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1. 发明授权

US4757144A Preparing tertiary amine from formaldehyde and primary and/or secondary amine 失效
标题翻译：从甲醛和伯胺和/或仲胺制备叔胺
公开(公告)号：US4757144A
公开(公告)日：1988-07-12
申请号：US913621
申请日：1986-09-30
申请人： Kazuhiko Okabe , Yukinaga Yokota , Kazuhito Matsutani , Tatuhiro Imanaka
发明人： Kazuhiko Okabe , Yukinaga Yokota , Kazuhito Matsutani , Tatuhiro Imanaka
IPC分类号： C07B61/00 , B01J23/00 , B01J23/40 , C07B43/04 , C07C67/00 , C07C209/00 , C07C209/26 , C07C211/09 , C07C211/17 , C07C211/22 , C07C213/02 , C07C215/12 , C07D295/12 , C07C85/08 , C07C87/127 , C07C87/14 , C07C87/28
CPC分类号： C07C209/26 , C07C211/08 , C07C211/12 , C07C211/34 , C07C213/08 , C07C215/12 , C07D295/13 , B01J23/42 , B01J23/44
摘要： A tertiary amine is effectively prepared by reacting a primary or secondary amine with formaldehyde in the presence of a palladium or platinum catalyst at a hydrogen pressure of 3 to 50 kg/cm2 (gauge pressure) at a temperature of 80.degree. to 180.degree. C., by controlling the addition of formaldehyde to the starting amine.
摘要翻译：在钯或铂催化剂的存在下，在氢压为3〜50kg / cm 2（表压）下，在80〜180℃的温度下，使伯胺或仲胺与甲醛反应，可有效制备叔胺。，通过控制向起始胺中加入甲醛。

2. 发明授权

US4625063A Production of tertiary amine 失效
标题翻译：生产叔胺
公开(公告)号：US4625063A
公开(公告)日：1986-11-25
申请号：US741979
申请日：1985-06-06
申请人： Yukinaga Yokota , Yuji Sawamoto , Hideki Taniguchi , Kazuhiko Okabe
发明人： Yukinaga Yokota , Yuji Sawamoto , Hideki Taniguchi , Kazuhiko Okabe
IPC分类号： B01J23/90 , C07B61/00 , C07C67/00 , C07C209/00 , C07C209/14 , C07C209/16 , C07C209/24 , C07C209/26 , C07C211/03 , C07C211/08 , C07C85/06 , C07C85/08
CPC分类号： C07C209/26 , C07C209/14 , C07C209/16 , C07C211/08
摘要： A tertiary amine of a high purity is prepared from an alcohol or an aldehyde and a primary or second amine at a low temperature, using a catalyst of copper, nickel and an element belonging to the VIII platinum group such as platinum, palladium, ruthenium and rhodium, while removing out water formed by the reaction.
摘要翻译：使用铜，镍和属于VIII铂族的元素如铂，钯，钌的催化剂，在低温下由醇或醛和伯或仲胺制备高纯度的叔胺，铑，同时除去由反应形成的水。

3. 发明授权

US4845002A Toner for development of electrostatically charged image 失效
标题翻译：用于开发静电荷图像的调色剂
公开(公告)号：US4845002A
公开(公告)日：1989-07-04
申请号：US127179
申请日：1987-12-01
申请人： Masao Niki , Shinichiro Yasuda , Yukinaga Yokota , Kazuhiko Okabe
发明人： Masao Niki , Shinichiro Yasuda , Yukinaga Yokota , Kazuhiko Okabe
IPC分类号： G03G9/087 , G03G9/097
CPC分类号： G03G9/08768 , G03G9/09758 , G03G9/09775
摘要： A toner for development of an electrostatically charged image which comprises at least a binder, a colorant and a compound having the formula (I) or (III): ##STR1## wherein A represents a phenol group-containing compound residue,B represents a group of the general formula (II): ##STR2## wherein R.sub.1 and R.sub.4 each represent a methylene or ethylene group,R.sub.2 and R.sub.3 each represent an alkyl, aryl, alkenyl, aralkyl or cyclic alkyl group or R.sub.2 and R.sub.3 may be combined to form a ring,R.sub.5 represents an alkylene group having 1 to 8 carbon atoms or an arylene group, preferably phenylene,R.sub.6 and R.sub.7 each represent a hydrogen atom or an alkyl, aryl, aminoalkyl, aralkyl or cyclic alkyl group having 1 to 8 carbon atoms or R.sub.6 and R.sub.7 may be combined to form a ring,p represents a number of 1 to 200,n.sub.1 and q each is zero or 1, r is zero or an integer of 1 to 3 and n.sub.2 is an integer of 1 to 3 or zero in the formula (I) and a number of 1 to 400 in the formula (III).

