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1. 发明授权

US4705619A Hydroprocessing with self-promoted molybdenum and tungsten sulfide catalyst 失效
标题翻译：用自身促进的钼和硫化钨催化剂进行加氢处理
公开(公告)号：US4705619A
公开(公告)日：1987-11-10
申请号：US7765
申请日：1987-01-28
申请人： Larry E. McCandlish , Teh C. Ho
发明人： Larry E. McCandlish , Teh C. Ho
IPC分类号： B01J37/08 , C10G45/04 , C10G45/08 , C10G45/50 , C10G47/04 , C10G47/12
CPC分类号： C10G45/04 , B01J37/086
摘要： Hydrocarbon feeds are upgraded by contacting same, at elevated temperature and in the presence of hydrogen, with a self-promoted catalyst prepared by heating one or more water soluble catalyst precursors in a non-oxidizing atmosphere in the presence of sulfur at a temperature of at least about 200.degree. C. The precursors will be one or more compounds of the formula ML(Mo.sub.y W.sub.1-y O.sub.4) wherein M is one or more promoter metals selected from the group consisting essentially of Mn, Fe, Co, Ni, Cu, Zn and mixtures thereof, wherein O.ltoreq.y.ltoreq.1 and wherein L is a nitrogen containing, neutral multidentate, chelating ligand. In a preferred embodiment the ligand L will comprise one or more chelating alkyl di or triamines and the non-oxidizing atmosphere and to form the catalyst will comprise H.sub.2 S.
摘要翻译：通过在升高的温度和在氢的存在下使其接触来提高烃进料与通过在硫的存在下在非氧化性气氛中在一定温度下加热一种或多种水溶性催化剂前体而制备的自促进催化剂至少约200℃。前体将是一种或多种式ML（MoyW1-yO4）的化合物，其中M是一种或多种选自基本上由Mn，Fe，Co，Ni，Cu，Zn和其混合物，其中O y为1，并且其中L为含氮中性多齿螯合配体。在优选的实施方案中，配体L将包含一种或多种螯合烷基二或三胺，并且非氧化性气氛和形成催化剂将包含H 2 S。

2. 发明授权

US4831002A Cr-promoted hydrotreating catalysts 失效
标题翻译： Cr促进加氢处理催化剂
公开(公告)号：US4831002A
公开(公告)日：1989-05-16
申请号：US79247
申请日：1987-07-29
申请人： Teh C. Ho , Larry E. McCandlish , Archie R. Young, II , Edward J. Osterhuber
发明人： Teh C. Ho , Larry E. McCandlish , Archie R. Young, II , Edward J. Osterhuber
IPC分类号： B01J23/85 , B01J27/047 , B01J31/16 , B01J31/18 , B01J37/20 , C10G45/04 , C10G45/08
CPC分类号： B01J31/1616 , B01J23/85 , B01J27/047 , B01J31/1805 , B01J37/20 , C10G45/04 , C10G45/08 , B01J2531/62
摘要： Self-promoted molybdenum and tungsten sulfide hydrotreating catalysts are prepared by heating one or more water soluble catalyst precursors in a non-oxidizing atmosphere in the presence of sulfur at a temperature of at least about 200.degree. C. The precursors are (Cr.sub.x M.sub.1-x L)[Mo.sub.y W.sub.1-y O.sub.4 ].sub.1+.5x wherein M is a divalent promoter metal selected from the group consisting of Mn, Fe, Co, Ni, Cu, Zn and mixtures thereof, x is any value from about 0.2 to 1, y is any value from 0 to 1, and wherein L is a nitrogen-containing, neutral multidentate, chelating ligand. In a preferred embodiment the lligand L will comprise one or more chelating alkyl di- or triamines and the non-oxidizing atmosphere will comprise H.sub.2 S.
摘要翻译：通过在至少约200℃的温度下在硫的存在下在非氧化性气氛中加热一种或多种水溶性催化剂前体来制备自促进的钼和硫化钨加氢处理催化剂。前体是（CrxM1-xL） [MoyW1-yO4] 1 + .5x其中M是选自Mn，Fe，Co，Ni，Cu，Zn及其混合物的二价促进剂金属，x是约0.2至1的任何值，y是任何值为0至1，并且其中L为含氮中性多齿螯合配体。在优选的实施方案中，配体L将包含一种或多种螯合烷基二胺或三胺，非氧化性气氛将包含H 2 S。

