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1. 发明授权

US06914239B2 System for analyzing mass spectrometric data 有权
标题翻译：质谱数据分析系统
公开(公告)号：US06914239B2
公开(公告)日：2005-07-05
申请号：US10705612
申请日：2003-11-10
申请人： Kiyomi Yoshinari , Kinya Kobayashi , Atsushi Otake , Toyoharu Okumoto
发明人： Kiyomi Yoshinari , Kinya Kobayashi , Atsushi Otake , Toyoharu Okumoto
IPC分类号： G01N27/62 , H01J49/26 , G06F19/00 , H01J49/00
CPC分类号： H01J49/26 , H01J49/0036 , H01J49/004
摘要： A system for analyzing mass spectrometric data is provided, which has an data input means for entering mass spectrometric data of a parent ion and dissociated ions resulting from multiple dissociation of the parent ion, and an analytical means for providing characteristics of a candidate for estimated structure of a precursor ion that is representative of pre-dissociation structure at each stage of dissociation. The system analyzes one of the structure of precursor ion at each stage of dissociation and the structure of parent ion based on the characteristics and spectrometric data.
摘要翻译：提供了一种用于分析质谱数据的系统，其具有用于输入母体离子的质谱数据和由母体离子的多次解离产生的离解离子的数据输入装置，以及用于提供估计结构的候选者的特征的分析装置的前体离子，其代表在解离的每个阶段的解离前结构。该系统基于特征和光谱数据分析了每个离解阶段的前体离子结构和母体离子的结构。

2. 发明申请

US20050253060A1 Ion trap/time-of-flight mass spectrometer and method of measuring ion accurate mass 有权
标题翻译：离子阱/飞行时间质谱仪和离子精确质量的测量方法
公开(公告)号：US20050253060A1
公开(公告)日：2005-11-17
申请号：US11128261
申请日：2005-05-13
申请人： Tadao Mimura , Yoshiaki Kato , Toyoharu Okumoto
发明人： Tadao Mimura , Yoshiaki Kato , Toyoharu Okumoto
IPC分类号： G01N27/62 , G01N30/72 , H01J49/26 , H01J49/40 , H01J49/42
CPC分类号： H01J49/42 , H01J49/0009 , H01J49/004 , H01J49/40
摘要： An ion trap/time-of-flight mass spectrometer, which can perform accurate mass measurement of a product ion based on MS/MS and MSn has an ion source for ionizing a sample, an ion trap capable of temporarily trapping ions, and a time-of-flight mass spectrometer. The ion source produces ions of the sample as a measurement target and ions of a reference sample each having a known mass value. A precursor ion is selected from among the ions of the measurement target sample, and the selected precursor ion is excited and fragmented in the ion trap to produce a product ion. The reference sample ions are introduced to and trapped in the ion trap. The trapped product ion and reference sample ions are expelled out of the ion trap and introduced to the time-of-flight mass spectrometer, thereby obtaining a mass spectrum.
摘要翻译：离子阱/飞行时间质谱仪可以基于MS / MS和MS进行产物离子的精确质量测量具有离子源，用于离子化样品，离子阱能力暂时捕获离子和飞行时间质谱仪。离子源产生样品的离子作为测量对象，每个参考样品的离子具有已知的质量值。从测量对象样品的离子中选择前体离子，并且将所选择的前体离子在离子阱中激发并碎裂以产生产物离子。将参考样品离子引入并捕获在离子阱中。捕获的产物离子和参考样品离子从离子阱中排出并引入飞行时间质谱仪，从而获得质谱。

