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1. 发明授权

US06663851B1 Surface-modified titanium dioxide 有权
标题翻译：表面改性二氧化钛
公开(公告)号：US06663851B1
公开(公告)日：2003-12-16
申请号：US09606202
申请日：2000-06-29
申请人： Klaus Deller , Dieter Kerner , Juergen Meyer
发明人： Klaus Deller , Dieter Kerner , Juergen Meyer
IPC分类号： A61K742
CPC分类号： G03G9/09708 , A61K8/29 , A61Q17/04 , C01P2006/10 , C01P2006/12 , C08K3/22 , C08K9/06 , C08K2003/2237 , C09C1/3684 , C09D7/62 , C09G1/02 , C09K3/1436 , C08L83/04
摘要： A product obtained by treating surface-modified, pyrogenically produced titanium dioxide with at least one ammonium-functional silane, such as by spraying the pyrogenically produced titanium dioxide with the at least one silane, alone or in ethanol solution, and tempering, and useful in the field of cosmetics in sunblocks, in toner powders, in paints and varnishes, in silicone rubber, as abrasives and polishes, for example, in the field of CMP.
摘要翻译：通过用至少一种铵官能硅烷处理表面改性的热解法生产的二氧化钛获得的产物，例如通过用至少一种硅烷单独或在乙醇溶液中喷雾热解产生的二氧化钛，并回火，并用于例如在CMP领域中的防晒霜，调色剂粉末，油漆和清漆中的化妆品领域，硅橡胶中的研磨剂和抛光剂。

2. 发明授权

US5776240A Granules based on pyrogenically prepared silicon dioxide, methods for their preparation and use thereof 失效
标题翻译：基于热解法制备的二氧化硅的颗粒，其制备方法和用途
公开(公告)号：US5776240A
公开(公告)日：1998-07-07
申请号：US597893
申请日：1996-02-05
申请人： Klaus Deller , Helmfried Krause , Juergen Meyer , Dieter Kerner , Hans Lansink-Rotgerink , Werner Hartmann
发明人： Klaus Deller , Helmfried Krause , Juergen Meyer , Dieter Kerner , Hans Lansink-Rotgerink , Werner Hartmann
IPC分类号： B01J2/10 , B01J21/08 , B01J35/10 , C01B33/12 , C01B33/18 , C08F4/00 , C08F4/02 , C08F4/60 , C08F4/64 , C08F10/00 , C08F10/02 , C09C1/30 , C04B14/04
CPC分类号： B01J21/08 , B01J35/0026 , B01J35/023 , B01J35/1014 , B01J35/1019 , B01J35/1042 , B01J35/1047 , B01J35/108 , C01B33/12 , C09C1/3027 , C09C1/3036 , C09C1/3081 , C01P2004/62 , C01P2006/12
摘要： Granules based on silicon dioxide and having the properties: Average particle size: 10 to 120 .mu.m BET surface area: 40 to 400 m.sup.2 /g Pore volume: 0.5 to 2.5 ml/g Pore size distribution: less than 5% of the total pore volume exists of pores with a diameter
摘要翻译：基于二氧化硅的颗粒，具有以下性质：平均粒径：10〜120μmBET表面积：40〜400m2 / g孔体积：0.5〜2.5ml / g孔径分布：小于总孔的5％体积存在直径小于5nm的孔，余数为中孔和大孔pH值：3.6至8.5抽头密度：220至700g / l它们通过将二氧化硅分散在水中，喷雾干燥和任选地加热和/ 或硅烷化。颗粒可用作催化剂载体。

