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1. 发明授权

US07491840B2 Compound and composition containing the same 有权
标题翻译：化合物和含有其的组合物
公开(公告)号：US07491840B2
公开(公告)日：2009-02-17
申请号：US11360501
申请日：2006-02-24
申请人： Kazuya Tsukamoto , Nobumasa Arashiba , Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
发明人： Kazuya Tsukamoto , Nobumasa Arashiba , Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
IPC分类号： C07C69/00
CPC分类号： C07C69/40 , B60C1/00 , C07C69/44 , C07C69/50
摘要： This invention provides a compound represented by the following general formula (1) and capable of suppressing the blooming, which is observed in the compounding of the resorcin or the RF resin, as far as possible while maintaining the workability and high humidity-aged adhesion of the rubber composition obtained by compounding with rubber, reducing the deterioration of the adhesiveness during the storage of the rubber composition and stably developing the adhesiveness as well as the composition containing the above-mentioned compound as a main component: (wherein R represents a divalent aliphatic group having a carbon number of 1-16).
摘要翻译：本发明提供一种由以下通式（1）表示的化合物，并且能够在保持加工性和高湿度老化粘合性的同时尽可能地抑制在间苯酚或RF树脂的配混中观察到的起霜通过与橡胶配混获得的橡胶组合物，减少橡胶组合物的保存期间的粘合性的劣化并且稳定地发挥粘合性以及含有上述化合物作为主要成分的组合物（其中R表示二价脂族碳数为1-16的基团）。

2. 发明授权

US09464183B2 Rubber composition and pneumatic tire using the same 有权
标题翻译：橡胶组合物和使用其的充气轮胎
公开(公告)号：US09464183B2
公开(公告)日：2016-10-11
申请号：US13035347
申请日：2011-02-25
申请人： Kazunori Kaneda , Yoshinori Kuriya , Kazuya Tsukamoto , Nobumasa Arashiba , Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
发明人： Kazunori Kaneda , Yoshinori Kuriya , Kazuya Tsukamoto , Nobumasa Arashiba , Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
IPC分类号： B60C1/00 , B60C9/02 , B60C9/18 , B29D30/00 , C08K5/098 , C08K5/134
CPC分类号： C08K5/098 , B60C1/00 , C08K5/134 , Y10T152/1081 , C08L21/00
摘要： This invention provides a rubber composition comprising 1-10 parts by mass of sulfur and 0.1-10 parts by mass of a compound represented by the following general formula (1) or a composition containing the compound as a main component based on 100 parts by mass of a rubber component as well as a pneumatic tire in which at least one of a carcass (4) and a belt (6) includes a layer composed of steel cords covered with a coating rubber, characterized in that the above rubber composition is used as the coating rubber covering the steel cords in at least one of the carcass (4) and the belt (6): (wherein R represents a divalent aliphatic group having a carbon number of 1-16 or a divalent aromatic group).

3. 发明申请

US20060205971A1 Compound and composition containing the same 有权
公开(公告)号：US20060205971A1
公开(公告)日：2006-09-14
申请号：US11360501
申请日：2006-02-24
申请人： Kazuya Tsukamoto , Nobumasa Arashiba , Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
发明人： Kazuya Tsukamoto , Nobumasa Arashiba , Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
IPC分类号： C07C69/02
CPC分类号： C07C69/40 , B60C1/00 , C07C69/44 , C07C69/50
摘要： This invention provides a compound represented by the following general formula (1) and capable of suppressing the blooming, which is observed in the compounding of the resorcin or the RF resin, as far as possible while maintaining the workability and high humidity-aged adhesion of the rubber composition obtained by compounding with rubber, reducing the deterioration of the adhesiveness during the storage of the rubber composition and stably developing the adhesiveness as well as the composition containing the above-mentioned compound as a main component: (wherein R represents a divalent aliphatic group having a carbon number of 1-16).