4. 发明授权

US4792622A Process for preparation of secondary amine 失效
标题翻译：仲胺的制备方法
公开(公告)号：US4792622A
公开(公告)日：1988-12-20
申请号：US934230
申请日：1986-11-21
申请人： Yukinaga Yokota , Yuzi Sawamoto , Hideki Taniguchi , Kazuhiko Okabe
发明人： Yukinaga Yokota , Yuzi Sawamoto , Hideki Taniguchi , Kazuhiko Okabe
IPC分类号： C07B61/00 , B01J23/00 , B01J23/89 , C07C67/00 , C07C209/00 , C07C209/16 , C07C209/26 , C07C211/02 , C07C211/08 , C07C215/08 , C07C85/08 , C07C85/06
CPC分类号： B01J23/8926
摘要： A secondary amine is effectively prepared by reacting an alcohol or an aldehyde with a primary amine in the presence of a catalyst of copper, nickel and a metal element belonging to the platinum group VIII at a pressure of the atmospheric pressure to 5 kg/cm.sup.2 G at a temperature of 150.degree. to 250.degree. C., while water produced in the reaction is being removed out, and separating the resulting secondary amine from the product mixture.
摘要翻译：在大气压至5kg / cm2G的压力下，在铜，镍和属于铂族VIII族的金属元素的催化剂存在下，使醇或醛与伯胺反应，可有效制备仲胺。温度为150℃至250℃，同时除去反应中产生的水，并将所得仲胺与产物混合物分离。

5. 发明授权

US5023003A Softener composition containing cis- and trans- isomers of ethylenically unsaturated quaternary ammonium salts 失效
标题翻译：含有烯属不饱和季铵盐的顺式和反式异构体的软化剂组合物
公开(公告)号：US5023003A
公开(公告)日：1991-06-11
申请号：US437882
申请日：1989-11-17
申请人： Masaaki Yamamura , Kazuhiko Okabe , Kohshiro Sotoya , Moriyasu Murata
发明人： Masaaki Yamamura , Kazuhiko Okabe , Kohshiro Sotoya , Moriyasu Murata
IPC分类号： D06M13/46 , C11D1/58 , C11D1/62 , C11D3/37 , D06M13/02 , D06M13/322 , D06M13/463 , D06M13/47 , D06M13/473 , D06M13/51 , D06M13/513 , D06M15/643
CPC分类号： C11D3/3738 , C11D1/58 , C11D1/62 , C11D3/373 , C11D3/3742
摘要： A softener composition comprising a quaternary ammonium salt having two hydrocarbon radicals having 12-22 carbon atoms and one unsaturated bond; the stereoisomeric structure of the above salt includes both the cis-isomer and the trans-isomer with the cis-isomer/trans-isomer ratio being in the range of from 25/75-90/10.
摘要翻译：一种软化剂组合物，其包含具有两个具有12-22个碳原子和一个不饱和键的烃基的季铵盐; 上述盐的立体异构结构包括顺式异构体和反式异构体，顺式异构体/反式异构体比例在25 / 75-90 / 10的范围内。

6. 发明授权

US4709045A Process for producing 1,2-substituted imidazoline compounds 失效
标题翻译： 1,2-取代咪唑啉化合物的制备方法
公开(公告)号：US4709045A
公开(公告)日：1987-11-24
申请号：US871651
申请日：1986-06-06
申请人： Makoto Kubo , Koshiro Sotoya , Kazuhiko Okabe
发明人： Makoto Kubo , Koshiro Sotoya , Kazuhiko Okabe
IPC分类号： C07D233/16 , C07D233/06 , C07D233/04
CPC分类号： C07D233/06
摘要： A 1,2-substituted imidazoline compound having the formula (I): ##STR1## in which R2 is an alkyl or alkenyl group having 8 to 22 carbon atoms and n is 2 or 3, is produced by (1) feeding in a reactor a dialkylenetriamine (II) with a higher fatty acid of R2COOH or an ester thereof (III) at a molar ratio of the compound (III) to the compound (II) in the range of 1.5:1 to 1.8:1, (2) effecting the reaction at an internal temperature of 100.degree. to 250.degree. C. at a reduced pressure, (3) adding to the reaction mixture so that the above defined molar ratio in total may reach at least 2.0:1 and (4) continuing the reaction at an internal temperature of 100.degree. to 250.degree. C. at a reduced pressure. The reaction proceeds with a high yield of the product (I), without by-production to primary and second amines.
摘要翻译：具有式（I）的1,2-取代咪唑啉化合物：其中R2是具有8-22个碳原子的烷基或烯基，n为2或3的式（I）化合物是通过（1）进料在反应器中，化合物（III）与化合物（II）的摩尔比在1.5:1至1.8:1的范围内具有R2COOH的高级脂肪酸或其酯（III）的二烷基三胺（II）（2）在减压下在内部温度为100-250℃下进行反应，（3）加入到反应混合物中，使得上述定义的摩尔比可以达到至少2.0:1，和（4 ）在减压下在内温100℃至250℃下继续反应。反应以高产率的产物（I）进行，而不会副产生到伯和仲胺。