3. 发明授权

US06455455B1 Silicon-aluminum mixed oxide 失效
标题翻译：硅铝混合氧化物
公开(公告)号：US06455455B1
公开(公告)日：2002-09-24
申请号：US09560190
申请日：2000-04-28
申请人： Klaus Deller , Rainer Golchert , Dieter Kerner , Helmut Mangold
发明人： Klaus Deller , Rainer Golchert , Dieter Kerner , Helmut Mangold
IPC分类号： C04B3510
CPC分类号： B82Y30/00 , C01B33/183 , C01F7/02 , C01F7/302 , C01P2002/02 , C01P2002/60 , C01P2002/72 , C01P2004/04 , C01P2004/50 , C01P2004/62 , C01P2004/64 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/22 , C09K3/1409
摘要： A silicon-aluminum mixed oxide produced by flame hydrolysis and having a composition of from 1 to 99.999 wt. % Al2O3, the remainder being SiO2, which mixed oxide exhibits an amorphous structure in the X-ray diffraction pattern and consists of intergrown primary particles, and in these primary particles crystallites are present. These crystallites having sizes of between one and 200 namometers and the specific surface of the powder being between 5 and 300 m2/g. These products are produced by a process wherein silicon halide and aluminum halide are vaporized in a particular ratio to one another and are homogeneously mixed with air, oxygen and hydrogen in a mixing unit by means of any carrier gas, this mixture undergoes combustion in a burner of known construction and, after the separation of the solids from the vapour phase, any traces of halide possibly adhering to the product are separated off in a further processing step by means of moist air at elevated temperature. The silicon-aluminum mixed oxide produced by flame hydrolysis are used in the form of dispersions for polishing, in particular in the electronics industry (CMP).
摘要翻译：通过火焰水解制备的硅铝混合氧化物，其组成为1至99.999wt。％Al 2 O 3，其余为SiO 2，该混合氧化物在X射线衍射图中呈现无定形结构并且由共生的一次粒子组成，并且在这些一次粒子中存在微晶。这些微晶的尺寸为1至200纳米，粉末的比表面积为5至300平方米/克。这些产品通过一种方法生产，其中卤化硅和卤化铝以特定比例彼此蒸发，并通过任何载气在混合单元中与空气，氧气和氢气均匀混合，该混合物在燃烧器中燃烧已知的结构，并且在从气相中分离出固体之后，任何痕量的可能附着在产品上的卤化物在另外的加工步骤中通过在高温下的潮湿空气分离出来。通过火焰水解生产的硅铝混合氧化物以抛光用分散体的形式使用，特别是在电子工业（CMP）中。

4. 发明授权

US06303256B1 Toners and/or toner mixtures 有权
公开(公告)号：US06303256B1
公开(公告)日：2001-10-16
申请号：US09703864
申请日：2000-11-02
申请人： Dieter Kerner , Helmut Mangold , Juergen Meyer
发明人： Dieter Kerner , Helmut Mangold , Juergen Meyer
IPC分类号： G03G9097
CPC分类号： G03G9/09708 , G03G9/09716
摘要： A toner or a mixture of toners, comprises a pyrogenically synthesized alumina-silica mixed oxide as a component in combination with other components necessary to complete a toner formulation. The surface of the mixed alumina-silica oxide material.

5. 发明授权

US06197469B1 Toners and/or toner mixtures 有权
标题翻译：调色剂和/或调色剂混合物
公开(公告)号：US06197469B1
公开(公告)日：2001-03-06
申请号：US09461752
申请日：1999-12-16
申请人： Dieter Kerner , Helmut Mangold , Juergen Meyer
发明人： Dieter Kerner , Helmut Mangold , Juergen Meyer
IPC分类号： G03G9097
CPC分类号： G03G9/09708 , G03G9/09716
摘要： A toner or a mixture of toners, comprises a pyrogenically synthesized alumina-silica mixed oxide as a component in combination with other components necessary to complete a toner formulation. The surface of the mixed alumina-silica oxide material.
摘要翻译：调色剂或调色剂的混合物包含热解合成的氧化铝 - 二氧化硅混合氧化物作为与完成调色剂配方所必需的其它组分组合的组分。混合氧化铝 - 二氧化硅材料的表面。

6. 发明申请

US20080139721A1 Surface-modified, doped, pyrogenically produced oxides 审中-公开
标题翻译：表面改性，掺杂，热解产生的氧化物
公开(公告)号：US20080139721A1
公开(公告)日：2008-06-12
申请号：US11980756
申请日：2007-10-31
申请人： Dieter Kerner , Helmut Mangold , Jurgen Meyer
发明人： Dieter Kerner , Helmut Mangold , Jurgen Meyer
IPC分类号： C08K3/22
CPC分类号： C09C3/12 , C01P2006/10 , C01P2006/12 , C01P2006/19 , C09C1/3081 , C09C1/3653 , C09C1/3684 , Y10T428/2991 , Y10T428/2995
摘要： Surface-modified, doped, pyrogenically produced oxides surface-modified with one or several compounds from the following groups: a) Organosilanes of the type (RO)3Si(CnH2n+1), (RO)3Si(CnH2n−1) b) R′x(RO)ySi(CnH2n+1), (RO)3Si(CnH2n+1) c) X3Si(CnH2n+1), X3Si(CnH2n−1) d) X2(R′)Si(CnH2n+1), X2(R′)Si(CnH2n−1) e) X(R′)2Si(CnH2n+1), X(R′)2Si(CnH2n−1) f) (RO)3Si(CH2)m—R′, g) (R″)x(RO)ySi(CH2)m—R′, h) X3Si(CH2)m—R′, i) (R)X2Si(CH2)m—R′, j) (R)2XSi(CH2)m—R′, k) Silazanes of the type l) Cyclic polysiloxanes, m) Polysiloxanes or silicone oils.
摘要翻译：表面改性，掺杂，热解产生的氧化物用一种或几种来自以下组的化合物进行表面改性：a）类型（RO）3 Si（C n） H 2 n + 1），（RO）3 Si（C n H 2n-1）b）R （RO）y y y y y>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>> 3 Si（C n H 2n + 1）c）X 3 Si（C n H n） H 2n + 1），X 3 Si（C n H 2n-1）d）X _{-R'，j）（R）2 XSi（CH 2）m -R a，k）1）的硅氮烷， C 聚硅氧烷，m）聚硅氧烷或硅油。}