3. 发明授权

US4663023A Hydrotreating with self-promoted molybdenum and tungsten sulfide catalyst 失效
标题翻译：用自身促进的钼和硫化钨催化剂加氢处理
公开(公告)号：US4663023A
公开(公告)日：1987-05-05
申请号：US687579
申请日：1984-12-28
申请人： Larry E. McCandlish , Teh C. Ho
发明人： Larry E. McCandlish , Teh C. Ho
IPC分类号： C10G45/08 , B01J27/00 , B01J31/00 , B01J37/08 , C10G45/04 , C10G45/50 , C10G47/04 , C10G47/12
CPC分类号： C10G45/04 , B01J37/086
摘要： Hydrocarbon feeds are upgraded by contacting same, at elevated temperature and in the presence of hydrogen, with a self-promoted catalyst prepared by heating one or more water soluble catalyst precursors in a non-oxidizing atmosphere in the presence of sulfur at a temperature of at least about 200.degree. C. The precursors will be one or more compounds of the formula ML(Mo.sub.y W.sub.1-y O.sub.4) wherein M is one or more promoter metals selected from the group consisting essentially of Mn, Fe, Co, Ni, Cu, Zn and mixtures thereof, wherein O.ltoreq.y.ltoreq.1 and wherein L is a nitrogen containing, neutral multidentate, chelating ligand. In a preferred embodiment the ligand L will comprise one or more chelating alkyl di or triamines and the non-oxidizing atmosphere and to form the catalyst will comprise H.sub.2 S.
摘要翻译：通过在升高的温度和在氢的存在下使其接触来提高烃进料与通过在硫的存在下在非氧化性气氛中在一定温度下加热一种或多种水溶性催化剂前体而制备的自促进催化剂至少约200℃。前体将是一种或多种式ML（MoyW1-yO4）的化合物，其中M是一种或多种选自基本上由Mn，Fe，Co，Ni，Cu，Zn和其混合物，其中O y为1，并且其中L为含氮中性多齿螯合配体。在优选的实施方案中，配体L将包含一种或多种螯合烷基二或三胺，并且非氧化性气氛和形成催化剂将包含H 2 S。

4. 发明授权

US4595672A Method of making self-promoted hydrotreating catalysts 失效
标题翻译：制备自催化加氢处理催化剂的方法
公开(公告)号：US4595672A
公开(公告)日：1986-06-17
申请号：US680379
申请日：1984-12-11
申请人： Teh C. Ho , Larry E. McCandlish
发明人： Teh C. Ho , Larry E. McCandlish
IPC分类号： B01J23/85 , B01J27/047 , B01J31/16 , B01J31/18 , B01J31/22 , B01J37/20 , C10G45/04 , C10G45/08 , B01J27/051 , B01J31/00 , C10G1/06
CPC分类号： B01J31/1616 , B01J23/85 , B01J27/047 , B01J31/1805 , B01J37/20 , C10G45/04 , C10G45/08 , B01J2531/16 , B01J2531/26 , B01J2531/72 , B01J2531/842 , B01J2531/845 , B01J2531/847
摘要： Self-promoted molybdenum and tungsten sulfide hydrotreating catalysts are prepared by heating one or more water soluble catalyst precursors in a non-oxidizing atmosphere in the presence of sulfur at a temperature of at least about 200.degree. C. The precursors will be one or more compounds of the formula ML(Mo.sub.y W.sub.1-y O.sub.4) wherein M is one or more promoter metals selected from the group consisting essentially of Mn, Fe, Co, Ni, Cu, Zn and mixtures thereof, wherein O.ltoreq.y.ltoreq.1 and wherein L is a nitrogen containing, neutral multidentate, chelating ligand. In a preferred embodiment the ligand L will comprise one or more chelating alkyl di or triamines and the non-oxidizing atmosphere will comprise H.sub.2 S.
摘要翻译：通过在至少约200℃的温度下在硫的存在下在非氧化性气氛中加热一种或多种水溶性催化剂前体来制备自促进的钼和硫化钨加氢处理催化剂。前体将是一种或多种化合物其中M是一种或多种选自基本上由Mn，Fe，Co，Ni，Cu，Zn组成的组的助催化剂金属及其混合物，其中O y = 其中L是含氮的中性多齿螯合配体。在优选的实施方案中，配体L将包含一种或多种螯合烷基二或三胺，非氧化性气氛将包含H 2 S。

