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    • 5. 发明授权
    • Apparatus for purifying crystals
    • 晶体净化装置
    • US4588562A
    • 1986-05-13
    • US631443
    • 1984-07-16
    • Shigeru SaitohMasaaki ShimadaTakeshi Imura
    • Shigeru SaitohMasaaki ShimadaTakeshi Imura
    • B01D9/02B01D9/00
    • B01D9/004
    • Crystals containing a molten liquid at the bottom of a purifying tower are cooled, so that three effects i.e., washing, sweating and recrystallization are improved while maintaining a heat balance within a tower to thereby obtain highly pure crystals. The apparatus according to this invention comprises a crystal purifying tower of a transversal cross sectional configuration in which two circles are partially joined to each other and in which a stirrer having blade members spirally attached around the surface of a rotational shaft is disposed at the center for each of the circles, the purifying tower having a starting material feed means about at the middle thereof, a heating means and a product take out port at the upper portion thereof, a cooled crystal feed means, a low purity crystal component take out means and a means for extracting a portion of the crystal component at low purity out of the system at the bottom thereof, wherein the crystal component at low purity taken out by the low purity crystal component take out means is crystallized and then cooled by a means disposed outside the purifying tower for crystallizing and then cooling the crystal component at low purity, and the crystals thus crystallized and then cooled are fed by means of the cooled crystal feed means to the purifying tower.
    • 在净化塔底部含有熔融液体的晶体被冷却,从而提高洗涤,出汗和重结晶三个效果,同时保持塔内的热平衡,从而获得高纯度的晶体。 根据本发明的装置包括横截面构造的晶体净化塔,其中两个圆部彼此部分地接合,并且其中具有围绕旋转轴的表面螺旋地附接的叶片构件的搅拌器设置在中心处 每个圆圈,净化塔具有大约在其中间的起始原料进料装置,加热装置和在其上部的产物取出口,冷却的晶体进料装置,低纯度的晶体组分取出装置和 在底部从系统中提取低纯度的部分晶体成分的方法,其中由低纯度晶体组分取出的低纯度晶体成分取出装置结晶,然后通过设置在外部的装置冷却 用于结晶并然后以低纯度冷却结晶组分的纯化塔,然后使晶体结晶然后冷却 通过冷却的晶体进料装置进料到净化塔。