4. 发明申请

US20080047650A1 Rubber Composition And Pneumatic Tire Using The Same 审中-公开
标题翻译：橡胶组成和气动轮胎使用它
公开(公告)号：US20080047650A1
公开(公告)日：2008-02-28
申请号：US10598688
申请日：2005-03-07
申请人： Kazunori Kaneda , Yoshinori Kuriya , Kazuya Tsukamoto , Nobumasa Arashiba , Akinori Nagatomo , Takeshi Kobayashi
发明人： Kazunori Kaneda , Yoshinori Kuriya , Kazuya Tsukamoto , Nobumasa Arashiba , Akinori Nagatomo , Takeshi Kobayashi
IPC分类号： C08L21/00 , B60C1/00 , C08K3/06
CPC分类号： C08K5/098 , B60C1/00 , C08K5/134 , Y10T152/1081 , C08L21/00
摘要： This invention provides a rubber composition comprising 1-10 parts by mass of sulfur and 0.1-10 parts by mass of a compound represented by the following general formula (1) or a composition containing the compound as a main component based on 100 parts by mass of a rubber component as well as a pneumatic tire in which at least one of a carcass (4) and a belt (6) includes a layer composed of steel cords covered with a coating rubber, characterized in that the above rubber composition is used as the coating rubber covering the steel cords in at least one of the carcass (4) and the belt (6): (wherein R represents a divalent aliphatic group having a carbon number of 1-16 or a divalent aromatic group).
摘要翻译：本发明提供一种橡胶组合物，其包含1-10质量份的硫和0.1-10质量份的由以下通式（1）表示的化合物或基于100质量份含有该化合物作为主要成分的组合物橡胶部件以及胎体（4）和带（6）中的至少一个包括由涂覆橡胶覆盖的钢丝帘线构成的层的充气轮胎，其特征在于，将上述橡胶组合物用作所述涂覆橡胶覆盖所述胎体（4）和所述带（6）中的至少一个中的钢丝帘线（其中R表示碳数为1-16的二价脂族基团或二价芳族基团）。

5. 发明授权

US08222446B2 Method for producing dihydroxybenzene derivative 有权
标题翻译：二羟基苯衍生物的制备方法
公开(公告)号：US08222446B2
公开(公告)日：2012-07-17
申请号：US12918852
申请日：2008-03-19
申请人： Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
发明人： Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
IPC分类号： C07C69/675
CPC分类号： C07C67/03 , C07C67/14 , C07C69/44 , C07C69/50
摘要： A method of producing a compound represented by the following general formula (3): [wherein R is a bivalent aliphatic group having a carbon number of 1-16 or a bivalent aromatic group], which comprises a step (i) of reacting a compound represented by the following general formula (1): with a carboxylic acid halide represented by the following general formula (2): [wherein R is a bivalent aliphatic group having a carbon number of 1-16 or a bivalent aromatic group and X is a halogen atom] in the presence of a basic compound to form an ester, and a step (ii) of conducting a heat treatment after the step (i) to decompose an oligomer in the ester.
摘要翻译：一种制备由以下通式（3）表示的化合物的方法：[其中R是碳数为1-16的二价脂族基或二价芳族基]，其包括步骤（i）使化合物由以下通式（1）表示：用下述通式（2）表示的羧酰卤：[其中R是碳数为1-16的二价脂族基或二价芳基，X为卤素原子]在碱性化合物存在下反应形成酯，和步骤（ii）在步骤（i）之后进行热处理以分解酯中的低聚物。

6. 发明申请

US20110004013A1 METHOD FOR PRODUCING DIHYDROXYBENZENE DERIVATIVE 有权
标题翻译：生产二羟基苯甲醛衍生物的方法
公开(公告)号：US20110004013A1
公开(公告)日：2011-01-06
申请号：US12918852
申请日：2008-03-19
申请人： Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
发明人： Akinori Nagatomo , Kouki Oogaki , Takeshi Kobayashi
IPC分类号： C07C69/675
CPC分类号： C07C67/03 , C07C67/14 , C07C69/44 , C07C69/50
摘要： A method of producing a compound represented by the following general formula (3): [wherein R is a bivalent aliphatic group having a carbon number of 1-16 or a bivalent aromatic group], which comprises a step (i) of reacting a compound represented by the following general formula (1): with a carboxylic acid halide represented by the following general formula (2): [wherein R is a bivalent aliphatic group having a carbon number of 1-16 or a bivalent aromatic group and X is a halogen atom] in the presence of a basic compound to form an ester, and a step (ii) of conducting a heat treatment after the step (i) to decompose an oligomer in the ester.
摘要翻译：一种制备由以下通式（3）表示的化合物的方法：[其中R是碳数为1-16的二价脂族基或二价芳族基]，其包括步骤（i）使化合物由以下通式（1）表示：用下述通式（2）表示的羧酰卤：[其中R是碳数为1-16的二价脂族基或二价芳基，X为卤素原子]在碱性化合物存在下反应形成酯，和步骤（ii）在步骤（i）之后进行热处理以分解酯中的低聚物。