5. 发明授权

US4851041A Multiphase composite particle 失效
标题翻译：多相复合颗粒
公开(公告)号：US4851041A
公开(公告)日：1989-07-25
申请号：US53267
申请日：1987-05-22
申请人： Richard S. Polizzotti , Larry E. McCandlish
发明人： Richard S. Polizzotti , Larry E. McCandlish
IPC分类号： B22F9/02 , B22F1/00 , B22F9/16 , B22F9/30 , C22C1/05 , C22C1/10 , C22C29/08 , C22C32/00
CPC分类号： C22C29/08 , B22F9/30 , C22C1/053 , C22C1/056
摘要： A compacted, single phase or multiphase composite article. Particles for use in the compacted article are produced by providing a precursor compound containing at least one or at least two metals and a coordinating ligand. The compound is heated to remove the coordinating ligand therefrom and increase the surface area thereof. It may then be reacted so that at least one metal forms a metal-containing compound. The particles may be consolidated to form a compacted article, and for this purpose may be used in combination with graphite or diamonds. The metal-containing compound may be a nonmetallic compound including carbides, nitrides and carbonitrides of a refractory metal, such as tungsten. Th metal-containing compound may be dispersed in a metal matrix, such as iron, nickel or cobalt.

6. 发明授权

US4337232A Ammonia synthesis process using molybdenum oxycarbonitride catalyst 失效
标题翻译：氨合成工艺采用碳氮化钼催化剂
公开(公告)号：US4337232A
公开(公告)日：1982-06-29
申请号：US243824
申请日：1981-03-16
申请人： Larry E. McCandlish , Edwin L. Kugler
发明人： Larry E. McCandlish , Edwin L. Kugler
IPC分类号： B01J23/28 , B01J27/24 , C01B21/082 , C01C1/04 , C07C1/04 , C07C1/10
CPC分类号： C07C1/04 , B01J23/28 , B01J27/24 , C01B21/0828 , C01C1/0411 , C07C1/10 , C01P2002/72 , C01P2002/77 , C01P2002/88 , C01P2006/12 , C07C2527/24 , Y02P20/52
摘要： A process for synthesizing ammonia is described wherein a mixture of nitrogen and hydrogen is contacted with novel molybdenum oxycarbonitride catalyst.
摘要翻译：描述了一种用于合成氨的方法，其中氮和氢的混合物与新的钼碳氮氧化物催化剂接触。

