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    • 5. 发明授权
    • Pyrogenic silicon dioxide powder and dispersion thereof
    • 热解二氧化硅粉末及其分散体
    • US07534409B2
    • 2009-05-19
    • US10549929
    • 2004-03-15
    • Kai SchumacherDieter Kerner
    • Kai SchumacherDieter Kerner
    • C01B33/12
    • B41M5/5218B01J21/08B01J35/002B01J35/0026B01J35/023B01J35/1009B01J35/1023B01J37/0072B01J37/086C01B33/1417C01B33/183C01P2004/62C01P2006/10C01P2006/12C01P2006/19C01P2006/22C01P2006/80C01P2006/90C09D17/007C09G1/02
    • Pyrogenically produced silicon dioxide powder with a specific surface area of between 5 and 600 m2/g and a carbon content of less than 500 ppm, which displays a specific dibutyl phthalate absorption of less than or equal to 1.2 g dibutyl phthalate/100 g SiO2 per m2 of specific surface area and a specific thickening action of less than 15 mPas/m2 of specific surface area. It is produced by supplying vaporous tetramethoxysilane and/or tetraethoxysilane together with air and separately hydrogen to a burner, and allowing the mixture of gases to react in a flame in a reaction chamber connected in series to the burner, and separating the solid reaction product from the gas stream by known means, the lambda value in the burner being between 0.95 and 1.5 and sufficient secondary air also being supplied to the reaction chamber that the lambda value in the reaction chamber is between 0.8 and 1.6. The invention also provides a dispersion containing the silicon dioxide powder and the use of the powder and of the dispersion.
    • 热塑性二氧化硅粉末的比表面积为5〜600m2 / g,碳含量小于500ppm,其特征在于邻苯二甲酸二丁酯的吸收值小于或等于1.2g邻苯二甲酸二丁酯/ 100g SiO 2 m2的比表面积和比表面积小于15mPas / m 2的比增稠作用。 它是通过将空气四甲氧基硅烷和/或四乙氧基硅烷与空气和单独的氢气一起向燃烧器供应的,并且允许气体混合物在与燃烧器串联连接的反应室中的火焰中反应,并将固体反应产物从 通过已知方式的气流,燃烧器中的λ值在0.95和1.5之间,并且足够的二次空气也被供应到反应室,反应室中的λ值在0.8和1.6之间。 本发明还提供了含有二氧化硅粉末的分散体以及粉末和分散体的用途。
    • 6. 发明授权
    • Pyrogenically produced silicon dioxide powder and silicone sealing compound containing this powder
    • 热解产生的二氧化硅粉末和含有这种粉末的硅氧烷密封化合物
    • US07439298B2
    • 2008-10-21
    • US11084022
    • 2005-03-21
    • Kai SchumacherDieter KernerUwe DienerMario Scholz
    • Kai SchumacherDieter KernerUwe DienerMario Scholz
    • C08K3/34
    • C08K3/36C01B33/183C09K3/1018C08L83/04C08L21/00
    • Pyrogenically produced silicon dioxide powder in the form of aggregates of primary particles having a BET surface area of 150±15 m2/g, wherein the aggregates display an average surface area of 12000 to 20000 nm2, an average equivalent circle diameter (ECD) of 90 to 120 nm and an average circumference of 1150 to 1700 nm. It is produced by a pyrogenic process in which silicon tetrachloride and a second silicon component comprising H3SiCl, H2SiCl2, HSiCl3, CH3SiCl3, (CH3)2SiCl2, (CH3)3SiCl and/or (n-C3H7)SiCl3 are mixed with primary air and a combustion gas and burnt into a reaction chamber, secondary air also being introduced into the reaction chamber, and the feed materials being chosen such that an adiabatic flame temperature of 1670 to 1730° C. is obtained. Silicone sealing compound containing the pyrogenically produced silicon dioxide powder.
    • 以BET表面积为150±15m 2 / g的一次粒子的聚集体形式的热解生成的二氧化硅粉末,其中聚集体的平均表面积为12000〜20000nm, 2,平均当量圆直径(ECD)为90〜120nm,平均圆周为1150〜1700nm。 它是通过热原法制造的,其中四氯化硅和包含H 3 SiCl,H 2 SiCl 2,HSiCl 3>与一次空气和燃烧气体混合并燃烧到反应室中,二次空气也被引入反应室,并且进料选择为使得绝热火焰温度为1670至1730℃ C.得到。 含有热解法生产的二氧化硅粉末的硅酮密封剂。