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1. 发明申请

US20070212561A1 Methacrylic Resin Composition, Methacrylic Resin Film, and Vinyl Chloride Molded Article with the Film Layered 有权
标题翻译：甲基丙烯酸树脂组合物，甲基丙烯酸树脂膜和氯乙烯模制品与薄膜分层
公开(公告)号：US20070212561A1
公开(公告)日：2007-09-13
申请号：US10594976
申请日：2005-03-28
申请人： Kazuhito Wada , Norito Doi , Kimihide Nishimura
发明人： Kazuhito Wada , Norito Doi , Kimihide Nishimura
IPC分类号： B32B27/30 , B32B27/18
CPC分类号： B32B27/30 , B32B27/08 , B32B27/22 , B32B27/308 , B32B2250/02 , B32B2250/246 , B32B2270/00 , B32B2307/412 , B32B2307/536 , B32B2307/558 , B32B2307/712 , B32B2419/00 , B32B2509/00 , B32B2605/003 , C08F265/06 , Y10T428/254 , Y10T428/31855 , Y10T428/31909 , Y10T428/31928 , Y10T428/31935
摘要： A resin composition suitable for forming a film excellent in transparency, weatherability, hardness, shock resistance, bending-fracturing resistance, and moldability; and a film excellent in weatherability even when laminated on a molded body comprising a PVC resin composition containing a plasticizer is provided. The film having the above characteristics can be obtained by making a methacrylic resin composition into a film, the methacrylic resin composition comprising a methacrylic resin composition (C) obtained by polymerizing a methacrylate polymer (A) obtained by polymerizing a monomer mixture mainly composed of alkyl methacrylate in the presence of acrylic crosslinked elastic particles (B) obtained by copolymerizing a monomer mixture mainly composed of alkyl acrylate and a polyfunctional monomer with two or more non-conjugated double bonds per a molecule; and being copolymerized with 0.01 to 50 parts by weight of an ultraviolet absorber represented by the general formula (1).
摘要翻译：适用于形成透明性，耐候性，硬度，耐冲击性，耐弯曲破坏性和成型性优异的膜的树脂组合物。以及即使在包含含有增塑剂的PVC树脂组合物的成型体上层叠时也具有耐候性优异的膜。具有上述特征的膜可以通过将甲基丙烯酸系树脂组合物成膜而得到，所述甲基丙烯酸系树脂组合物含有通过聚合由主要由烷基构成的单体混合物聚合得到的甲基丙烯酸酯聚合物（A）而得到的甲基丙烯酸系聚合物（A）在通过使主要由丙烯酸烷基酯和多官能单体共聚的单体混合物每分子具有两个或更多个非共轭双键而获得的丙烯酸交联弹性颗粒（B）的存在下，并与0.01〜50重量份的由通式（1）表示的紫外线吸收剂共聚。