7. 发明授权

US5666631A Metal article and method for producing the same 失效
标题翻译：金属制品及其制造方法
公开(公告)号：US5666631A
公开(公告)日：1997-09-09
申请号：US560126
申请日：1995-11-17
申请人： Richard S. Polizzotti , Larry E. McCandlish , Edwin L. Kugler
发明人： Richard S. Polizzotti , Larry E. McCandlish , Edwin L. Kugler
IPC分类号： C04B35/56 , C22C1/05 , B22F1/02
CPC分类号： C04B35/56 , C04B35/5626 , C22C1/053 , C22C1/056
摘要： A compacted, single phase or multiphase composite article. Particles for use in the compacted article are produced by providing a precursor compound containing at least one or at least two metals and a coordinating ligand. The compound is heated to remove the coordinating ligand therefrom and increase the surface area thereof. It may then be reacted so that at least one metal forms a metal-containing compound. The particles may be consolidated to form a compacted article, and for this purpose may be used in combination with graphite or diamonds. The metal-containing compound may be a nonmetallic compound including carbides, nitrides and carbonitrides of a refractory metal, such as tungsten. The metal-containing compound may be dispersed in a metal matrix, such as iron, nickel or cobalt. The dispersed nonmetallic compound particles are no larger than about 0.1 micron in particle size and have a volume fraction greater than about 0.15 within the metal matrix.
摘要翻译：压实的单相或多相复合制品。用于压实制品的颗粒通过提供含有至少一种或至少两种金属和配位配体的前体化合物来制备。加热化合物以从其中除去配位配体并增加其表面积。然后可以使其反应，使得至少一种金属形成含金属的化合物。颗粒可以被固结以形成压实制品，并且为此目的可以与石墨或菱形组合使用。含金属的化合物可以是包括难熔金属如钨的碳化物，氮化物和碳氮化物的非金属化合物。含金属化合物可以分散在诸如铁，镍或钴的金属基质中。分散的非金属化合物颗粒的粒度不大于约0.1微米，并且在金属基体内具有大于约0.15的体积分数。

8. 发明授权

US5490968A Metal article and method for producing the same (c-2580) 失效
标题翻译：金属制品及其制造方法（c-2580）
公开(公告)号：US5490968A
公开(公告)日：1996-02-13
申请号：US405631
申请日：1995-03-17
申请人： Richard S. Polizzotti , Larry E. McCandlish , Edwin L. Kugler
发明人： Richard S. Polizzotti , Larry E. McCandlish , Edwin L. Kugler
IPC分类号： C04B35/56 , C22C1/05 , B22F3/12
CPC分类号： C04B35/56 , C04B35/5626 , C22C1/053 , C22C1/056
摘要： A compacted, single phase or multiphase composite article. Particles for use in the compacted article are produced by providing a precursor compound containing at least one or at least two metals and a coordinating ligand. The compound is heated to remove the coordinating ligand therefrom and increase the surface area thereof. It may then be reacted so that at least one metal forms a metal-containing compound. The particles may be consolidated to form a compacted article, and for this purpose may be used in combination with graphite or diamonds. The metal-containing compound may be a nonmetallic compound including carbides, nitrides and carbonitrides of a refractory metal, such as tungsten. The metal-containing compound may be dispersed in a metal matrix, such as iron, nickel or cobalt. The dispersed nonmetallic compound particles are no larger than about 0.1 micron in particle size and have a volume fraction greater than about 0.15 within the metal matrix.
摘要翻译：压实的单相或多相复合制品。用于压实制品的颗粒通过提供含有至少一种或至少两种金属和配位配体的前体化合物来制备。加热化合物以从其中除去配位配体并增加其表面积。然后可以使其反应，使得至少一种金属形成含金属的化合物。颗粒可以被固结以形成压实制品，并且为此目的可以与石墨或菱形组合使用。含金属的化合物可以是包括难熔金属如钨的碳化物，氮化物和碳氮化物的非金属化合物。含金属化合物可以分散在诸如铁，镍或钴的金属基质中。分散的非金属化合物颗粒的粒度不大于约0.1微米，并且在金属基体内具有大于约0.15的体积分数。