7. 发明授权

US08198482B2 Method for producing carboxylic acid chloride 有权
标题翻译：羧酸氯化物的制备方法
公开(公告)号：US08198482B2
公开(公告)日：2012-06-12
申请号：US12529307
申请日：2008-02-27
申请人： Takeshi Kobayashi , Kiyomi Kido , Akinori Nagatomo
发明人： Takeshi Kobayashi , Kiyomi Kido , Akinori Nagatomo
IPC分类号： C07C51/58
CPC分类号： C07C51/60 , C07C51/64 , C07C55/36
摘要： This invention relates to a method for producing a carboxylic acid chloride, which efficiently decomposes a Vilsmeier reagent type compound in a carboxylic acid chloride lacking a thermal stability or a carboxylic acid chloride hardly distilled in practice due to a high boiling point with a simple operation and has no adverse effect on a subsequent step, and more particularly to a method for producing a carboxylic acid chloride, characterized by comprising reacting a carboxylic acid with a chlorinating agent in the presence of a catalyst, removing the excessive chlorinating agent from a reaction system after the reaction, and then further adding 1.0 to 3.0 equivalents of the starting carboxylic acid based on the catalyst to the reaction system to decompose a Vilsmeier reagent type compound remaining in the reaction system.
摘要翻译：本发明涉及一种生产羧酸氯化物的方法，该方法通过简单的操作由于沸点高而在实际上难以蒸馏的Vilsmeier试剂型化合物在不具有热稳定性的羧酸氯化物或羧酸氯化物中有效分解，对后续步骤没有不利影响，更具体地说，涉及一种制备羧酰氯的方法，其特征在于包括在催化剂存在下使羧酸与氯化剂反应，在反应体系之后从反应体系中除去过量的氯化剂反应，然后将基于催化剂的1.0〜3.0当量的起始羧酸加入到反应体系中以分解残留在反应体系中的Vilsmeier试剂型化合物。

8. 发明申请

US20100099911A1 METHOD FOR PRODUCING CARBOXYLIC ACID CHLORIDE 有权
标题翻译：生产羧酸氯化物的方法
公开(公告)号：US20100099911A1
公开(公告)日：2010-04-22
申请号：US12529307
申请日：2008-02-27
申请人： Takeshi Kobayashi , Kiyomi Kido , Akinori Nagatomo
发明人： Takeshi Kobayashi , Kiyomi Kido , Akinori Nagatomo
IPC分类号： C07C51/60
CPC分类号： C07C51/60 , C07C51/64 , C07C55/36
摘要： This invention relates to a method for producing a carboxylic acid chloride, which efficiently decomposes a Vilsmeier reagent type compound in a carboxylic acid chloride lacking a thermal stability or a carboxylic acid chloride hardly distilled in practice due to a high boiling point with a simple operation and has no adverse effect on a subsequent step, and more particularly to a method for producing a carboxylic acid chloride, characterized by comprising reacting a carboxylic acid with a chlorinating agent in the presence of a catalyst, removing the excessive chlorinating agent from a reaction system after the reaction, and then further adding 1.0 to 3.0 equivalents of the starting carboxylic acid based on the catalyst to the reaction system to decompose a Vilsmeier reagent type compound remaining in the reaction system.
摘要翻译：本发明涉及一种生产羧酸氯化物的方法，该方法通过简单的操作由于沸点高而在实际上难以蒸馏的Vilsmeier试剂型化合物在不具有热稳定性的羧酸氯化物或羧酸氯化物中有效分解，对后续步骤没有不利影响，更具体地说，涉及一种制备羧酰氯的方法，其特征在于包括在催化剂存在下使羧酸与氯化剂反应，在反应体系之后从反应体系中除去过量的氯化剂反应，然后将基于催化剂的1.0〜3.0当量的起始羧酸加入到反应体系中以分解残留在反应体系中的Vilsmeier试剂型化合物。