2. 发明授权

US07999032B2 Methacrylic resin composition 有权
标题翻译：甲基丙烯酸树脂组合物
公开(公告)号：US07999032B2
公开(公告)日：2011-08-16
申请号：US11994746
申请日：2006-07-05
申请人： Kazuhito Wada , Kimihide Nishimura , Norito Doi
发明人： Kazuhito Wada , Kimihide Nishimura , Norito Doi
IPC分类号： C04B35/634
CPC分类号： C08J5/18 , B32B27/18 , B32B27/30 , C08F265/06 , C08J2351/00 , C08K5/3475 , C08L33/06 , C08L33/12 , C08L51/00 , C09D5/32 , Y10T428/254 , Y10T428/31909 , Y10T428/31928 , C08F220/14 , C08L2666/24 , C08L2666/04
摘要： An acrylic resin composition suitable for use as films excellent in transparency, weatherability, hardness, impact resistance, flex cracking resistance, and formability. The resin composition comprises an acrylic graft copolymer (A) including a rubbery acrylic ester polymer (A-a) and a methacrylic polymer (B) comprising 80 wt. % or more methyl methacrylate units, the acrylic resin composition having a specific value of reduced viscosity (0.2-0.8 dl/g), specific values of content (5-45 wt. %) and average particle diameter (50-200 nm) of the rubbery polymer (A-a), a specific relationship between the particle diameter and the crosslinking agent amount (0.02d≦w≦0.05d; d, average particle diameter (nm); w, amount of crosslinking agent (wt. %)), and a specific value of the degree of grafting (50-250%). The resin composition contains an ultraviolet absorber incorporated therein through copolymerization.
摘要翻译：适合用作透明性，耐候性，硬度，耐冲击性，抗开裂性和成型性优异的薄膜的丙烯酸树脂组合物。树脂组合物包含丙烯酸接枝共聚物（A），其包含橡胶状丙烯酸酯聚合物（A-a）和甲基丙烯酸类聚合物（B），其包含80重量％％以上的甲基丙烯酸甲酯单元，丙烯酸树脂组合物的比浓粘度（0.2〜0.8dl / g），比重值（5-45重量％）和平均粒径（50〜200nm）橡胶状聚合物（Aa），粒径与交联剂量的相关关系（0.02d＆nlE; w＆nlE; 0.05d; d，平均粒径（nm）; w，交联剂量（重量％））和接枝度的具体值（50-250％）。该树脂组合物含有通过共聚合结合在其中的紫外线吸收剂。

3. 发明授权

US07722946B2 Methacrylic resin composition, methacrylic resin film, and vinyl chloride molded article with the film layered 有权
标题翻译：甲基丙烯酸树脂组合物，甲基丙烯酸树脂膜和氯乙烯模塑制品具有膜层状
公开(公告)号：US07722946B2
公开(公告)日：2010-05-25
申请号：US10594976
申请日：2005-03-28
申请人： Kazuhito Wada , Norito Doi , Kimihide Nishimura
发明人： Kazuhito Wada , Norito Doi , Kimihide Nishimura
IPC分类号： B32B5/16 , B32B27/00 , B32B27/08
CPC分类号： B32B27/30 , B32B27/08 , B32B27/22 , B32B27/308 , B32B2250/02 , B32B2250/246 , B32B2270/00 , B32B2307/412 , B32B2307/536 , B32B2307/558 , B32B2307/712 , B32B2419/00 , B32B2509/00 , B32B2605/003 , C08F265/06 , Y10T428/254 , Y10T428/31855 , Y10T428/31909 , Y10T428/31928 , Y10T428/31935
摘要： A resin composition suitable for forming a film excellent in transparency, weatherability, hardness, shock resistance, bending-fracturing resistance, and moldability; and a film excellent in weatherability even when laminated on a molded body comprising a PVC resin composition containing a plasticizer is provided. The film having the above characteristics can be obtained by making a methacrylic resin composition into a film, the methacrylic resin composition comprising a methacrylic resin composition (C) obtained by polymerizing a methacrylate polymer (A) obtained by polymerizing a monomer mixture mainly composed of alkyl methacrylate in the presence of acrylic crosslinked elastic particles (B) obtained by copolymerizing a monomer mixture mainly composed of alkyl acrylate and a polyfunctional monomer with two or more non-conjugated double bonds per a molecule; and being copolymerized with 0.01 to 50 parts by weight of an ultraviolet absorber represented by the general formula (1).
摘要翻译：适用于形成透明性，耐候性，硬度，耐冲击性，耐弯曲破坏性和成型性优异的膜的树脂组合物。以及即使在包含含有增塑剂的PVC树脂组合物的成型体上层叠时也具有耐候性优异的膜。具有上述特征的膜可以通过将甲基丙烯酸系树脂组合物成膜而得到，所述甲基丙烯酸系树脂组合物含有通过聚合由主要由烷基构成的单体混合物聚合得到的甲基丙烯酸酯聚合物（A）而得到的甲基丙烯酸系聚合物（A）在通过使主要由丙烯酸烷基酯和多官能单体共聚的单体混合物每分子具有两个或更多个非共轭双键而获得的丙烯酸交联弹性颗粒（B）的存在下，并与0.01〜50重量份的由通式（1）表示的紫外线吸收剂共聚。