9. 发明授权

US5352269A Spray conversion process for the production of nanophase composite powders 失效
标题翻译：用于生产纳米相复合粉末的喷雾转化工艺
公开(公告)号：US5352269A
公开(公告)日：1994-10-04
申请号：US734285
申请日：1991-07-09
申请人： Larry E. McCandlish , Bernard H. Kear , Swarn J. Bhatia
发明人： Larry E. McCandlish , Bernard H. Kear , Swarn J. Bhatia
IPC分类号： B01D1/18 , B01J2/00 , B01J8/18 , B22F1/00 , B22F9/02 , B22F9/22 , C01B13/18 , C22C1/05 , B22F9/26
CPC分类号： B82Y30/00 , B01D1/18 , B01J8/1836 , B22F1/0018 , B22F9/026 , B22F9/22 , C01B13/185 , C22C1/056 , B01J2208/00088 , B01J2208/00212 , B01J2208/00407 , B01J2208/0053 , B22F2999/00 , C01P2002/72 , C01P2002/84 , C01P2004/03 , C01P2004/64
摘要： A process is described for the production of composite powders with ultrafine microstructures. The process involves three coordinated steps:1) preparation and mixing of an appropriate starting solution;2) spray drying to form a chemically homogeneous precursor powder; and3) fluid bed thermochemical conversion of the precursor into the desired nanophase composite powder.Both spray drying and fluid bed conversion are scaleable technologies, and together provide the means for producing bulk quantities of nanophase composite powders at low manufacturing cost. Processing parameters are controlled to ensure maintenance of chemical and microstructural uniformity at the nanoscale (less than 0.1 micron) level.Spray conversion processing is a versatile technology, which can be applied to a variety of metal--metal (e.g. W--Cu), ceramic-metal (e.g. WC--Co), and ceramic--ceramic (e.g. Al.sub.2 O.sub.3 --SiO.sub.2) nanophase composite powders ceramic-metal (e.g. WC--Co), and ceramic--ceramic (e.g. Al.sub.2 O.sub.3 --SiO.sub.2) nanophase composite powders.
摘要翻译：描述了用于生产具有超细微结构的复合粉末的方法。该过程涉及三个协调步骤：1）制备和混合适当的起始溶液; 2）喷雾干燥以形成化学均匀的前体粉末; 和3）流化床将前体热化学转化成所需的纳米相复合粉末。喷雾干燥和流化床转化都是可扩展的技术，并且一起提供了以低制造成本生产大量纳米相复合粉末的方法。控制加工参数以确保纳米级（小于0.1微米）水平下的化学和微结构均匀性的维持。喷雾转化处理是一种多功能技术，可应用于各种金属（如W-Cu），陶瓷 - 金属（如WC-Co）和陶瓷陶瓷（如Al2O3-SiO2）纳米相复合粉末陶瓷金属（例如WC-Co）和陶瓷陶瓷（如Al2O3-SiO2）纳米相复合粉末。

10. 发明授权

US4426366A Novel molybdenum oxycarbonitride compositions 失效
标题翻译：新型钼碳氮化物组合物
公开(公告)号：US4426366A
公开(公告)日：1984-01-17
申请号：US372486
申请日：1982-04-28
申请人： Larry E. McCandlish , Larissa W. Turaew
发明人： Larry E. McCandlish , Larissa W. Turaew
IPC分类号： B01J23/28 , B01J27/24 , C01B21/082 , C01C1/04 , C07C1/04 , C07C1/10 , C01C3/00
CPC分类号： C07C1/04 , B01J23/28 , B01J27/24 , C01B21/0828 , C01C1/0411 , C07C1/10 , C01P2002/72 , C01P2002/77 , C01P2002/88 , C01P2006/12 , C07C2527/24 , Y02P20/52
摘要： Novel molybdenum oxycarbonitride compositions are described together with a general method of synthesis. The compositions can be obtained by the relatively low temperature thermal decomposition of an amine molybdate and can be amorphous, poorly crystalline, or substantially crystalline, and can unexpectedly possess high surface areas in the region of about 60 to 130 m.sup.2 /g and higher. The compositions have the general formula: MoO.sub.a C.sub.b N.sub.c, where a, b and c are non-zero decimal values and the sum: a+b+c, is less than or equal to about one, as evidenced by X-ray diffraction and chemical analyses. The compositions are useful as abrasives, as for removing oxide coatings from metals.
摘要翻译：新型钼碳氮氧化物组合物与一般合成方法一起描述。组合物可以通过钼酸铵的相对低温热分解获得，并且可以是无定形的，结晶性差的或基本上结晶的，并且可以意外地在约60至130m 2 / g和更高的区域中具有高表面积。组合物具有以下通式：MoOaCbNc，其中a，b和c是非零十进制值，并且总和：a + b + c小于或等于约1，如X射线衍射和化学分析所证明。组合物可用作研磨剂，用于从金属中除去氧化物涂层。

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