3. 发明授权

US5616918A Plasma ion mass spectrometer and plasma mass spectrometry using the same 失效
标题翻译：等离子体离子质谱仪和等离子体质谱仪使用
公开(公告)号：US5616918A
公开(公告)日：1997-04-01
申请号：US539258
申请日：1995-10-05
申请人： Konosuke Oishi , Toyoharu Okumoto , Masamichi Tsukada , Takashi Iino
发明人： Konosuke Oishi , Toyoharu Okumoto , Masamichi Tsukada , Takashi Iino
IPC分类号： G01N27/62 , H01J49/06 , H01J49/10 , H01J49/26
CPC分类号： H01J49/105
摘要： A plasma ion mass spectrometer capable of improving detection accuracy in mass spectrometry by reducing background noise due to ultraviolet radiation and neutral particles, and a plasma ion mass spectrometry using the same. A sample is ionized with plasma in a plasma generating portion. The flow of the ionized sample is shielded by a shield plate after an elapse of a specified time, and ions of the sample accumulated before the shielding is held in an ion trap type mass spectrometric portion for a specified time. The ions of the sample held for the specified time are then subjected to mass spectrometry. During ions of the sample accumulated before the shielding are held, ultraviolet radiation mixed with the ions of the sample disappears, and thereby only ions of the sample can be subjected to mass spectrometry. As a result, background noise is reduced, to improve detection accuracy in mass spectrometry.
摘要翻译：能够通过降低由于紫外线辐射和中性粒子引起的背景噪声而提高质谱检测精度的等离子体离子质谱仪和使用其的等离子体离子质谱法。在等离子体产生部分中用等离子体离子化样品。离子化样品的流动在经过规定时间后被屏蔽板屏蔽，并且在屏蔽之前累积的样品的离子在离子阱型质谱部分中保持一定时间。然后将保持规定时间的样品的离子进行质谱分析。在保持屏蔽之前累积的样品的离子中，与样品的离子混合的紫外线辐射消失，从而只能对样品的离子进行质谱分析。结果，降低背景噪声，提高质谱检测的准确性。

4. 发明授权

US5108178A Atomic absorption spectrophotometer and electromagnetic shut-off valve for use therein 失效
标题翻译：原子吸收光谱仪和电磁切断阀
公开(公告)号：US5108178A
公开(公告)日：1992-04-28
申请号：US500880
申请日：1990-03-29
申请人： Konosuke Oishi , Katsuhito Harada , Masamichi Tsukada , Kazuo Moriya , Toyoharu Okumoto
发明人： Konosuke Oishi , Katsuhito Harada , Masamichi Tsukada , Kazuo Moriya , Toyoharu Okumoto
IPC分类号： G01N21/31 , G01N21/74
CPC分类号： G01N21/74
摘要： An atomic absorption spectrophotometer includes a sample-atomizing portion for ashing and atomizing a sample, a power source operable to supply electric current to the sample-atomizing portion, a controller for controlling the operation of the power source, a pair of pressure regulators for setting a flow rate of an inert gas according to an ashing step and an atomization step in the sample-atomizing portion, a pair of movable valves respectively provided downstream of and connected to the pair of pressure regulators, and a filter device provided between the pair of movable valves and the sample-atomizing portion. Either of the pair of movable valves is activated into open or closed condition in synchronism with the operation of the power source so as to select the flow rate of the inert gas into the sample-atomizing portion. An electromagnetic shut-off valve for use in the atomic absorption spectrophotometer includes a valve housing having a valve chamber, and a movable valve body housed in the valve chamber. The movable valve body is movable between open and closed positions so as to open and close a gas flow line. The wall of the valve chamber is coated with a non-metallic material.

5. 发明授权

US07186973B2 Ion trap/time-of-flight mass analyzing apparatus and mass analyzing method 有权
标题翻译：离子阱/飞行时间质量分析仪和质量分析方法
公开(公告)号：US07186973B2
公开(公告)日：2007-03-06
申请号：US11149263
申请日：2005-06-10
申请人： Yasushi Terui , Toyoharu Okumoto , Tsukasa Shishika , Shinji Nagai , Masaru Tomioka
发明人： Yasushi Terui , Toyoharu Okumoto , Tsukasa Shishika , Shinji Nagai , Masaru Tomioka
IPC分类号： B01D59/44
CPC分类号： H01J49/424 , H01J49/0009 , H01J49/0031 , H01J49/004 , H01J49/40 , H01J49/427
摘要： An “ion trap-TOF/MS” capable of calibrating the observed mass for each of an ion trap and a TOF. In the ion trap-TOF/MS, sample ions having known mass numbers and ionized by an ion source are trapped within an ion trap. Auxiliary AC voltages having a frequency component ω are applied to the end cap electrodes of the ion trap to expel unwanted ions out of the ion trap. A measurement process is carried out by applying DC voltages to the ring electrode and the end cap electrodes to expel an ion remaining within the ion trap, and measuring the mass number of the expelled ion by the time-of-flight mass spectrometer. The measurement process is repeated while changing the frequency component ω, and the ion signal intensity measured by the time-of-flight mass spectrometer is compared with a previously stored threshold, thereby making calibration of the frequency component ω for the ion having the known mass number. Thus, the calibrating of the observed mass can be realized for each of the ion trap and the TOF.
摘要翻译：能够校准每个离子阱和TOF的观察质量的“离子阱TOF / MS”。在离子阱TOF / MS中，已知质量数和离子源电离的样品离子被捕获在离子阱内。具有频率分量ω的辅助AC电压被施加到离子阱的端盖电极以将不需要的离子排出离子阱。通过向环形电极和端盖电极施加直流电压以排出留在离子阱内的离子，并且通过飞行时间质谱仪测量排出的离子的质量数来进行测量处理。在改变频率分量ω时重复测量过程，并将通过飞行时间质谱仪测量的离子信号强度与先前存储的阈值进行比较，从而对具有已知质量的离子进行频率分量ω的校准数。因此，可以为每个离子阱和TOF实现观察到的质量的校准。