4. 发明申请

US20080318072A1 Imide Resin, Production Method of Imide Resin, and Usage of Imide Resin 审中-公开
标题翻译：酰亚胺树脂，酰亚胺树脂的制备方法和酰亚胺树脂的用途
公开(公告)号：US20080318072A1
公开(公告)日：2008-12-25
申请号：US10581267
申请日：2004-12-01
申请人： Hirosuke Kawabata , Tomoki Hiiro , Yasuhiro Sekiguchi , Kazuhito Wada , Kimihide Nishimura , Norito Doi
发明人： Hirosuke Kawabata , Tomoki Hiiro , Yasuhiro Sekiguchi , Kazuhito Wada , Kimihide Nishimura , Norito Doi
IPC分类号： B32B15/08 , C08F120/06 , C08F8/32
CPC分类号： C08G73/10 , C08F8/48 , C08F2800/20 , Y10T428/31692 , C08F8/32 , C08F220/14 , C08F212/08
摘要： To realize an imide resin which is favorable in optical use.The imide resin according to the present invention includes: a repeating unit represented by General Formula (1); a repeating unit represented by General Formula (2); and a repeating unit represented by General Formula (3), wherein an orientation birefringence of the imide resin ranges from −0.1×10−3 to 0.1×10−3, where each of R1 and R2 independently represents a hydrogen atom or an alkyl group having 1 to 8 carbon atoms, and R3 represents a hydrogen atom, an alkyl group having 1 to 18 carbon atoms, a cycloalkyl group having 3 to 12 carbon atoms, or an aryl group having 6 to 10 carbon atoms, where each of R4 and R5 independently represents a hydrogen atom or an alkyl group having 1 to 8 carbon atoms, and R6 represents an alkyl group having 1 to 18 carbon atoms, a cycloalkyl group having 3 to 12 carbon atoms, or an aryl group having 6 to 10 carbon atoms, where R7 represents a hydrogen atom or an alkyl group having 1 to 8 carbon atoms, and R8 represents an aryl group having 6 to 10 carbon atoms.
摘要翻译：实现光学用途有利的酰亚胺树脂。根据本发明的酰亚胺树脂包括：由通式（1）表示的重复单元; 由通式（2）表示的重复单元; 和由通式（3）表示的重复单元，其中酰亚胺树脂的取向双折射率为-0.1×10-3至0.1×10-3，其中R1和R2各自独立地表示氢原子或具有1个至8个碳原子，并且R 3表示氢原子，具有1至18个碳原子的烷基，具有3至12个碳原子的环烷基或具有6至10个碳原子的芳基，其中R 4和R 5各自独立地表示氢原子或碳原子数1〜8的烷基，R 6表示碳原子数1〜18的烷基，碳原子数3〜12的环烷基或碳原子数6〜10的芳基， R7表示氢原子或碳原子数1〜8的烷基，R8表示碳原子数6〜10的芳基。

