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    • 3. 发明授权
    • Soft X-ray microscope
    • 软X射线显微镜
    • US5434901A
    • 1995-07-18
    • US162470
    • 1993-12-07
    • Komei NagaiYoshiaki HorikawaYoshinori IketakiShoichiro Mochimaru
    • Komei NagaiYoshiaki HorikawaYoshinori IketakiShoichiro Mochimaru
    • G21K7/00
    • G21K7/00
    • In a soft X-ray microscope including a soft X-ray source for emitting soft X-rays, a condenser lens for focusing the soft X-rays onto a specimen under inspection, an objective lens for focusing soft X-rays emanating from the specimen, a soft X-ray detector for receiving the soft X-rays focused by the objective lens, and a visually observing optical system for forming a visible image of the specimen by converting an optical property of the specimen other than contrast and color into a contrast in brightness or color. The visually observing optical system may be formed as phase contrast microscope, dark field microscope, polarizing microscope, differential interference microscope, or fluorescent microscope. Then, alignment and focus adjustment can be performed by observing the visible image of the specimen without irradiating the specimen with the soft X-rays even if the specimen has substantially no contrast and color.
    • 在包括用于发射软X射线的软X射线源的软X射线显微镜中,用于将软X射线聚焦到检查样本上的聚光透镜,用于聚焦从样本发出的软X射线的物镜 用于接收由物镜聚焦的软X射线的软X射线检测器,以及用于通过将除了对比度和颜色之外的样本的光学性质转换成对比度而形成样本的可见图像的目视观察光学系统 亮度或颜色。 视觉观察光学系统可以形成为相差显微镜,暗视野显微镜,偏光显微镜,微分干涉显微镜或荧光显微镜。 然后,即使样本基本上没有对比度和颜色,也可以通过观察样本的可见图像而不用软X射线照射样本来进行对准和聚焦调整。
    • 4. 发明授权
    • Sample vessel for X-ray microscopes
    • X射线显微镜样品容器
    • US5528646A
    • 1996-06-18
    • US425233
    • 1995-04-18
    • Yoshinori IketakiShoichiro MochimaruYoshiaki HorikawaKomei Nagai
    • Yoshinori IketakiShoichiro MochimaruYoshiaki HorikawaKomei Nagai
    • G21K7/00
    • G21K7/00
    • A sample vessel for X-ray microscopes comprising a first silicon base plate having an entrance window covered with a thin film of silicon nitride, and a second silicon base plate which has an exit window covered with a thin film of silicon nitride and matched with the entrance window. The second silicon base plate being connected the first base plate by way of a spacer so as to form a sealed space capable of accommodating samples to be observed. Disposed in the space is a mesh member made of a wire material having an angle of contact with water smaller than 90.degree. at a location adjacent to the thin film of silicon nitride covering the entrance window or a thin film of aluminium is evaporation-coated over the thin film of silicon nitride. This sample vessel makes it possible to enhance mechanical strength of the thin film of silicon nitride and limits shifting of samples within very narrow ranges with water films formed in meshes of the mesh member, thereby remarkably facilitating observation of the samples with X-rays and soft X-rays.
    • 一种用于X射线显微镜的样品容器,包括具有覆盖有氮化硅薄膜的入口窗口的第一硅基板和具有覆盖有氮化硅薄膜的出射窗口的第二硅基板,并与 入口窗口 第二硅基板通过间隔件连接第一基板,以便形成能够容纳观察样品的密封空间。 在该空间中设置的是由与覆盖入口窗口的氮化硅薄膜相邻的位置处的与水接触的角度小于90°的网状构件,或者薄膜的铝被蒸发涂覆 氮化硅薄膜。 该样品容器使得可以提高氮化硅薄膜的机械强度,并且通过在网状构件的网眼中形成的水​​膜限制样品在非常窄的范围内的移动,从而显着地促进了用X射线和软的样品的观察 X光片。
    • 5. 发明授权
    • Device for detecting X-rays
    • 用于检测X射线的装置
    • US5352897A
    • 1994-10-04
    • US31470
    • 1993-03-15
    • Yoshiaki HorikawaYoshinori IketakiShoichiro MochimaruKoumei Nagai
    • Yoshiaki HorikawaYoshinori IketakiShoichiro MochimaruKoumei Nagai
    • G01T1/24H01L27/146H01L31/115
    • H01L27/14665G01T1/24H01L27/146H01L31/115
    • A soft X-ray detector includes a surface electrode layer, a photoelectric conversion layer, and a semiconductor detector having an electrode connected to the photoelectric conversion layer, for detecting an electric charge produced In the photoelectric conversion layer. The photoelectric conversion layer and the surface electrode layer have thicknesses satisfying conditionsdA.gtoreq.0.183.lambda./KAdB.ltoreq.0.183.lambda./KBwhere dA is a thickness of the photoelectric conversion layer, dB is a thickness of the surface electrode layer, KA is an extinction coefficient of radiation of a wavelength .lambda. in a substance constituting the photoelectric conversion layer, and KB is an extinction coefficient of radiation of the wavelength .lambda.in a substance constituting the surface electrode layer. Thus, the soft X-ray detector has a high sensitivity to soft X rays and a lower sensitivity to visible light, so that only soft X rays can be selectively detected. Further, the detector has two kinds of pixels, with one kind sensitive to soft X-rays and the other kind sensitive to visible light. In addition, the detector includes a plurality of pixels, to which the surface electrode layer is divided to correspond so that it has a plurality of regions to obtain a desired wavelength.