7. 发明申请

US20060155052A1 Pyrogenically produced silicondioxide powder 有权
标题翻译：热解产生的二氧化硅粉末
公开(公告)号：US20060155052A1
公开(公告)日：2006-07-13
申请号：US11084170
申请日：2005-03-21
申请人： Kai Schumacher , Dieter Kerner , Roland Schilling , Juergen Flesch , Thomas Schiener
发明人： Kai Schumacher , Dieter Kerner , Roland Schilling , Juergen Flesch , Thomas Schiener
IPC分类号： C08L83/04 , C08K3/36 , C08L67/00 , C01B33/12
CPC分类号： C01B33/18 , C01B33/183 , C01P2004/64 , C01P2006/12 , C09C1/30
摘要： Pyrogenically produced silicon dioxide powder in the form of aggregates of primary particles having a BET surface area of 200±25 m2/g, wherein the aggregates display an average surface area of 7000 to 12000 nm2, an average equivalent circle diameter (ECD) of 80 to 100 nm and an average circumference of 850 to 1050 nm. It is produced by a pyrogenic process in which silicon tetrachloride and a second silicon component comprising H3SiCl, H2SiCl2, HSiCl3, CH3SiCl3, (CH3)2SiCl2, (CH3)3SiCl and/or (n-C3H7)SiCl3 are mixed with primary air and a combustion gas and burnt into a reaction chamber, secondary air also being introduced into the reaction chamber, and the feed materials being chosen such that an adiabatic flame temperature of 1570 to 1630° C. is obtained. It can be used as a filler.
摘要翻译：以BET表面积为200±25m 2 / g的一次粒子的聚集体的形式的热解生成的二氧化硅粉末，其中聚集体的平均表面积为7000〜12000nm， 2，平均当量圆直径（ECD）为80〜100nm，平均周长为850〜1050nm。它是通过热原法制造的，其中四氯化硅和包含H 3 SiCl，H 2 SiCl 2，HSiCl 3＆gt;与一次空气和燃烧气体混合并燃烧到反应室中，二次空气也被引入反应室，并且进料选择为使绝热火焰温度为1570至1630℃ C.得到。它可以用作填料。

8. 发明授权

US6083859A Boron oxide-silicon dioxide mixed oxide 失效
标题翻译：氧化硼 - 二氧化硅混合氧化物
公开(公告)号：US6083859A
公开(公告)日：2000-07-04
申请号：US878824
申请日：1997-06-19
申请人： Helmut Mangold , Manfred Ettlinger , Dieter Kerner , Peter Kleinschmit
发明人： Helmut Mangold , Manfred Ettlinger , Dieter Kerner , Peter Kleinschmit
IPC分类号： C01B35/10 , C03C1/00 , C03C3/04
CPC分类号： C03C1/00 , C01B35/10 , C01P2006/12
摘要： A boron oxide-silicon dioxide mixed oxide which has a BET surface of less than 100 m.sup.2 g, and optionally containing oxides of aluminium, titanium or zirconium, is prepared pyrogenically by flame hydrolysis. The mixed oxide is used in glass making.
摘要翻译：通过火焰水解热原制备具有小于100m 2 g的BET表面和任选地含有铝，钛或锆的氧化物的氧化硼 - 二氧化硅混合氧化物。混合氧化物用于制造玻璃。