5. 发明申请

US20090012215A1 METHACRYLIC RESIN COMPOSITION 有权
标题翻译：甲基丙烯酸树脂组合物
公开(公告)号：US20090012215A1
公开(公告)日：2009-01-08
申请号：US11994746
申请日：2006-07-05
申请人： Kazuhito Wada , Kimihide Nishimura , Norito Doi
发明人： Kazuhito Wada , Kimihide Nishimura , Norito Doi
IPC分类号： C08L33/04
CPC分类号： C08J5/18 , B32B27/18 , B32B27/30 , C08F265/06 , C08J2351/00 , C08K5/3475 , C08L33/06 , C08L33/12 , C08L51/00 , C09D5/32 , Y10T428/254 , Y10T428/31909 , Y10T428/31928 , C08F220/14 , C08L2666/24 , C08L2666/04
摘要： An acrylic resin composition suitable for use as films excellent in transparency, weatherability, hardness, impact resistance, flex cracking resistance, and formability. The resin composition comprises an acrylic graft copolymer (A) including a rubbery acrylic ester polymer (A-a) and a methacrylic polymer (B) comprising 80 wt. % or more methyl methacrylate units, the acrylic resin composition having a specific value of reduced viscosity (0.2-0.8 dl/g), specific values of content (5-45 wt. %) and average particle diameter (50-200 nm) of the rubbery polymer (A-a), a specific relationship between the particle diameter and the crosslinking agent amount (0.02d≦w≦0.05d; d, average particle diameter (nm); w, amount of crosslinking agent (wt. %)), and a specific value of the degree of grafting (50-250%). The resin composition contains an ultraviolet absorber incorporated therein through copolymerization.
摘要翻译：适合用作透明性，耐候性，硬度，耐冲击性，抗开裂性和成型性优异的薄膜的丙烯酸树脂组合物。树脂组合物包含丙烯酸接枝共聚物（A），其包含橡胶状丙烯酸酯聚合物（A-a）和甲基丙烯酸类聚合物（B），其包含80重量％％以上的甲基丙烯酸甲酯单元，丙烯酸树脂组合物的比浓粘度（0.2〜0.8dl / g），比重值（5-45重量％）和平均粒径（50〜200nm）橡胶状聚合物（Aa），粒径和交联剂量之间的具体关系（0.02d≤w≤0.05d; d，平均粒径（nm）; w，交联剂的量（重量％））），接枝度的具体值（50〜250％）。该树脂组合物含有通过共聚合结合在其中的紫外线吸收剂。

6. 发明授权

US6136918A Rubber latexes, graft copolymers, and thermoplastic resin compositions 失效
标题翻译：橡胶胶乳，接枝共聚物和热塑性树脂组合物
公开(公告)号：US6136918A
公开(公告)日：2000-10-24
申请号：US68014
申请日：1998-04-30
申请人： Ikuhiro Mishima , Norito Doi , Youichi Matsumura , Shigemi Matsumoto , Shinobu Ochikoshi , Kazuhito Wada , Hiroki Yoshino
发明人： Ikuhiro Mishima , Norito Doi , Youichi Matsumura , Shigemi Matsumoto , Shinobu Ochikoshi , Kazuhito Wada , Hiroki Yoshino
IPC分类号： C08C1/07 , C08F265/04 , C08F279/02 , C08L21/02 , C08L51/04 , C08F291/02 , C08L33/06
CPC分类号： C08L21/02 , C08C1/07 , C08F265/04 , C08F279/02 , C08L51/04
摘要： A rubber latex with its particles grown through cohesion by adding 100 weight parts of (B) a rubber latex (solid), 0.1-15 weight parts (solid) of (A) an acid group-containing latex having an average particle size of 50-500 nm prepared by polymerizing a monomer mixture comprising (a), (b), (c) and (d) [wherein (a)+(b)+(c)+(d)=100 weight %]: (a) 5-25 weight % of at least one of unsaturated acids selected from the group consisting of acrylic acid, methacrylic acid, itaconic acid and crotonic acid, (b) 20-95 weight % of at least one of alkyl methacrylates with its alkyl group 1-12 in carbon number, (c) 0-30 weight % of at least one of alkyl acrylates with its alkyl group 1-12 in carbon number, (d) 0-40 weight % of at least one selected from the group consisting of aromatic vinyls, compounds having at least two polymerizable functional groups in a molecule and vinyl cyanides, copolymerizable with the aforementioned (a), (b) and (c) is provided. The rubber latex and a graft copolymer containing it and thermoplastic resins incorporating said graft copolymer are excellent in impact strength, heat resistance and workability.
摘要翻译： PCT No.PCT / JP95 / 02548 Sec。 371日期：1998年4月30日 102（e）1998年4月30日PCT 1995年12月13日PCT PCT。出版物WO97 / 21770 日期：1996年6月19日通过加入100重量份（B）橡胶胶乳（固体），0.1-15重量份（固体）（A）含酸基胶乳的胶乳（其具有通过聚合包含（a），（b），（c）和（d）[其中（a）+（b）+（c）+（d））= 100重量的单体混合物制备的平均粒径为50-500nm ％）：（a）5-25重量％的选自丙烯酸，甲基丙烯酸，衣康酸和巴豆酸的不饱和酸中的至少一种，（b）20-95重量％的至少一种烷基其碳原子数为1-12的甲基丙烯酸酯，（c）0-30重量％的碳原子数为1-12的烷基丙烯酸烷基酯中的至少一种，（d）0-40重量％的至少一种选自芳族乙烯基，分子中具有至少两个可聚合官能团的化合物和可与上述（a），（b）和（c）共聚的乙烯基氰化物）。橡胶胶乳和含有它的接枝共聚物和结合所说接枝共聚物的热塑性树脂具有优异的冲击强度，耐热性和可加工性。