7. 发明授权

US5425891A Detergent composition containing an antifoaming mixture of a soap and a glycerine oxide adduct 失效
标题翻译：含有皂和甘油氧化物加合物的消泡混合物的洗涤剂组合物
公开(公告)号：US5425891A
公开(公告)日：1995-06-20
申请号：US230013
申请日：1994-04-19
申请人： Enrique Pujol , Francisco Pujadas , Antoni Prat , Kazuhiko Okabe
发明人： Enrique Pujol , Francisco Pujadas , Antoni Prat , Kazuhiko Okabe
IPC分类号： C11D1/22 , C11D1/72 , C11D10/04 , C11D1/831 , C11D17/06
CPC分类号： C11D3/0026 , C11D10/045 , C11D1/22 , C11D1/72
摘要： The detergent composition comprises ethoxylated glycerine, compound represented by the formula (I) and fatty acid alkaline metal salt, represented by the formula (II); the weight ratio of the former to the latter [(I)/(II)], being essentially 10/90-90/10, preferably 1/5 to 5/1, and most preferably 1/3 to 3/1. ##STR1## wherein: R' represents H or CH.sub.3, and each of n, m and l independently represents an integer from 0 to 20; being m+n+l=2-60 preferably 10-45.R--COOM (II)wherein R represents alkyl or alkenyl group having C.sub.7-21, and M represents an alkaline metal.The combination of compounds (I) and (II) permits a saving in the amount of antifoaming agents, as well as shows a better performance in skin irritation, oral toxicity and biodegradation, without deteriorating its detergency.
摘要翻译：洗涤剂组合物包含乙氧基化甘油，由式（I）表示的化合物和由式（II）表示的脂肪酸碱金属盐; 前者与后者[（I）/（II）]的重量比基本上为10 / 90-90 / 10，优选为1/5至5/1，最优选为1/3至3/1。（I）其中：R'表示H或CH3，n，m和l各自独立地表示0至20的整数; m + n + 1 = 2-60，优选10-45。 R-COOM（II）其中R表示具有C7-21的烷基或烯基，M表示碱金属。化合物（I）和（II）的组合允许节省消泡剂的量，并且在皮肤刺激，口服毒性和生物降解中表现出更好的性能，而不会降低其去污力。

8. 发明授权

US5403509A Detergent composition comprising a mono-, di- and tri-ester mixture and method of manufacturing same 失效
标题翻译：包含单酯，二酯和三酯混合物的洗涤剂组合物及其制备方法
公开(公告)号：US5403509A
公开(公告)日：1995-04-04
申请号：US93621
申请日：1993-07-20
申请人： Enrique Pujol , Francisco Pujadas , Antonio Prat , Kazuhiko Okabe
发明人： Enrique Pujol , Francisco Pujadas , Antonio Prat , Kazuhiko Okabe
IPC分类号： C11D1/74 , C11D1/825 , C11D1/722 , C11D11/04
CPC分类号： C11D1/74
摘要： A detergent composition comprising a mixture of mono-, di- and tri-ester nonionic compounds represented by formula (I) and a nonionic compound represented by formula (II), wherein the weight ratio of said mono-, di and tri-ester nonionic compounds is 46-90/9-30/1-15, ##STR1## wherein B represents a hydrogen atom or a ##STR2## group and R represents an alkyl or alkenyl group having 6 to 22 carbon atoms, R' represents H or a CH.sub.3 group, and each of n, m and p independently represents an integer from 0 to 40 and m+n+p=2-100; said detergent composition exhibiting outstanding biodegradability, non-toxicity, non-irritancy, foam stability and better dye inhibition transfer, while maintaining and even improving detergency.
摘要翻译：一种洗涤剂组合物，其包含由式（I）表示的单酯，二酯和三酯非离子化合物和由式（II）表示的非离子化合物的混合物，其中所述单酯，二酯和三酯非离子表面活性剂的重量比化合物是46-90 / 9-30 / 1-15，其中B代表氢原子或基团，R代表具有6-22个碳原子的烷基或链烯基碳原子，R'表示H或CH3基，n，m和p各自独立地表示0〜40的整数，m + n + p = 2〜100。所述洗涤剂组合物显示出优异的生物降解性，无毒性，无刺激性，泡沫稳定性和更好的染料抑制转移，同时保持甚至改善去污力。