6. 发明授权

US5763877A Analyzer using plasma and analysis method using plasma, interface used for the same and sample introducing component used for the same 失效
标题翻译：使用等离子体分析仪和使用等离子体的分析方法，用于相同的界面和用于相同的样品引入组分
公开(公告)号：US5763877A
公开(公告)日：1998-06-09
申请号：US715587
申请日：1996-09-18
申请人： Konosuke Oishi , Masamichi Tsukada , Toyoharu Okumoto , Takashi Iino
发明人： Konosuke Oishi , Masamichi Tsukada , Toyoharu Okumoto , Takashi Iino
IPC分类号： G01N27/62 , G01N21/73 , H01J49/04 , H01J49/10
CPC分类号： H01J49/105 , G01N21/73
摘要： In an analyzer in which plasma is generated, a sample is supplied to the plasma though an aerosol guide tube and analyzed by a quadrapole mass filter, the top end portion of the aerosol guide tube is made of sapphire.
摘要翻译：在其中产生等离子体的分析仪中，通过气溶胶引导管将样品供应到等离子体，并通过四极质量过滤器分析，气溶胶引导管的顶端部分由蓝宝石制成。

7. 发明授权

US5104220A Atomic absorption spectrophotometer and analyzing method 失效
标题翻译：原子吸收光谱仪和分析方法
公开(公告)号：US5104220A
公开(公告)日：1992-04-14
申请号：US316964
申请日：1989-02-28
申请人： Toyoharu Okumoto , Katsuhito Harada , Konosuke Oishi
发明人： Toyoharu Okumoto , Katsuhito Harada , Konosuke Oishi
IPC分类号： G01N21/31 , G01N21/74
CPC分类号： G01N21/74
摘要： An atomic absorption spectrophotometer comprising means for setting the ashing temperature for that of the element having the lowest ashing temperature; means for setting the atomizing temperature for that of the element having the highest atomizing temperature; and means for effecting background correction utilizing Zeeman effect.
摘要翻译：一种原子吸收分光光度计，包括用于设定具有最低灰度温度的元件的灰度温度的装置; 用于设定具有最高雾化温度的元件的雾化温度的装置; 以及利用塞曼效应进行背景校正的方法。

8. 发明授权

US4840484A Atomic absorption spectrophotometer with furnace at pressure equal or near light source pressure 失效
标题翻译：原子吸收分光光度计，炉内压力等于或接近光源压力
公开(公告)号：US4840484A
公开(公告)日：1989-06-20
申请号：US175320
申请日：1988-03-30
申请人： Konosuke Oishi , Toyoharu Okumoto , Hayato Tobe , Masamichi Tsukada
发明人： Konosuke Oishi , Toyoharu Okumoto , Hayato Tobe , Masamichi Tsukada
IPC分类号： G01N21/31 , G01N21/74
CPC分类号： G01N21/74 , G01N2021/745
摘要： In an atomic absorption spectrophotometer including an electric furnace for drying and ashing a liquid sample to be analyzed and then atomizing the sample to generate atomic vapor, a low-pressure lamp for emitting light having a spectrum of an element to be analyzed onto the atomic vapor atomized in the electric furnace, a monochromator for splitting the transmitted light from the electric furnace and selecting a wavelength of an atomic absorption line absorbed by the element to be analyzed, and a signal processing unit for performing signal processing on the light having the selected wavelength supplied from the monochromator, the electric furnace is an airtight mechanism for maintaining airtightness of the inside of the electric furnace and an evacuation unit for evacuating the inside of the electric furnace to a pressure equal to the pressure inside the lamp.
摘要翻译：在包括用于干燥和灰化待分析的液体样品的电炉，然后将样品雾化以产生原子蒸气的原子吸收分光光度计中的低压灯，用于将具有待分析元素的光谱发射到原子蒸气上的光在电炉中雾化的单色仪，用于分离来自电炉的透射光并选择待分析元件吸收的原子吸收线的波长的单色仪，以及对具有所选波长的光进行信号处理的信号处理单元电炉是用于保持电炉内部的气密性的气密机构和用于将电炉的内部抽空至与灯内的压力相等的压力的排气单元。