    • 软X射线检测器包括表面电极层,光电转换层和具有连接到光电转换层的电极的半导体检测器,用于检测在光电转换层中产生的电荷。 光电转换层和表面电极层具有满足条件dA> / =0.183λ/ KA dB
    • 7. 发明授权
    • Method of microscopic observation
    • 显微镜观察方法
    • US06184535B2
    • 2001-02-06
    • US09156775
    • 1998-09-18
    • Shingo KashimaYoshinori Iketaki
    • Shingo KashimaYoshinori Iketaki
    • G01N2164
    • G01N21/6458G01N21/6428G01N2021/6419G02B21/002G02B21/16
    • In a method of observing a specimen through a fluorescence microscope, molecules that could cause double-resonance absorption process in an appropriate manner are used to dye the specimen, and the specimen is irradiated with a plurality of light beams of different wavelengths in a good timing, so that a microscopic image with high spatial resolution is obtained. In the microscope to be used in the method of observation, the specimen is irradiated with two light beams of different wavelength bands via an aperture with an annular-zonal structure and an optical system that has different in-focus positions for these two wavelength bands, so that one of the two light beam is focused on a surface of the specimen and the other light beam is defocused thereon. Consequently, the microscope achieves improvement of the spatial resolution as to overcome the diffraction limit determined by the wavelengths in use.
    • 在通过荧光显微镜观察样品的方法中,使用可以以适当的方式引起双共振吸收过程的分子染色样品,并且以良好的时间用多个不同波长的光束照射样品 ,从而获得具有高空间分辨率的显微图像。在用于观察方法的显微镜中,通过具有环形区域结构和光学系统的孔径,用两个不同波长带的光束照射样品 对于这两个波长带具有不同的对焦位置,使得两个光束中的一个被聚焦在样本的表面上,并且另一个光束在其上散焦。 因此,显微镜实现空间分辨率的提高,以克服由使用的波长确定的衍射极限。
    • 9. 发明授权
    • Microscope with wavelength compensation
    • 具有波长补偿的显微镜
    • US07095556B2
    • 2006-08-22
    • US10771729
    • 2004-02-04
    • Yoshinori IketakiTakeshi WatanabeMasaaki FujiiYasunori IgasakiToshio Suzuki
    • Yoshinori IketakiTakeshi WatanabeMasaaki FujiiYasunori IgasakiToshio Suzuki
    • G02B21/06G01J3/30
    • G02B26/08
    • A microscope capable of being shaped into a beam with complete hollow shape by removing the disorder of the wavefront to the erase light, particularly, and capable of improving the spatial resolution by inducing a super-resolution near the limit, is provided. In the microscope, wherein a first light to excite a molecule from a ground-state to first electron excited state or a second light to excite the molecule from the first electron excited state to the second electron excited state with higher energy level, for a sample 56 including the molecule with three electronic states including at least a ground-state, are spatial phase-modulated into the prescribed beam shape, and parts of these first light and the second light are overlapped and focused to detect luminescence from the sample 56, a wavefront compensation means 61 is provided in the optical path of the first light and/or in the optical path of the second light, and the wavefront aberration caused in the first light and/or in the second light, is removed by the wavefront compensation means 61.
    • 提供了能够通过将擦除光的波阵面除去特别是并且能够通过在接近极限附近引起超分辨率来改善空间分辨率而将具有完全中空形状的光束成形为显微镜的显微镜。 在显微镜中,其中将分子从基态激发到第一电子激发态的第一光或第二光以将分子从第一电子激发态激发至具有较高能级的第二电子激发态,对于样品 包括具有至少包括基态的三种电子状态的分子被空间相位调制成规定的波束形状,并且这些第一光和第二光的一部分被重叠和聚焦以检测来自样品56的发光, 波前补偿装置61设置在第一光的光路和/或第二光的光路中,并且在第一光和/或第二光中引起的波前像差被波前补偿装置除去 61。