9/42 , A23G9/52 , C07J75/00
CPC分类号： C07J13/00 , A23G9/045 , A23G9/42 , A23G9/52 , A23G2200/14 , A23L2/52 , A23L33/11 , C07J75/00
摘要： A stigmasterol-rich phytosterol composition is prepared wherein the composition comprises at least 50% stigmasterol, based on the total weight of phytosterols, no more than 1000 ppm water, no more than 50 ppm ethanol, and wherein stigmasterol is at least 98% in the anhydrous form. A ready-to-freeze beverage is provided comprising the stigmasterol-rich composition and water, with optional additives. A frozen beverage is prepared from the ready-to-freeze beverage as a pourable slush. There are further provided processes to prepare the ready-to-freeze beverage and the frozen slush beverage.
摘要翻译：制备富含豆甾醇的植物甾醇组合物，其中所述组合物包含至少50％的豆甾醇，基于植物甾醇的总重量，不超过1000ppm的水，不超过50ppm的乙醇，并且其中豆甾醇在至少98％无水形式。提供包含富含豆甾醇的组合物和水的可冷却饮料和可选的添加剂。冷冻饮料由即将冷冻的饮料制成，作为可倾倒的泥浆。还提供了制备即冻即饮料和冷冻冷冻饮料的方法。

10. 发明授权

US08017817B2 Process for the preparation of 1,1,3,3,3-pentafluoropropene and 1,2,3,3,3-pentafluoropropene 失效
标题翻译：制备1,1,3,3,3-五氟丙烯和1,2,3,3,3-五氟丙烯的方法
公开(公告)号：US08017817B2
公开(公告)日：2011-09-13
申请号：US11988257
申请日：2006-08-04
申请人： Velliyur Nott Mallikarjuna Rao , H. David Rosenfeld , Allen Capron Sievert , Shekhar Subramoney
发明人： Velliyur Nott Mallikarjuna Rao , H. David Rosenfeld , Allen Capron Sievert , Shekhar Subramoney
IPC分类号： C07C7/00
CPC分类号： B01J37/03 , B01J23/868 , B01J37/0009 , B01J37/26 , C07C17/21 , C07C17/23 , C07C17/25 , C07C21/18 , C07C19/10 , C07C19/08
摘要： A process for the manufacture of CF3CH═CF2 and CF3CF═CHF is disclosed. The process involves (a) reacting HF and chlorine and at least one halopropene of the formula CX3CCI═CCIX (where each X is independently F or Cl) to produce a product including both CF3CCI2CF3 and CF3CCIFCCIF2; (b) reacting CF3CCI2CF3 and CF3CCIFCCIF2 produced in (a) with hydrogen to produce a product including both CF3CH2CF3 and CF3CHFCHF2; (c) dehydrofluorinating CF3CH2CF3 and CF3CHFCHF2 produced in (b) to produce a product including both CF3CH═CF2 and CF3CF═CHF; and (d) recovering CF3CH═CF2 and CF3CF═CHF from the product produced in (c). In (a), both CF3CCI2CF3 and CF3CCIFCCIF2 are produced in the presence of a chlorofluorination catalyst consisting of (i) compositions comprising a crystalline alpha-chromium oxide where at least 0.05 atom % of the chromium atoms in the alpha-chromium oxide lattice are replaced by copper, and (H) compositions of (i) which have been treated with a fluorinating agent.
摘要翻译：公开了制备CF 3 CH 2 CF 2和CF 3 CF = CHF的方法。该方法包括（a）使HF和氯与至少一种式CX3CCI = CCIX的卤代丙烯（其中每个X独立地为F或Cl）反应，以产生包含CF 3 CCl 2 CF 3和CF 3 CClFCCIF 2的产物; （b）使（a）中制备的CF 3 CCl 2 CF 3和CF 3 CClFCCIF 2与氢反应以产生包含CF 3 CH 2 CF 3和CF 3 CHFCHF 2的产物; （c）在（b）中制备的CF 3 CH 2 CF 3和CF 3 CHFCHF 2脱氟化氟化产生包括CF 3 CH 2 CF 2和CF 3 CF = CHF的产物; 和（d）从（c）中制备的产物中回收CF 3CH≡CF2和CF 3 CF = CHF。在（a）中，CF 3 CCl 2 CF 3和CF 3 CClFCCIF 2均在氯氟化催化剂存在下制备，所述氯氟化催化剂由（i）包含α-氧化铬晶格中至少0.05原子％的铬原子的结晶α-氧化铬的组合物组成通过铜和（H）组合物（i）已用氟化剂处理。

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