7. 发明授权

US5798414A Resin composition excellent in impact strength 失效
标题翻译：树脂成分冲击强度优异
公开(公告)号：US5798414A
公开(公告)日：1998-08-25
申请号：US656295
申请日：1996-06-13
申请人： Ikuhiro Mishima , Norito Doi , Youichi Matsumura , Shigemi Matsumoto
发明人： Ikuhiro Mishima , Norito Doi , Youichi Matsumura , Shigemi Matsumoto
IPC分类号： C08L25/02 , C08L25/08 , C08L51/04
CPC分类号： C08L25/08 , C08L25/02 , C08L51/04 , C08L2205/02
摘要： A resin composition is disclosed, which comprizes (I) a graft copolymer using a medium-size rubber particles grown by an acid-group-containing latex, (II) a graft copolymer using small-size rubber particles, (III) a styrene-acrylonitrile copolymer, and/or (IV) a styrene-maleimide copolymer, said resin composition containing 5-40 weight % of rubber. The resin composition is not only superior in impact strength, planar impact strength in particular and gloss, but is favorable in moldability and heat resistance.
摘要翻译： PCT No.PCT / JP95 / 02243 Sec。 371日期：1996年6月13日 102（e）1996年6月13日PCT 1996年11月2日PCT PCT。公开号WO96 / 15188 日期1996年5月23日公开了一种树脂组合物，其包括（I）使用由含酸基的胶乳生长的中等尺寸的橡胶颗粒的接枝共聚物，（II）使用小尺寸橡胶颗粒的接枝共聚物（III ）苯乙烯 - 丙烯腈共聚物和/或（IV）苯乙烯 - 马来酰亚胺共聚物，所述树脂组合物含有5-40重量％的橡胶。该树脂组合物的冲击强度，平面冲击强度，光泽度均不但优异，而且成型性和耐热性也良好。