9. 发明授权

US6072024A Production process of cross-linked polyaspartic acid resin 失效
标题翻译：交联聚天冬氨酸树脂的生产工艺
公开(公告)号：US6072024A
公开(公告)日：2000-06-06
申请号：US42942
申请日：1998-03-17
申请人： Yoshihiro Irizato , Makoto Sukegawa , Toshio Katoh , Hiroaki Tamatani , Akinori Nagatomo , Masaru Wada
发明人： Yoshihiro Irizato , Makoto Sukegawa , Toshio Katoh , Hiroaki Tamatani , Akinori Nagatomo , Masaru Wada
IPC分类号： C08G73/10 , C08G69/10
CPC分类号： C08G73/1092
摘要： A process is disclosed for producing with good productivity a cross-linked polyaspartic acid resin having biodegradability and high water absorbency. The process features inclusion of one of the following steps: (a) a polysuccinimide, which has been brought into a dispersed state by a dispersant, and a cross-linking agent are reacted to produce the cross-linked polyaspartic acid resin; (b) imide rings of a cross-linked polysuccinimide are subjected to a hydrolysis reaction while controlling a swelling degree of a resulting gel, whereby the cross-linked polyaspartic acid resin is produced; and (c) a gel of a cross-linked polysuccinimide, which has been obtained by reacting a cross-linking agent to a solution of a polysuccinimide in an organic solvent, is disintegrated to subject imide rings of the cross-linked polysuccinimide to a hydrolysis reaction, so that the cross-linked polyaspartic acid resin is produced. The process may also include one or both of the following steps as needed: (d) a gel of the cross-linked polyaspartic acid resin is washed with water and/or a water-miscible organic solvent; and (e) the polysuccinimide is produced using a basic amino acid as a cross-linking agent.
摘要翻译：公开了一种具有生物降解性和高吸水性的交联聚天冬氨酸树脂以高生产率生产的方法。该方法包括以下步骤之一：（a）已经通过分散剂进入分散状态的聚琥珀酰亚胺和交联剂反应生成交联聚天冬氨酸树脂; （b）交联聚琥珀酰亚胺的酰亚胺环进行水解反应同时控制所得凝胶的溶胀度，从而制得交联聚天冬氨酸树脂; 和（c）通过使交联剂与聚琥珀酰亚胺在有机溶剂中的溶液反应而获得的交联聚琥珀酰亚胺的凝胶被分解以使交联的聚琥珀酰亚胺的酰亚胺环进行水解反应，制成交联聚天冬氨酸树脂。该方法还可以根据需要包括以下步骤中的一种或两种：（d）用水和/或水混溶性有机溶剂洗涤交联聚天冬氨酸树脂的凝胶; 和（e）使用碱性氨基酸作为交联剂制备聚琥珀酰亚胺。

10. 发明授权

US5484945A Preparation process of polysuccinimide 失效
标题翻译：聚琥珀酰亚胺的制备工艺
公开(公告)号：US5484945A
公开(公告)日：1996-01-16
申请号：US288454
申请日：1994-08-10
申请人： Akinori Nagatomo , Hiroaki Tamatani , Masanobu Ajioka , Akihiro Yamaguchi
发明人： Akinori Nagatomo , Hiroaki Tamatani , Masanobu Ajioka , Akihiro Yamaguchi
IPC分类号： C08G73/10 , C07D207/10
CPC分类号： C08G73/1092
摘要： In the process for preparing polysuccinimide by dehydration condensation of aspartic acid in an organic solvent, polysuccinimide can be obtained simply and suitably in industry by removing a portion or more of the organic solvent from the reaction mixture while charging to the reaction mixture an additional organic solvent containing less amount of water than that of the removed organic solvent.
摘要翻译：在通过天冬氨酸在有机溶剂中脱水缩合制备聚琥珀酰亚胺的方法中，通过从反应混合物中除去一部分或更多种有机溶剂，可以简单适当地在工业上获得聚琥珀酰亚胺，同时向反应混合物中加入另外的有机溶剂含有比去除的有机溶剂少的水量。

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