9. 发明授权

US5266730A Process for preparing N-substituted amine 失效
标题翻译：制备N-取代胺的方法
公开(公告)号：US5266730A
公开(公告)日：1993-11-30
申请号：US529928
申请日：1990-05-29
申请人： Hiroshi Abe , Jun Aikawa , Kazuhiko Okabe , Kohshiro Sotoya
发明人： Hiroshi Abe , Jun Aikawa , Kazuhiko Okabe , Kohshiro Sotoya
IPC分类号： B01J23/76 , B01J23/89 , C07C209/16 , C07C209/26 , C07C209/02 , C07C209/04
CPC分类号： B01J23/8926 , B01J23/76 , B01J23/8933 , B01J23/8946 , B01J23/8986 , B01J23/8993 , C07C209/16 , C07C209/26
摘要： An N-substituted amine is produced by reacting an alcohol or aldehyde with ammonia, a primary amine or a secondary amine in the presence of a catalyst comprising:(a) (1) copper, (2) a metal selected from the group consisting of chromium, manganese, iron and zinc and (3) a metal of the platinum VIII group;(b) (1) copper, (2) cobalt and (3) a metal of the platinum VIII group;(c) (1) copper, (2) a metal selected from the group consisting of chromium, manganese, iron, cobalt, nickel and zinc, (3) a metal of the platinum VIII group and (4) a metal selected from the group consisting of alkali metals and alkaline earth metals; or(d) (1) copper, (2) a metal selected from the group consisting of chromium, manganese, iron, cobalt, nickel and zinc, (3) a metal of the platinum VIII group and (4) a metal selected from the group consisting of aluminum, tungsten and molybdenum.
摘要翻译：通过使醇或醛与氨，伯胺或仲胺在催化剂存在下反应制备N-取代的胺，所述催化剂包含：（a）（1）铜，（2）选自以下的金属：铬，锰，铁和锌和（3）铂VIII族金属; （b）（1）铜，（2）钴和（3）铂VIII族金属; （c）（1）铜，（2）选自铬，锰，铁，钴，镍和锌的金属，（3）铂VIII族金属和（4）由碱金属和碱土金属组成的组; 或（d）（1）铜，（2）选自铬，锰，铁，钴，镍和锌的金属，（3）铂VIII族金属和（4）该组由铝，钨和钼组成。

10. 发明授权

US4885112A Surface active secondary amidoamino acid or salt compounds 失效
标题翻译：表面活性二级酰胺基氨基酸或盐化合物
公开(公告)号：US4885112A
公开(公告)日：1989-12-05
申请号：US118887
申请日：1987-11-10
申请人： Kohshiro Sotoya , Makoto Kubo , Kazuhiko Okabe , Masanobu Tanigaki , Masaji Yamanishi , Hajime Hirota
发明人： Kohshiro Sotoya , Makoto Kubo , Kazuhiko Okabe , Masanobu Tanigaki , Masaji Yamanishi , Hajime Hirota
IPC分类号： B01F17/28 , A61K8/00 , A61K8/41 , A61K8/42 , A61Q5/02 , B01D61/44 , B01D61/48 , B01D61/54 , B01F17/00 , B01F17/38 , C07C67/00 , C07C231/00 , C07C231/12 , C07C233/35 , C07C233/36 , C07C233/38 , C07C235/10 , C11D1/88 , C11D1/90
CPC分类号： B01D61/44 , B01F17/0042 , Y10S516/06
摘要： A surface active agent comprising a specific type of secondary amidoamino acid or ammonium ion or triethanolammonium salt thereof, ##STR1## as a major component, and not more than 0.2 mole of an inorganic salt per 100 gm of said secondary amidoamino acid or 100 gm of a salt thereof as converted to the acid type secondary amidoamino acid. The surface active agent can be prepared by subjecting the alkali metal salt of secondary amidoamino acid, usually containing a great amount of impurities such as sodium chloride, to electrodialysis. It has excellent compatibility with various additives such as water-soluble polymer due to its low ionic strength and yet exhibits a good low-temperature stability when made into an aqueous solution owing to its low Krafft point.
摘要翻译：包含特定类型的二级酰氨基氨基酸或其铵离子或三乙醇铵盐作为主要成分的表面活性剂和每100克所述仲氨基氨基酸不超过0.2摩尔的无机盐或100克其盐转化为酸型仲氨基氨基酸。表面活性剂可以通过将通常含有大量杂质如氯化钠的仲氨基氨基酸的碱金属盐进行电渗析来制备。由于其低离子强度，它与各种添加剂如水溶性聚合物具有优异的相容性，并且由于其低克拉夫特点而在制成水溶液时表现出良好的低温稳定性。

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