8. 发明申请

US20060110592A1 Acrylic film and laminates comprising the same 有权
标题翻译：丙烯酸膜和包含其的层压制品
公开(公告)号：US20060110592A1
公开(公告)日：2006-05-25
申请号：US10531282
申请日：2002-12-19
申请人： Norito Doi , Takao Shibata , Yoichi Matsumura , Shigemi Matsumoto
发明人： Norito Doi , Takao Shibata , Yoichi Matsumura , Shigemi Matsumoto
IPC分类号： B32B27/30 , C08L51/00
CPC分类号： C08L33/10 , C08J5/18 , C08J2333/10 , C08J2351/04 , C08L33/12 , C08L51/04 , Y10T428/254 , Y10T428/31935 , C08L2666/24
摘要： To provide an acrylic film, composed of a resin composition (C) that includes an acrylic graft copolymer (A) containing an acrylic ester rubber-like polymer and a methacrylic polymer (B) containing 80% by weight or more of methyl methacrylate, wherein (1) the content of the acrylic ester rubber-like polymer in the resin composition (C) is 5% by weight or more and 30% by weight or less, (2) the average particle size of the acrylic ester rubber-like polymer is 500 to 2000 Å, (3) the relationship between the average particle size d (Å) of the acrylic ester rubber-like polymer and the amount w (% by weight) of crosslinking agent used in the acrylic ester rubber-like polymer satisfies the following equation: 0.002d≦w≦0.005d, (4) the graft ratio of the acrylic graft copolymer (A) is 30% or more and 200% or less, and (5) the reduced viscosity of methyl ethyl ketone soluble matter in the resin composition (C) is 0.2 to 0.8 dl/g.
摘要翻译：为了提供一种由含有丙烯酸酯类橡胶状聚合物的丙烯酸接枝共聚物（A）和含有80重量％以上的甲基丙烯酸甲酯的甲基丙烯酸系聚合物（B）的树脂组合物（C）构成的丙烯酸系膜，其中，（1）树脂组合物（C）中丙烯酸酯类橡胶状聚合物的含量为5重量％以上且30重量％以下，（2）丙烯酸酯类橡胶状聚合物的平均粒径为500〜2000埃，（3）丙烯酸酯类橡胶状聚合物的平均粒径d（）与丙烯酸酯类橡胶状聚合物中使用的交联剂的w（重量％）的量之间的关系满足以下等式：0.002d <= w <= 0.005d，（4）丙烯酸接枝共聚物（A）的接枝率为30％以上且200％以下，（5）甲基乙基酮的比浓粘度树脂组合物（C）中的可溶物质为0.2〜0.8dl / g。

9. 发明授权

US07195816B2 Acrylic film and laminates comprising the same 有权
标题翻译：丙烯酸膜和包含其的层压制品
公开(公告)号：US07195816B2
公开(公告)日：2007-03-27
申请号：US10531282
申请日：2002-12-19
申请人： Norito Doi , Takao Shibata , Yoichi Matsumura , Shigemi Matsumoto
发明人： Norito Doi , Takao Shibata , Yoichi Matsumura , Shigemi Matsumoto
IPC分类号： B32B5/16 , B32B27/30 , C08G63/48 , C08L31/02 , C08L33/06
CPC分类号： C08L33/10 , C08J5/18 , C08J2333/10 , C08J2351/04 , C08L33/12 , C08L51/04 , Y10T428/254 , Y10T428/31935 , C08L2666/24
摘要： To provide an acrylic film, composed of a resin composition (C) that includes an acrylic graft copolymer (A) containing an acrylic ester rubber-like polymer and a methacrylic polymer (B) containing 80% by weight or more of methyl methacrylate, wherein (1) the content of the acrylic ester rubber-like polymer in the resin composition (C) is 5% by weight or more and 30% by weight or less, (2) the average particle size of the acrylic ester rubber-like polymer is 500 to 2000 Å, (3) the relationship between the average particle size d (Å) of the acrylic ester rubber-like polymer and the amount w (% by weight) of crosslinking agent used in the acrylic ester rubber-like polymer satisfies the following equation: 0.002d≦w≦0.005d, (4) the graft ratio of the acrylic graft copolymer (A) is 30% or more and 200% or less, and (5) the reduced viscosity of methyl ethyl ketone soluble matter in the resin composition (C) is 0.2 to 0.8 dl/g.
摘要翻译：为了提供一种由含有丙烯酸酯类橡胶状聚合物的丙烯酸接枝共聚物（A）和含有80重量％以上的甲基丙烯酸甲酯的甲基丙烯酸系聚合物（B）的树脂组合物（C）构成的丙烯酸系膜，其中，（1）树脂组合物（C）中丙烯酸酯类橡胶状聚合物的含量为5重量％以上且30重量％以下，（2）丙烯酸酯类橡胶状聚合物的平均粒径为500〜2000埃，（3）丙烯酸酯类橡胶状聚合物的平均粒径d（）与丙烯酸酯类橡胶状聚合物中使用的交联剂的w（重量％）的量之间的关系满足以下等式：0.002d <= w <= 0.005d，（4）丙烯酸接枝共聚物（A）的接枝率为30％以上且200％以下，（5）甲基乙基酮的比浓粘度树脂组合物（C）中的可溶物质为0.2〜0.8dl / g。

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