9. 发明授权

US5672330A Flame-hydrolytically produced titanium dioxide mixed oxide method of its production and its use 失效
标题翻译：火焰水解生产的二氧化钛混合氧化法的生产及其应用
公开(公告)号：US5672330A
公开(公告)日：1997-09-30
申请号：US423349
申请日：1995-04-18
申请人： Werner Hartmann , Helmut Mangold , Dieter Kerner
发明人： Werner Hartmann , Helmut Mangold , Dieter Kerner
IPC分类号： B01J21/06 , B01J21/12 , B01J32/00 , B01J35/02 , B01J37/08 , C01B33/18 , C01F7/02 , C01G23/00 , C01G23/04 , C01G23/07 , C04B35/46 , C08F4/16 , C01G23/047
CPC分类号： B01J21/063 , B01J21/12 , B01J37/088 , C01G23/003 , C01G23/07 , C04B35/46 , C01P2006/12 , C01P2006/13
摘要： Flame-hydrolytically produced titanium dioxide mixed oxide having a BET surface of 10 to 150 m.sup.2 /g and 1 to 30% by weight aluminum oxide or 1 to 30% by weight silicon dioxide is produced by evaporating aluminum chloride or silicon tetrachloride, transferring the evaporated aluminum chloride or silicon tetrachloride, together with an inert gas, into the mixing chamber of a burner, mixing them with hydrogen, air and gaseous titanium tetrachloride, burning the resulting 4-component mixture in the reaction chamber of the burner, and separating the titanium dioxide mixed oxide from the gaseous reaction products.
摘要翻译：通过蒸发氯化铝或四氯化硅来制造BET表面积为10〜150m2 / g和1〜30％（重量）氧化铝或1〜30％（重量）二氧化硅的火焰水解制备的二氧化钛混合氧化物，氯化铝或四氯化硅与惰性气体一起进入燃烧器的混合室，将其与氢气，空气和气态四氯化钛混合，将所得的四组分混合物燃烧在燃烧器的反应室中，并将钛来自气态反应产物的二氧化硅混合氧化物。

10. 发明授权

US5034207A Finely, divided, precipitated silica with high structure, method of its preparation and use 失效
标题翻译：精细分散，沉淀二氧化硅结构高，制备方法齐全
公开(公告)号：US5034207A
公开(公告)日：1991-07-23
申请号：US542809
申请日：1990-06-22
申请人： Dieter Kerner , Adolf Wagner , Felix Schmidt , Dietrich Bauer
发明人： Dieter Kerner , Adolf Wagner , Felix Schmidt , Dietrich Bauer
IPC分类号： C01B33/187 , C01B33/193 , C09C1/30 , C09D7/00
CPC分类号： C09C1/30 , C01B33/193 , C09C1/3027 , C09D7/005 , C01P2004/51 , C01P2004/61 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/19 , C01P2006/82
摘要： Finely divided precipitated silica for use as a delustering agent with high structure and a______________________________________ BET surface (DIN 66 132) of 150 to 350 m.sup.2 /g Stamping density (DIN 53 194) between 60 and 120 g/l DBP absorption number between 3.0 and 4.0 ml/g Particle size distribution at least 70% from 1 to 6 .mu.m ______________________________________ can be prepared by heating a mixture of water and sodium silicate under agitation to a temperature of 70.degree. to 80.degree. C., adding concentrated sulfuric acid into this mixture until half of the alkali present has been neutralized, shearing the reaction mixture and optionally raising the temperature at the same time to 86.degree..+-.5.degree. C. Concentrated sulfuric acid is added after a period of 30 to 120 minutes at a rather high rate until the pH of the silica suspension produced is 3.0 to 3.5. The resulting silica suspension is ultimately filtered off by known filter devices, the silica filter cake washed free of sulfate, and a dry product is ultimately obtained.
摘要翻译：精细分离的沉淀二氧化硅用作具有高结构的消光剂和150至350m 2 / g的-BET表面（DIN 66 132） - 冲压密度（DIN 53 194），介于60至120g / l -DBP吸收数之间 3.0和4.0ml / g - 粒度分布至少70％，从1至-6μm可以通过在搅拌下将水和硅酸钠的混合物加热到70℃至80℃的温度，加入浓缩将硫酸加入到该混合物中，直到存在的一半碱已经被中和，剪切反应混合物并任选地将温度升高至86℃+/- 5℃。在30至120℃加入浓硫酸分钟，直到产生的二氧化硅悬浮液的pH为3.0〜3.5。所得二氧化硅悬浮液最终通过已知的过滤装置过滤，二氧化硅滤饼洗涤无硫酸盐，最终获得干燥产物。

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