9. 发明申请

US20070069121A1 Ion trap/time-of-flight mass spectrometer and method of measuring ion accurate mass 审中-公开
标题翻译：离子阱/飞行时间质谱仪和离子精确质量的测量方法
公开(公告)号：US20070069121A1
公开(公告)日：2007-03-29
申请号：US11606046
申请日：2006-11-30
申请人： Tadao Mimura , Yoshiaki Kato , Toyoharu Okumoto
发明人： Tadao Mimura , Yoshiaki Kato , Toyoharu Okumoto
IPC分类号： H01J49/00
CPC分类号： H01J49/42 , H01J49/0009 , H01J49/004 , H01J49/40
摘要： An ion trap/time-of-flight mass spectrometer, which can perform accurate mass measurement of a product ion based on MS/MS and MSn has an ion source for ionizing a sample, an ion trap capable of temporarily trapping ions, and a time-of-flight mass spectrometer. The ion source produces ions of the sample as a measurement target and ions of a reference sample each having a known mass value. A precursor ion is selected from among the ions of the measurement target sample, and the selected precursor ion is excited and fragmented in the ion trap to produce a product ion. The reference sample ions are introduced to and trapped in the ion trap. The trapped product ion and reference sample ions are expelled out of the ion trap and introduced to the time-of-flight mass spectrometer, thereby obtaining a mass spectrum.
摘要翻译：离子阱/飞行时间质谱仪可以基于MS / MS和MS进行产物离子的精确质量测量具有离子源，用于离子化样品，离子阱能力暂时捕获离子和飞行时间质谱仪。离子源产生样品的离子作为测量对象，每个参考样品的离子具有已知的质量值。从测量对象样品的离子中选择前体离子，并且将所选择的前体离子在离子阱中激发并碎裂以产生产物离子。将参考样品离子引入并捕获在离子阱中。捕获的产物离子和参考样品离子从离子阱中排出并引入飞行时间质谱仪，从而获得质谱。

10. 发明授权

US5793039A Mass spectrometer, skimmer cone assembly, skimmer cone and its manufacturing method 失效
标题翻译：质谱仪，撇渣锥组件，撇渣器及其制造方法
公开(公告)号：US5793039A
公开(公告)日：1998-08-11
申请号：US605572
申请日：1996-02-22
申请人： Konosuke Oishi , Masamichi Tsukada , Toyoharu Okumoto , Takashi Iino
发明人： Konosuke Oishi , Masamichi Tsukada , Toyoharu Okumoto , Takashi Iino
IPC分类号： G01N27/62 , G21K1/02 , H01J49/04 , H01J49/26 , G01D59/44 , H01J49/00
CPC分类号： H01J49/067
摘要： Disclosed is a structure comprising; (a) Plasma gas is supplied to torch tube 8 from inert pressure vessel 1. (b) Nebulizer 3 absorbs sample 4 to vaporize the sample as aerosol and to introduce it into plasma 5. (c) Plasma 5 touches sampling cone 10 having an opening at the apex and a conical surface, whereby an ion stream is extracted through the opening of the sampling cone whose pressure is reduced at the rear face thereof. (d) The extracted ion stream further touches skimmer cone 12 of the conical surface having a small hole at the apex, and is absorbed into vacuum chamber 13 where the pressure is further reduced at the rear face. (e) The ion stream is flowed into quadruple pole filter 18 to carry out the mass spectrometry analysis of the ion stream.
摘要翻译：公开了一种结构，包括：（a）将等离子体气体从惰性压力容器1供应给割炬管8.（b）雾化器3吸收样品4以使气溶胶蒸发，并将其引入等离子体5.（c）等离子体5接触采样锥10，在顶点处开口并具有锥形表面，由此通过其后面压力减小的取样锥体的开口提取离子流。（d）提取的离子流进一步接触顶点处具有小孔的圆锥形表面的撇渣器锥体12，并被吸收到真空室13中，在该真空室13中后面进一步减小压力。（e）离子流流入四极过滤器18，进行离子流的质谱分析。

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